Search Results for pressure-assisted sintering

Sintering is a thermal treatment process in which a powder or a porous material, already formed into the required shape, is converted into a useful article with the requisite microstructure. Sintering can be classified as solid-state, viscous, liquid-phase, and pressure-assisted (or pressure) sintering. This article provides information on the mechanisms and theoretical analysis of sintering and focuses on the types, mechanisms, process and microstructural variables, computer simulation, stages, and fundamentals of densification and grain growth of solid-state sintering and liquid-phase sintering. It describes the models for viscous sintering and the methods used in pressure-assisted sintering, namely, uniaxial hot pressing, hot isostatic pressing, sinter forging, and spark plasma sintering.

This article discusses two major sintering methods: pressureless and pressure-assisted sintering. Pressureless sintering techniques include vacuum and partial-pressure, hydrogen, and microwave sintering. Pressure-assisted consolidation techniques include overpressure sintering, sintering followed by postsinter hot isostatic pressing, hot pressing, and several rapid hot consolidation techniques. The article describes nitrogen sintering and the sintering of cermets. It reviews the furnaces used for sintering and presents the lubrication removal techniques. The article also outlines the need to control carbon and oxygen to obtain optimal properties and explains microstructure development and grain size control.

The application of three-dimensional printers can be revolutionary as a tool for the customization and personalization of pharmaceutical dosage forms. The areas of 3D printing applicable to pharmaceutical manufacturing can be segregated into three categories: extrusion technologies, powder-bed fusion, and stereolithography. Common extrusion-based technologies are fused deposition modeling and pressure-assisted microsyringe; powder-bed fusion is separated by binder jet and selective laser sintering. The synergies between pharmaceutical, or active pharmaceutical ingredient (API), and polymer printing are discussed in this article, with particular attention to how the incorporation of small-molecule APIs changes the material selection, design considerations, processing parameters, and challenges associated with each technology.

This article reviews various segments of the powder metallurgy (PM) process from powder production and powder processing through the characterization of the materials and their properties. It covers the processing methods for consolidating metal powders including options for processing to full density. The article outlines the freeform fabrication process, also known as additive manufacturing and describes finishing operations of PM parts. It concludes with information on the applications of PM parts.

This article describes part selection, feedstock (powders and binders) characteristics and properties, tool design, and material and tooling for fabrication of metal powder injection molding (MIM) machines. It discusses the process parameters, operation sequence, molding machines, debinding techniques, consolidation (sintering) techniques, advantages, and limitations of MIM.

This article presents the governing equations and methodologies to model the press and sinter powder metallurgy, including continuum, micromechanical, multiparticle, and molecular dynamics approaches. It describes the constitutive relation for compaction and sintering. The article discusses the experimental determination of material properties and simulation verification for compaction and sintering. It reviews the use of modeling and simulation of press and sinter powder metallurgy, including gravitational distorting in sintering, compaction optimization, sintering optimization, and coupled press and sinter optimization.

This article discusses continuum modeling, which is the most relevant approach in modeling grain growth, densification, and deformation during sintering. Continuum plasticity models are frequently used to describe the mechanical response of metal powders during compaction. The article illustrates the typical procedure for computer simulation for press and sinter process. It describes the procedure to obtain the material properties based on the generalized Shima-Oyane model. The article presents a wide variety of tests, accounting for data on the grain growth, densification, and distortion where these data help in the development of a constitutive model for sintering simulation. Finally, the article provides information on the simulation approaches used to optimize die compaction and sintering.

Friction materials are the components of a mechanism that converts mechanical energy into heat upon sliding contact. This article discusses the selection criteria, manufacturing process, and applications of friction powder metallurgy materials. It provides information on the manufacturing process of powder metallurgy friction materials through a process of mixing/blending, compacting, and sintering. The final machining that they undergo, to ensure that they meet dimensional specifications, is also discussed.

This article discusses the pressing and sintering of various refractory metal powders for the production of intermediate products as well as special cases of finished products. The metal powders considered include tungsten, molybdenum, tantalum, niobium and their alloys, as well as rhenium.

This article provides an overview of the compaction of metal powder in a rigid die and reviews the compaction characteristics of stainless steel powders, including green density, compressibility, green strength, apparent density, flow rate, and sintered density. It describes the influence of compaction characteristics of stainless steel powders in tool materials selection, lubrication, annealing, double pressing/double sintering, and warm compaction.

This article characterizes the physical differences between powder metallurgy (PM) and wrought or cast materials, as they apply to joining. It discusses acceptable joining procedures and techniques, including welding and brazing and solid-state methods. Information on the weldability of various PM materials is presented. The article also describes the effects of porosity on several important properties that affect the welding characteristics.

This article discusses the requirements for safe design, installation, operation, inspection, testing, and maintenance of sintering atmosphere generators and atmosphere supply systems for both personal and environment safety. The four intrinsic dangers associated with producing and using common sintering atmosphere gases are explosion, fire, toxicity, and asphyxiation.

Sintering provides the interparticle bonding that generates the attractive forces needed to hold together the otherwise loose ceramic powder mass. It also improves hardness, strength, transparency, toughness, electrical conductivity, thermal expansion, magnetic saturation, corrosion resistance, and other properties. This article discusses the fundamentals of sintering and its effects on pore structures and particle density. It addresses some of the more common sintering methods, including solid-state, liquid-phase, and gas pressure sintering, and presents alternative processes such as reaction sintering and self-propagating, high-temperature synthesis. It also describes several pressure densification methods, including hot isostatic pressing, gas pressure sintering, molten particle deposition, and sol-gel processing. The article concludes with a section on grain growth that discusses the underlying mechanisms and kinetics and the relationship between grain growth and densification.

This article provides an overview of key abradable thermal spray coating systems based on predominant function and key design criteria. It describes two families of coatings which have evolved for use at higher temperature: flame (combustion)-sprayed abradable powders and atmospheric plasma-sprayed abradable powders. Three classic examples of flame spray abradables are nickel-graphite powders, NiCrAl-bentonite powders, and NiCrFeAl-boron nitride powders. The article provides information on various abradable coating testing procedures, namely, abradable incursion testing; aging, corrosion, thermal cycle and thermal shock testing; hardness testing; and erosion resistance testing.

Directed-energy deposition (DED) is a kind of additive manufacturing (AM) technology based on synchronous powder feeding or wire feeding. This article provides a comprehensive coverage of DED for ceramic AM, beginning with an overview of DED equipment setup, followed by a discussion on DED materials and the DED deposition process. The bulk of the article is devoted to the discussion on the microstructure and properties of oxide ceramics, namely alumina and zirconia ceramics.

This article begins with a discussion on general powder metallurgy design considerations that assist in the selection of the appropriate processing method. It reviews powder processing techniques, conventional press-and-sinter methods, and full-density processes to understand the design restrictions of each powder processing method. The article provides comparison of powder processing methods based on their similarities, differences, advantages, and disadvantages. It concludes with a discussion on design issues for the components of powder processing technologies.

This article describes the capabilities, limitations, advantages, and disadvantages of the powder metallurgy (PM) gear manufacturing process. It discusses the types of gears that can be produced by PM and presents the design guidelines for PM gears. The article provides information on gear tolerances and performance of PM gears. It also explains various procedures to inspect and test the mechanical properties, dimensional specifications, and surface durability (hardness).