This article presents a general description of pulsed-laser deposition. It describes the components of pulsed-laser deposition equipment. The article also discusses the effects of angular distribution of materials. Finally, the article reviews the characteristics of high-temperature superconductors and ferroelectric materials.

Laser-ultrasonics is a particular implementation of ultrasonic nondestructive inspection in which ultrasound is generated and detected by lasers. This article discusses the various mechanisms that ensure ultrasound generation and explains the possibility to get the equivalent of phase-array by numerical processing of an array of previously acquired laser-ultrasonic signals. The article describes the ultrasound generation by thermoelastic mechanism and ablation or vaporization. It illustrates the principle of optical detection of ultrasound with confocal Fabry-Perot interferometer and photorefractive two-wave mixing interferometer. The article concludes with information on the industrial applications of laser-ultrasonics, including thickness measurement, flaw detection, and material characterization.

For most nondestructive evaluation (NDE) applications, the term thermography actually refers to surface-excited thermography (SET) that involves thermal mapping of surface temperature as heat flows from, to, or through a test object in response to excitation applied to the sample surface. This article discusses the strategies for implementing thermography for NDE, including the steady-state/whole-body approach and transient heat conduction. It describes the most common signal-processing methods, such as thermographic signal reconstruction, lock-in thermography, and pulsed-phase thermography. The article concludes with a discussion on the use of thermal methods for thermal diffusivity measurement and characterization of multilayer structures.

Ultrasonic inspection is a family of nondestructive methods in which beams of high-frequency mechanical waves are introduced into materials, using transducers, for the detection and characterization of both surface and subsurface anomalies and flaws in the material. This article describes the basic equipment in ultrasonic inspection systems, and lists the advantages and disadvantages of these systems. It discusses the applications of ultrasonic inspection and also the general characteristics of ultrasonic waves in terms of wave propagation, longitudinal waves, transverse waves, surface waves, and lamb waves. The article reviews the major variables in ultrasonic inspection, including frequency, acoustic impedance, angle of incidence, and beam intensity. It discusses the attenuation of ultrasonic beams and provides information on the pulse-echo and transmission methods for implementing ultrasonic inspection.

Microjoining methods are commonly used to fabricate medical components and devices. This article describes key challenges involved during microjoining of medical device components. The primary mechanisms used in microjoining for medical device applications include microresistance spot welding (MRSW) and laser welding. The article illustrates the fundamental principles involved in MRSW and laser welding. Most multicomponent medical devices implement microjoining techniques to join various forms of materials and geometries. The article presents examples of various microjoining methods used in medical device applications, including pacemaker and nitinol microscopic forceps.

This article endeavors to familiarize the reader with a selection of different ionization designs and instrument components to provide knowledge for sorting the various analytical strategies in the field of solid analysis by mass spectrometry (MS). It begins with a description of the general principles of MS. This is followed by sections providing a basic understanding of instrumentation and discussing the operating requirements as well as practical considerations related to solid sample analysis by MS. Instrumentation discussed include the triple quadrupole mass spectrometer and the time-of-flight mass spectrometer. Inductively coupled plasma and thermal ionization MS provide atomic information, and direct analysis in real-time and matrix-assisted laser-desorption ionization MS are used to analyze molecular compositions. The article describes various factors pertinent to ionization methods, namely glow discharge mass spectrometry and secondary ion mass spectrometry. It concludes with a section on various examples of applications and interpretation of MS for various materials.

Nontraditional finishing processes include electrochemical machining (ECM), electrodischarge machining (EDM), and laser beam machining. These processes belong to nonabrasive finishing methods where surface generation occurs with an insignificant amount of mechanical interaction between the processing tool and the workpiece surfaces. This article provides information on the equipment used, applications, process capabilities, and limitations of ECM and EDM.

This article discusses the advantages, disadvantages, applications, and selection criteria of various technologies and transduction modalities that can generate and detect ultrasonic waves. These include piezoelectric transducers, electromagnetic acoustic transducers (EMATs), laser ultrasound phased array transducers, magnetostriction transducers, and couplants. The article discusses four basic types of search units with piezoelectric transducers. These include the straight-beam contact type, the angle-beam contact type, the dual-element contact type, and the immersion type. The article concludes with information on immersion or contact type focused search units.

This article discusses the fundamentals and operating principles of the following acoustic microscopy methods: scanning laser acoustic microscopy, C-mode scanning acoustic microscopy, and scanning acoustic microscopy. It describes the applications of acoustic microscopy for detecting defects in metals, ceramics, glasses, polymers, and composites with examples.

This article discusses the fundamentals and applications of localized heat treating methods: induction hardening and tempering, laser surface transformation hardening, and electron-beam heat treatment. The article provides information about equipment and describes the selection of frequency, power, duration of heating, and coil design for induction hardening. The article also discusses the scope, application, methods, and operation of flame hardening.

This article provides an overview of the characteristics of Rayleigh waves plus methods for generation and detection of waves, including using piezoelectric transducers or noncontact techniques such as lasers, electromagnetic acoustic transducers, or air-coupled ultrasonics. It reviews the methods for using Rayleigh waves for defect detection and materials characterization, alongside nonlinear ultrasonic inspection and surface acoustic wave (SAW) microscopy. The article concludes with information on the standards that use Rayleigh waves for nondestructive evaluation (NDE) of different structures.

Ceramics usually require some form of machining prior to use to meet dimensional and surface quality standards. This article focuses on abrasive machining, particularly grinding, and addresses common methods and critical process factors. It covers cylindrical, centerless, and disk grinding and provides information on tooling, wheel selection, work material, and operational factors. It also discusses precision slicing and slotting, lapping, honing, and polishing as well as abrasive waterjet, electrical discharge, laser, and ultrasonic machining.

This article reviews cleaning and finishing operations that have proven to be effective on titanium, its alloys, and semi-fabricated titanium products. It explains how to remove scale, tarnish films, grease, and other soils and how to achieve required finishes and/or improve wear and oxidation resistance through the use of polishing, buffing, and wire brushing operations. The article also covers a wide range of surface modification and coating processes, including ion implantation, diffusion, chemical and physical vapor deposition, plating, anodizing, and chemical conversion coatings as well as sprayed and sol-gel coatings and laser and electron-beam treatments.

This article introduces the principal methodologies and some advanced technologies that are being applied for nondestructive evaluation (NDE) of fiber-reinforced polymer-matrix composites. These include acoustic emission, ultrasonic, eddy-current, computed tomography, electromagnetic acoustic transducer, radiography, thermography, and low-frequency vibration methods. The article also provides information on NDE methods commonly used for metal-matrix composites.

This article is a detailed account of optical emission spectroscopy (OES) for elemental analysis. It begins with a discussion on the historical background of OES and development trends in OES methods. This is followed by a description of the general principles and optical systems of OES, along with various types of emission sources commonly used for OES. Some of the processes involved in calibration and quantification of OES for direct solids analysis by the ratio method are then described. The article ends with a discussion on the applications of each type of emission sources.

This article discusses the basic principles of inductively coupled plasma mass spectrometry (ICP-MS), covering different instruments used for performing ICP-MS analysis. The instruments covered include the sample-introduction system, ICP ion source, mass analyzer, and ion detector. Emphasis is placed on ICP-MS applications in the semiconductor, photovoltaic, materials science, and other electronics and high-technology areas.

Holography is basically a two-step process for creating a whole three dimensional image of a diffusely reflecting object having some arbitrary shape. This article discusses the advantages, disadvantages and applications of using the optical holography method in nondestructive evaluation. It also discusses the types of acoustical holography, including liquid-surface acoustical holography and scanning acoustical holography. The article concludes by comparing liquid-surface and scanning systems.

This article uses metal and alloy powders as examples to briefly discuss how to perform the characterization of powders. It begins by reviewing some of the techniques involved in the sampling of powders to ensure accurate characterization. This is followed by a discussion on the important properties to characterize powders, namely the particle size, surface area, density, porosity, particle hardness, compressibility, green strength, and flowability. For characterization of powders, both individual particles and bulk powders are used to evaluate their physical and chemical properties. The article also discusses the important characteristics and compositions of powder as well as impurities that directly affect powder properties. It ends with a description of the ignition and dust-explosion characteristics of organic and metal powders.

This article describes various methods of electrochemical analysis, namely coulometry, electrogravimetry, voltammetry, electrometric titration, and nanometer electrochemistry. The discussion covers the general uses, sample requirements, application examples, advantages, and limitations of these methods. Some of the factors pertinent to electrochemical cells are also provided. In addition, the article provides information on various potentiometric membrane electrodes used to quantify numerous ionic and nonionic species.