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Prasan K. Samal
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Sami M. El-Soudani
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Peter A dePoutiloff
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Daniel Eylon, F.H. (Sam) Froes
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Bryan A. Chin, Probal Banerjee, Jiayan Liu, Shaofeng Chen
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Cross-product contamination: (a) iron powder contamination of a water atomi...
Available to PurchasePublished: 30 September 2015
Fig. 6 Cross-product contamination: (a) iron powder contamination of a water atomized low-alloy steel powder; (b) low-alloy powder contamination of a water atomized iron powder
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Image
Iron powder contamination of water-atomized low-alloy steel powder. Source:...
Available to PurchasePublished: 01 January 2005
Image
Detrimental effects of iron and 410L stainless steel powder contamination o...
Available to PurchasePublished: 30 September 2015
Fig. 5 Detrimental effects of iron and 410L stainless steel powder contamination on the corrosion resistance of hydrogen-sintered 316L as a function of contamination level and sintering temperature. Reprinted with permission from Metal Powder Industries Federation, Princeton, NJ. Source: Ref
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Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006068
EISBN: 978-1-62708-175-7
... the two types of quality assurance testing measures for powder metallurgy stainless steels: tests for powder contamination and tests of chemical and physical properties. annealing chemical properties drying gas atomization lubricating physical properties powder characteristics powder...
Abstract
This article provides information on the process details that differ from general water atomization of metals as they relate to basic and engineering properties that are specific to stainless steel powders. The discussion focuses on the compacting-grade stainless steel powders. The process details include raw materials, melting method, and control of physical and chemical powder characteristics. The article describes the gas atomization of stainless steel powders and processes that are done after water atomization: drying, screening, annealing, and lubricating. It also discusses the two types of quality assurance testing measures for powder metallurgy stainless steels: tests for powder contamination and tests of chemical and physical properties.
Book Chapter
Corrosion Resistance of Powder Metallurgy Stainless Steels
Available to PurchaseBook: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006113
EISBN: 978-1-62708-175-7
..., carbon, nitrogen, iron powder contamination), then the scatter in the data will be high. The A and B hour corrosion lives are usually considered to be significant for applications that require good corrosion resistance. Even with very carefully processed samples, some scatter is seen in their A hour test...
Abstract
This article reviews various test methods used for evaluating the corrosion resistance of powder metallurgy stainless steels. These include immersion testing, salt spray testing, and electrochemical testing. The article discusses the factors that affect corrosion resistance of sintered stainless steels: compaction-related factors, sintering-related factors, and effects of alloy composition. Corrosion resistance data for sintered stainless steels is provided.
Series: ASM Handbook
Volume: 14A
Publisher: ASM International
Published: 01 January 2005
DOI: 10.31399/asm.hb.v14a.a0003988
EISBN: 978-1-62708-185-6
... 21 Iron Powder Contamination Water-atomized low-alloy steel powders are generally produced and processed in a plant that also manufactures pure iron powders. In the early days of alloy development when alloy powder production was limited, procedures were developed to minimize cross...
Abstract
Powder forging is an extension of the conventional press and sinter powder metallurgy process, which is recognized as an effective technology for producing a variety of parts to net or near-net shape. This article focuses on the material considerations, such as powder characteristics, alloy development, and inclusion assessment; and process considerations, such as process stages, tool design, and secondary operations; of ferrous alloy powder forging. The mechanical properties of powder forged materials are also reviewed. The article discusses the quality assurance tests for powder forged materials: the part dimensions and surface finish measurement, magnetic particle inspection, metallographic analysis, and nondestructive testing. It concludes with a discussion on the applications of powder forged parts with examples.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006112
EISBN: 978-1-62708-175-7
... Test Method for Nonmetallic Inclusion Level of Powder Forged Steel Parts.” Fig. 5 Three types of nonmetallic inclusion: (a) duplex sulfide, (b) spotty oxide, (c) exogenous slag Iron Powder Contamination Water-atomized low-alloy steel powders are generally produced and processed...
Abstract
Powder forging is a process in which unsintered, presintered, and sintered powder metallurgy preforms are hot formed in confined dies. This article provides information on the basic forms of powder forging and describes the material considerations, process considerations, and mechanical properties of powder forged (PF) steels. It reviews the parameters involved in quality assurance tests for PF parts. The article includes examples of PF components and highlights the reasons for selecting them over those made by competing forming methods.
Series: ASM Handbook
Volume: 5B
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v05b.a0006015
EISBN: 978-1-62708-172-6
...-film coatings, offering very smooth finishes. They also are excellent for clear coats because of their exceptional clarity and hardness. Disadvantages The GMA acrylics are highly contaminating and should not be sprayed side by side with other powder coatings. Separate powder booths and air...
Abstract
Powder coatings are widely used by manufacturers as a finish of choice to enhance the appearance and performance of their products. This article begins with a discussion on advantages and disadvantages of powder coatings. It describes the selection of coating-types and uses of powder coatings in appliance industries, furniture industries, computer industries, fixture industries, architectural industries, automotive industries, agriculture and construction equipment industries, recreational equipment industries, and general industries. Powder coating formulations consist of binder systems, pigments, extenders, and additives. The basic process flow for the manufacture of powder coatings consists of premix, extrusion, grinding, and packing. The article also provides information on application of powder coatings, including pretreatment, deposition, and curing as well as on troubleshooting, trends and challenges for the powder coatings.
Book Chapter
Properties and Selection of Powder Metallurgy Titanium and Its Alloys
Available to PurchaseBook: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006095
EISBN: 978-1-62708-175-7
... and/or moisture into the BE powder mixing environment, and furthermore the efficiency of the sintering process itself had to be improved by reducing its duration considerably, because this was identified as another contributing source of oxygen uptake. Table 8 also indicates that once oxygen contamination takes...
Abstract
This article focuses on mechanical testing characterization of blended elemental powder metallurgy (PM) titanium alloys and prealloyed PM titanium alloys. It examines the tensile properties, fracture toughness, stress-corrosion threshold resistance, fatigue strength, crack propagation properties, and processing-microstructure-property relationships of these alloys. The article also reviews five considerations for powder process selection.
Book Chapter
Secondary Operations for Powder Metallurgy Stainless Steels
Available to PurchaseBook: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006119
EISBN: 978-1-62708-175-7
... Abstract Powder metallurgy (PM) stainless steels, as with conventional PM steels, are often used in the as-sintered condition. In addition to cost considerations, minimization of postsinter handling and secondary operations is also preferred because it reduces the potential for contamination...
Abstract
Powder metallurgy (PM) stainless steels, as with conventional PM steels, are often used in the as-sintered condition. In addition to cost considerations, minimization of postsinter handling and secondary operations is also preferred because it reduces the potential for contamination of the parts with particulates and residues, which can result in the appearance of surface rust. This article provides information on various secondary operations, including tumbling, re-pressing, resin impregnation, annealing or heat treating, brazing, machining, and welding. It describes those aspects relating to welding of PM stainless steels, specifically, the effects of density, residual porosity, and sintered chemistry on weldability. Further, the article investigates the influence the sintering atmosphere has on machinability, as well as differences created by the presence of residual porosity.
Series: ASM Handbook
Volume: 5B
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v05b.a0006007
EISBN: 978-1-62708-172-6
... in powder handling are moisture pickup and removal, impact fusion, and removal of contamination and agglomerates. FBE powders quickly pick up moisture from the air ( Ref 34 ). The powder-reclaim system uses a large quantity of air, and the powder picks up moisture from the air that conveys it through...
Abstract
Functional fusion-bonded epoxy (FBE) coatings are used as external pipe coatings, base layer for three-layer pipe-coating systems, internal pipe linings, and corrosion coatings for concrete reinforcing steel (rebar). This article provides information on the chemistries of FBE, and discusses the application procedures for internal and external FBE pipe coating. The procedures involve pipe inspection, surface preparation, heating, powder application, curing, cooling, coating inspection, and repairing. It describes the problems and solutions for FBE external pipe coatings, girth weld FBE application, FBE custom coatings, internal FBE pipe linings, and FBE rebar coatings.
Image
Prior particle boundary precipitates formed on a hot isostatically pressed ...
Available to PurchasePublished: 01 January 1996
Fig. 2 Prior particle boundary precipitates formed on a hot isostatically pressed steel as the result of contamination during powder fabrication. 500×
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Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006440
EISBN: 978-1-62708-190-0
..., and similar discontinuities. It is extensively used for the inspection of wrought and cast products of both ferrous and nonferrous metals, powder metallurgy parts, ceramics, plastics, and glass objects. The liquid penetrant method does not depend on ferromagnetism (as does, for example, magnetic particle...
Abstract
Liquid penetrant inspection is a nondestructive method of revealing discontinuities that are open to the surfaces of solid and essentially nonporous materials. This article provides information on physical principles, evolution, description, and processing parameters of liquid penetrant inspection as well as materials used. It discusses some of the more generally used types of equipment used in penetrant inspection and their requirements. The article describes various penetrant methods and their selection criteria and provides information on precleaning and postcleaning of workpieces before and after penetrant inspection. The quality assurance and maintenance of penetrant inspection materials are also discussed. The article concludes with information on specifications and standards applicable to penetrant inspection.
Image
Plot of measured diffraction intensity (points) versus calculated (solid li...
Available to PurchasePublished: 01 January 1986
Fig. 7 Plot of measured diffraction intensity (points) versus calculated (solid line) for Nd 2 (Co 0.1 Fe 0.9 ) 14 B powder sample. Regions near 9°, 14°, 67°, and 78° 2θ are rejected due to presence of alpha-iron contamination. The lower curve is the difference between the observed, l obs
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Image
Corrosion resistances obtainable for various grades of stainless steel, sin...
Available to PurchasePublished: 30 September 2015
Fig. 20 Corrosion resistances obtainable for various grades of stainless steel, sintered under optimized (O) and nonoptimized (N/O) conditions. DA, dissociated ammonia. All examples are based on atmosphere-sintered parts made from contamination-free powders having sintered densities of 6.4
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Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006639
EISBN: 978-1-62708-213-6
... superficial gases and contaminations on a sample can be introduced into the analytical chamber. This necessitates that the surface be cleaned and the underlying material, the material of interest, be exposed to a clean environment so that it can be analyzed. The cleaning is accomplished by a scanning ion gun...
Abstract
This article focuses on the principles and applications of X-ray photoelectron spectroscopy (XPS) for the analysis of elemental and chemical composition. The discussion covers the nomenclature, instruments, and specimen preparation process of XPS. Some of the factors pertinent to the calibration of materials for accurate measurements using XPS are provided, along with some aspects of the accuracy in quantitative analysis by XPS. In addition, the article presents examples of how XPS data can be used to solve problems with surface interactions.
Book Chapter
Titanium Powder Metallurgy Products
Available to PurchaseSeries: ASM Handbook
Volume: 2
Publisher: ASM International
Published: 01 January 1990
DOI: 10.31399/asm.hb.v02.a0001083
EISBN: 978-1-62708-162-7
.... The powder is sintered at temperatures in the range of 1150 to 1315 °C (2100 to 2400 °F) in a vacuum to prevent gas contamination that can severely degrade compact properties. The high sintering temperature is needed to provide particle bonding and to homogenize the chemistry. It is well above the β transus...
Abstract
This article focuses on the mechanical properties, production of titanium powder metallurgy (P/M) compacts, namely, blended elemental (BE) compacts and prealloyed (PA) compacts. It explains the postcompaction treatments of titanium P/M compacts, including heat treatment, and thermochemical processing. The article talks about the applications of titanium P/M products, namely, BE and PA products. It concludes with a short note on the future trends in titanium P/M technology.
Book Chapter
Special Metallurgical Welding Considerations for Refractory Metals
Available to PurchaseSeries: ASM Handbook
Volume: 6
Publisher: ASM International
Published: 01 January 1993
DOI: 10.31399/asm.hb.v06.a0001426
EISBN: 978-1-62708-173-3
... contamination, welding in vacuum or in an inert-gas-filled chamber is recommended. A high-purity shield gas is effective in promoting ductile joints. Hot cracking and weld porosity represent other problems that can arise when welding powder metallurgy alloys. These problems often occur even when the welds...
Abstract
This article discusses special metallurgical considerations during the fusion welding of refractory metal alloys. These considerations are: microstructure, interstitial impurities, and welding conditions that are considered during the fusion welding of refractory metal alloys, including tantalum, niobium, rhenium, molybdenum, and tungsten. Refractory metal alloys are discussed in the order of decreasing weldability: tantalum, niobium, rhenium, molybdenum, and tungsten.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006074
EISBN: 978-1-62708-175-7
... to contamination by the working fluid. With reactive fine powders, such as aluminum, in large molds water leakage into the mold can produce a hazardous exothermic reaction. Not all metals and alloys of interest are readily available in the suitable particle size distribution and shape for application...
Abstract
This article describes the unique aspects of cold isostatic pressing (CIP) in comparison with die compaction, for powder metallurgy parts. It details the components of CIP equipment, including pressure vessels, pressure generators, and tooling material. The article reviews the part shapes and their influence in determining tap density of the filled mold. It provides a discussion on process parameters, such as dwell time, depressurization rate, evaluation of green strength and density, and thermal processing, and illustrates a process flowchart for the production of CIP parts.
Book: Thermal Spray Technology
Series: ASM Handbook
Volume: 5A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v05a.a0005719
EISBN: 978-1-62708-171-9
... for a given installation. After a repeatable condition has been established that reduces coating quality or powder sprayability, these conditions may be used as indicators for gas contamination levels and hardware replacement. When a computerized plasma spray system is used, gun efficiency can be set to alarm...
Abstract
This article discusses various control processes carried out in powder feeding, thermal spraying, and gas flow of the thermal spray process to standardize the coating quality. Quality of the entire powder feeding process can be achieved by controlling the processing of feeding equipment as well as the characteristics of the powder being fed. Gas flow control can be achieved by using rotameters, critical orifices, and thermal mass flowmeters, whose ability to provide useful information is defined by their resolution, accuracy, linearity, and repeatability. The commercial thermal spray controls discussed here include the open-loop input-based, open-loop output-based, closed-loop input-based, and closed-loop output-based or adaptive controls. The article discusses the common causes and practical solutions for arc starting problems. It also outlines certain important developments in measuring individual and collective particle velocities, temperature, and trajectories as well as other plume characteristics for the plasma spray process.
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