This article summarizes sampling of powders, which includes the sampling of stored material and flowing streams, sample reduction and evaluation, and weight of sample required. It also summarizes the classification of powders. Classifiers are divided into two categories: counterflow equilibrium and crossflow separation. Classification methods are used to exclude certain powder sizes from a powder distribution and to obtain particular powder distributions. For example, sieving methods are used to obtain particular powder distributions and to obtain narrow size ranges of a powder. The article summarizes the sieving methods for powders. The sieving methods include hand sieving, machine sieving, manual wet sieving, air jet sieving, sonic sifter, wet sieving by machine, the Seishin robot sifter, automated systems, and ultrasonic machine sieving. The article outlines the sieve types and the process variables of the sieving process. An appendix reviews dispersion of powders in liquids.

Particle size and size distribution have a significant effect on the behavior of metal powders during their processing. This article provides an overview of the sample preparation process for particle size measurement, which is a key step in the measurement of particle size distributions. Common particle size measuring techniques discussed in this article include sieve analysis, quantitative image analysis, laser diffraction, sedimentation methods, aerodynamic time-of-flight method, electrical zone sensing, and photon correlation spectroscopy. The advantages and disadvantages of these methods are reviewed.

This article provides a basic introduction to the various aspects of full density powder metallurgy, including properties, applications, processing methods, and process parameters.

This article discusses the characteristics, properties, and production methods of copper powders and copper alloy powders. Bulk of the discussion is devoted to production and applications of powder metallurgy (P/M) parts, including pure copper P/M parts, bronze P/M parts, brass and nickel silver P/M parts, copper-nickel P/M parts, copper-lead P/M parts, copper-base P/M friction materials, copper-base P/M electrical contact materials, copper-base P/M brush materials, infiltrated parts, and oxide-dispersion-strengthened copper P/M materials.

This article explains how ceramic powders are made. It begins by briefly describing the raw materials used in structural clay products, whitewares, refractories, and advanced ceramics. It then examines various additives that promote uniformity at different stages of the process. After a description of the comminution process (wet and dry milling methods), it discusses batching and mixing operations and granulation methods. The article also deals with the effect of process variables and the steps involved in chemical synthesis, including preparation from solution and gas-phase reactions, filtration and washing, and powder recovery techniques. It concludes with a discussion on characterization, centering on size distribution analysis, specific surface area, density, porosity chemical composition, phase, and surface composition.

This article provides information on the microstructure of powder metal alloys and the special handling requirements of porous materials. It covers selection, sectioning, mounting, grinding, and polishing, and describes procedures, such as washing, liquid removal, and impregnation, meant to preserve pore structures and keep them open for analysis. The article compares and contrasts the microstructures of nearly 50 powder metal alloys, using them to illustrate the effect of consolidation and compaction methods as well as particle size, composition, and shape. It discusses imaging equipment and techniques and provides data on etchants and etching procedures.

The discovery of the high-critical-temperature oxide superconductors has accelerated the interest for superconducting applications due to its higher-temperature operation at liquid nitrogen or above and thus reduces the refrigeration and liquid helium requirement. It also permits usage of the high-critical-temperature oxides in magnets or power applications in high-current-carrying wire or tape with acceptable mechanical capability. This article discusses the powder techniques mainly based on the production of an oxide powder precursor, which is then subjected to various processing, including powder-in-tube processing, vapor deposition processing, and melt processing. It further discusses the microstructural, anisotropy and weak link influences on these processes.

This article discusses three types of powder-feeder systems that are commonly used throughout the thermal spray (TS) industry: gravity-based devices, rotating wheel devices, and fluidized-bed systems. It provides information on the various mechanical methods for producing powders, namely, crushing, milling, attriting, and machining. The article describes two prime methods of agglomeration. One method uses a binder by way of agglutination, while the other relies on a sintering operation. The article discusses the technology and principles of the processes that relate to thermal spraying, and offers an understanding for choosing particular feedstock materials that are classified based on the thermal spray process, material morphology, chemical nature of the material, and applications. Sieving, the most common method of separating powders into their size fractions, is also reviewed. The article also provides information on the topical areas and precautions to be undertaken to protect the operator from safety hazards.

This article briefly reviews the subject of copper-base powder-metallurgy (P/M) products in terms of powder production methods (atomization, oxide reduction, electrolysis, and hydrometallurgy) and the product properties/consolidation practices of the major applications. Of the four major methods for making copper and copper alloy powders, atomization and oxide reduction are presently practiced on a large scale in North America. The article provides information on the mechanism, production, properties, composition and applications of different types of copper-base P/M products, including self-lubricating sintered bearings, structural parts, oxide-dispersion-strengthened copper, sintered metal friction materials, and porous filters.

Liquid-penetrant inspection is a nondestructive method used to find discontinuities that are open to the surface of solid, essentially nonporous materials. This article describes the physical principles and the process of liquid-penetrant inspection. It also describes the basic penetrant systems, such as the water-washable system, the post-emulsifiable system, and the solvent-removable system. The article provides information on the liquid-penetrant materials, emulsifiers, solvent cleaners, and developers. It details the equipment requirements, selection of penetrant system, and specifications and standards for the liquid-penetrant inspection.

This article surveys common additive manufacturing (AM) data-acquisition methods, covering preprocess materials characterization in the lab, machine calibration in the field, in-process monitoring during a build, and the postprocess part inspections and tests. The focus is to identify acquisition-related metadata for AM data sets to improve data usability and reusability. Also included in the article are exemplar metadata definitions for a data set acquired from light-scattering-based particle size analysis.

High-temperature sintering of ferrous components continues to be important in the powder metallurgy (PM) industry. Improvements in both production rates and properties are possible as sintering temperatures increase above 1120 deg C. This article provides an overview of the different various stages of the sintering process and the physical, chemical, and metallurgical phenomena occur within the mass of metal powder particles. It discusses the four advantages of high-temperature sintering of various ferrous PM materials: improved mechanical properties, improved physical properties, development of liquid phase, and ability to sinter active elements in alloy steels. The article also provides information on three sources of process control requirements, namely, the powder blend, green density, and sintering conditions.

Ceramic-forming processes usually start with a powder which is then compacted into a porous shape, achieving maximum particle packing density with a high degree of uniformity. This article compares and contrasts several forming processes, including mechanical consolidation, dry pressing, cold isostatic pressing, slip casting, tape casting, roll compaction, extrusion, and injection molding. It describes the advantages, equipment and tooling, and material requirements of green machining, the machining of ceramics in an unfired state with the intent of producing parts as close to as possible to their final shape. The article also provides useful information on drying methods, shrinkage, and defects as well as the removal of organic processing aids such as dispersants, binders, plasticizers, and lubricants.

This article uses metal and alloy powders as examples to briefly discuss how to perform the characterization of powders. It begins by reviewing some of the techniques involved in the sampling of powders to ensure accurate characterization. This is followed by a discussion on the important properties to characterize powders, namely the particle size, surface area, density, porosity, particle hardness, compressibility, green strength, and flowability. For characterization of powders, both individual particles and bulk powders are used to evaluate their physical and chemical properties. The article also discusses the important characteristics and compositions of powder as well as impurities that directly affect powder properties. It ends with a description of the ignition and dust-explosion characteristics of organic and metal powders.

This article discusses the advantages, limitations, and applications of material jetting of ceramics, focusing on two primary methods of droplet formation: continuous stream and drop on demand (thermal and piezoelectric) ink jetting processes.

The overall chemical composition of metals and alloys is most commonly determined by X-ray fluorescence (XRF) and optical emission spectroscopy (OES), and combustion and inert gas fusion analysis. This article provides information on the capabilities, uses, detection threshold and precision methods, and sample requirements. The amount of material that needs to be sampled, operating principles, and limitations of the stated methods are also discussed.

This article discusses the applications of high-strength aluminum powder metallurgy (P/M) alloys, detailing the advantages, properties, and the various steps involved in P/M technology, including powder production, powder processing, and degassing and consolidation. Three areas of design efforts to push the inherent advantages of aluminum alloys to new limits are also covered: high ambient-temperature strength with improved corrosion and stress corrosion cracking resistance; improved elevated-temperature properties so aluminum alloys can more effectively compete with titanium alloys; and increased stiffness and/or reduced density for aluminum alloys to compete with organic composites. An appendix provides a detailed account of the properties, processing, and applications of conventionally pressed and sintered aluminum P/M alloys.

The highly irregular morphologies of ceramic powder particles due to their process history present a challenge to binder jetting additive manufacturing (BJ-AM) ceramic powder feedstock processability, but knowledge of powder metallurgy of ceramics benefits the development and analysis of the BJ-AM ceramic processes. Understanding BJ-AM process principles and ceramics processing challenges requires reviewing a number of fundamental principles, which this article delineates. The discussion covers the processability considerations, a brief summary of some fundamental aspects of modeling of liquid permeation in the powder bed, and process capabilities and advantages of BJ-AM technology.

Alkaline cleaning is a commonly used method for removing a wide variety of soils from the surface of metals. This article focuses on the composition, operating conditions, and test and control of alkaline cleaners, as well as equipment used and their application methods. It describes the mechanisms of alkaline cleaning, such as saponification, displacement, emulsification and dispersion, and metal oxide dissolution. The article concludes with information of the safety and environmental considerations in the usage of alkaline cleaners.

Ceramic-metal composites, or cermets, combine the heat and wear resistance of ceramics with the formability of metals, filling an application niche that includes cutting tools, brake pads, heat shields, and turbine components. This article examines a wide range of cermets, including oxide cermets, carbide and carbonitride cermets, boride cermets, and other refractory types. It describes the powder metallurgy process by which cermets are produced, examining each step from powder preparation to post treatment. It discusses forming and compacting, injection molding, extrusion, rolling, pressing, slip casting, and sintering. It also discusses fundamental concepts such as chemical bonding, chemical composition, microstructure, and the development of physical and mechanical properties.