Milling of materials, whether hard and brittle or soft and ductile, is of prime interest and of economic importance to the powder metallurgy (PM) industry. This article discusses the principles of milling, milling parameters, and the powder characteristics required for the process. It discusses the changes in powder particle morphology that occur during milling of metal powders produced by various processes such as microforging, fracturing, agglomeration, and deagglomeration. The article also provides useful information on milling equipment such as tumbler ball mills, vibratory ball mills, attrition mills, and hammer and rod mills.

Particle image analysis of metal powders can be easily performed with optical macroscopes and microscopes. This article provides examples of the particle image analysis on powders used in the powder metallurgy industry.

This article provides an overview of the general methods of metal powder production. It details the primary methods for particle sizing used in additive manufacturing: sieving, laser diffraction and scattering, and digital image analysis. Methods of interpreting and understanding particle size distribution (PSD) data are presented, with an emphasis on the differences between count- and volume-based PSDs. The article then outlines practices for both qualitative and quantitative assessment of particle morphology.

This article uses metal and alloy powders as examples to briefly discuss how to perform the characterization of powders. It begins by reviewing some of the techniques involved in the sampling of powders to ensure accurate characterization. This is followed by a discussion on the important properties to characterize powders, namely the particle size, surface area, density, porosity, particle hardness, compressibility, green strength, and flowability. For characterization of powders, both individual particles and bulk powders are used to evaluate their physical and chemical properties. The article also discusses the important characteristics and compositions of powder as well as impurities that directly affect powder properties. It ends with a description of the ignition and dust-explosion characteristics of organic and metal powders.

Calcium phosphates react to form more stable salts in aqueous solutions. This phenomenon has been applied to the solidification process for the dental and medical cement calcium phosphate cement, which consists of multiple phases of calcium phosphates and calcium salts; solidification occurs by the formation of hydroxyapatite. Dicalcium phosphate consists of crystal water along with anhydrous and dihydrate salts. This article summarizes research achievements regarding dicalcium phosphate dihydrate (DCPD) production with controlled morphology and reactivity, including effects of an additive and of production conditions on precipitation. It also summarizes achievements made in the hybridization of nano-apatite onto DCPD particles.

This article briefly describes the production of beryllium powder and beryllium/beryllium oxide metal-matrix powder. It discusses fully dense consolidation methods: vacuum hot pressing, hot isostatic pressing, and cold isostatic pressing. Secondary fabrication operations of beryllium and aluminum-beryllium alloys such as extrusion, rolling, welding, joining, and machining are discussed. The article discusses quality control and provides information on the structural, optical, and high-purity grades of beryllium.

Friction materials are the components of a mechanism that converts mechanical energy into heat upon sliding contact. This article discusses the selection criteria, manufacturing process, and applications of friction powder metallurgy materials. It provides information on the manufacturing process of powder metallurgy friction materials through a process of mixing/blending, compacting, and sintering. The final machining that they undergo, to ensure that they meet dimensional specifications, is also discussed.

This article provides an overview of the compaction of metal powder in a rigid die and reviews the compaction characteristics of stainless steel powders, including green density, compressibility, green strength, apparent density, flow rate, and sintered density. It describes the influence of compaction characteristics of stainless steel powders in tool materials selection, lubrication, annealing, double pressing/double sintering, and warm compaction.

The raw materials used in thermal spray processes are a critical parameter in the finished coating because the variations in their size, morphology, chemistry, and phase composition can significantly impact coating properties. Therefore, it is important to test and characterize the raw materials. This article discusses various characterization methods for powders. Topics discussed include: methods for determining particle size and/or size distribution; powder and coating stoichiometry; particle chemistry; and phase analysis by x-ray diffraction. This article discusses the characterization of thermal spray powders which involves the determination of particle size and/or size distribution and phase analysis by x-ray diffraction. It provides information on preferential volatilization and rapid solidification that influence compositional differences. Wet chemical methods, spectographic analysis, and atomic absorption spectrometry are also discussed.

This article discusses three types of powder-feeder systems that are commonly used throughout the thermal spray (TS) industry: gravity-based devices, rotating wheel devices, and fluidized-bed systems. It provides information on the various mechanical methods for producing powders, namely, crushing, milling, attriting, and machining. The article describes two prime methods of agglomeration. One method uses a binder by way of agglutination, while the other relies on a sintering operation. The article discusses the technology and principles of the processes that relate to thermal spraying, and offers an understanding for choosing particular feedstock materials that are classified based on the thermal spray process, material morphology, chemical nature of the material, and applications. Sieving, the most common method of separating powders into their size fractions, is also reviewed. The article also provides information on the topical areas and precautions to be undertaken to protect the operator from safety hazards.

This article focuses on the production of particulate reinforcements that are used in discontinuously reinforced metal-matrix composite (DRMMC) materials systems, their physical and materials properties, and the particle shape and overall morphology. The most common DRMMC materials systems used for aerospace structural applications are silicon carbide and boron carbide particulate reinforcement in an aluminum alloy matrix. The article concludes with information on reinforcement chemistry for designing DRMMC materials systems.

This article discusses the production of aluminum and aluminum alloy powders with emphasis on the gas atomization method and the atomizing nozzle. It illustrates the particle formation mechanism and details the requisites for particle size distribution, control, and morphology. The article presents information on the mean oxide thickness formed on atomized powders. It also describes the mechanical and physical properties of aluminum and aluminum alloy powders, as well as their applications.

This article describes the methods for determining the flow rate of metal powders. It examines the factors affecting flow rate, apparent density, and angle of repose of metal powders. The article reviews the frictional properties, cohesive strength, frictional properties, tap density, and compressibility of metal powders. It explains the mechanisms of powder segregation. The article provides information on green strength and springback value of rectangular test bar. It concludes with a discussion on the chemical composition of metal powders.

The highly irregular morphologies of ceramic powder particles due to their process history present a challenge to binder jetting additive manufacturing (BJ-AM) ceramic powder feedstock processability, but knowledge of powder metallurgy of ceramics benefits the development and analysis of the BJ-AM ceramic processes. Understanding BJ-AM process principles and ceramics processing challenges requires reviewing a number of fundamental principles, which this article delineates. The discussion covers the processability considerations, a brief summary of some fundamental aspects of modeling of liquid permeation in the powder bed, and process capabilities and advantages of BJ-AM technology.

This article provides an overview of the supply chain for metallic additively manufactured materials, with an emphasis on spherical alloy powders. The article describes powder production processes as well as the various metal alloys that can be produced using powder AM techniques. It also reviews the basic characteristics of powder feedstocks and the management of metallic powders.

This article discusses various control processes carried out in powder feeding, thermal spraying, and gas flow of the thermal spray process to standardize the coating quality. Quality of the entire powder feeding process can be achieved by controlling the processing of feeding equipment as well as the characteristics of the powder being fed. Gas flow control can be achieved by using rotameters, critical orifices, and thermal mass flowmeters, whose ability to provide useful information is defined by their resolution, accuracy, linearity, and repeatability. The commercial thermal spray controls discussed here include the open-loop input-based, open-loop output-based, closed-loop input-based, and closed-loop output-based or adaptive controls. The article discusses the common causes and practical solutions for arc starting problems. It also outlines certain important developments in measuring individual and collective particle velocities, temperature, and trajectories as well as other plume characteristics for the plasma spray process.