This article provides an overview of the general methods of metal powder production. It details the primary methods for particle sizing used in additive manufacturing: sieving, laser diffraction and scattering, and digital image analysis. Methods of interpreting and understanding particle size distribution (PSD) data are presented, with an emphasis on the differences between count- and volume-based PSDs. The article then outlines practices for both qualitative and quantitative assessment of particle morphology.

X-ray powder diffraction (XRPD) techniques are used to characterize samples in the form of loose powders or aggregates of finely divided material that readily diffract x-rays in specified patterns. This article provides an introduction to XRPD, beginning with a review of sensing devices, including pinhole/Laue cameras, Debye-Scherrer/Gandolfi cameras, Guinier cameras, glancing angle cameras, conventional diffractometers, thin film diffractometers, Guinier diffractometers, and micro diffractometers. The article then describes several quantitative measurement methods, such as lattice parameter, absorption diffraction, spiking, and direct comparison, explaining where each may be used. It also identifies potential sources of error in XRPD measurements.

This article provides information on the microstructure of powder metal alloys and the special handling requirements of porous materials. It covers selection, sectioning, mounting, grinding, and polishing, and describes procedures, such as washing, liquid removal, and impregnation, meant to preserve pore structures and keep them open for analysis. The article compares and contrasts the microstructures of nearly 50 powder metal alloys, using them to illustrate the effect of consolidation and compaction methods as well as particle size, composition, and shape. It discusses imaging equipment and techniques and provides data on etchants and etching procedures.

Functional fusion-bonded epoxy (FBE) coatings are used as external pipe coatings, base layer for three-layer pipe-coating systems, internal pipe linings, and corrosion coatings for concrete reinforcing steel (rebar). This article provides information on the chemistries of FBE, and discusses the application procedures for internal and external FBE pipe coating. The procedures involve pipe inspection, surface preparation, heating, powder application, curing, cooling, coating inspection, and repairing. It describes the problems and solutions for FBE external pipe coatings, girth weld FBE application, FBE custom coatings, internal FBE pipe linings, and FBE rebar coatings.

Powder coatings are widely used by manufacturers as a finish of choice to enhance the appearance and performance of their products. This article begins with a discussion on advantages and disadvantages of powder coatings. It describes the selection of coating-types and uses of powder coatings in appliance industries, furniture industries, computer industries, fixture industries, architectural industries, automotive industries, agriculture and construction equipment industries, recreational equipment industries, and general industries. Powder coating formulations consist of binder systems, pigments, extenders, and additives. The basic process flow for the manufacture of powder coatings consists of premix, extrusion, grinding, and packing. The article also provides information on application of powder coatings, including pretreatment, deposition, and curing as well as on troubleshooting, trends and challenges for the powder coatings.

The raw materials used in thermal spray processes are a critical parameter in the finished coating because the variations in their size, morphology, chemistry, and phase composition can significantly impact coating properties. Therefore, it is important to test and characterize the raw materials. This article discusses various characterization methods for powders. Topics discussed include: methods for determining particle size and/or size distribution; powder and coating stoichiometry; particle chemistry; and phase analysis by x-ray diffraction. This article discusses the characterization of thermal spray powders which involves the determination of particle size and/or size distribution and phase analysis by x-ray diffraction. It provides information on preferential volatilization and rapid solidification that influence compositional differences. Wet chemical methods, spectographic analysis, and atomic absorption spectrometry are also discussed.

Powder forging is an extension of the conventional press and sinter powder metallurgy process, which is recognized as an effective technology for producing a variety of parts to net or near-net shape. This article focuses on the material considerations, such as powder characteristics, alloy development, and inclusion assessment; and process considerations, such as process stages, tool design, and secondary operations; of ferrous alloy powder forging. The mechanical properties of powder forged materials are also reviewed. The article discusses the quality assurance tests for powder forged materials: the part dimensions and surface finish measurement, magnetic particle inspection, metallographic analysis, and nondestructive testing. It concludes with a discussion on the applications of powder forged parts with examples.

This article discusses the fracture and fatigue properties of powder metallurgy (P/M) materials depending on the microstructure. It describes the effects of porosity on the P/M processes relevant to fatigue and fracture resistance. The article details the factors determining fatigue and fracture resistance of P/M materials. It reviews the methods employed to improve fatigue and fracture resistance, including carbonitriding, surface strengthening and sealing treatments, shot-peening, case hardening, repressing and resintering, coining, sizing, and postsintering heat treatments. Safety factors for P/M materials are also detailed.

Powder metallurgy is a near-net shape process capable of producing complex parts with little or no need for secondary operations such as machining, joining, or assembly. However, the inability to produce certain geometrical figures such as transverse holes, undercuts, and threads frequently necessitates some machining, particularly drilling. This article provides a discussion on the measures that can optimize the machining of P/M materials. It reviews the factors influencing machinability of P/M components, including workpiece and tool material properties, cutting conditions, machine and cutting tool parameters as well as some P/M material and production process parameters. These parameters discussed include the particle size, part geometry, porosity, compaction and sintering methods. In addition, the article presents guidelines for the various machining processes, namely, turning and boring, milling, drilling, grinding, reaming, burnishing, tapping, and honing and lapping.

Certain metal products can be produced only by powder metallurgy; among these products are materials whose porosity is controlled. Successful production by powder metallurgy depends on the proper selection and control of process variables: powder characteristics; powder preparation; type of compacting press; design of compacting tools and dies; type of sintering furnace; composition of the sintering atmosphere; choice of production cycle, including sintering time and temperature; and secondary operations and heat treatment. When the application of a powder metallurgy part requires high levels of strength, toughness, or hardness, the mechanical properties can be improved or modified by infiltration, heat treatment, or a secondary mechanical forming operation such as cold re-pressing or powder forging. The article also discusses the effect of the secondary processes on P/M mechanical properties.

This article focuses on the mechanical properties, production of titanium powder metallurgy (P/M) compacts, namely, blended elemental (BE) compacts and prealloyed (PA) compacts. It explains the postcompaction treatments of titanium P/M compacts, including heat treatment, and thermochemical processing. The article talks about the applications of titanium P/M products, namely, BE and PA products. It concludes with a short note on the future trends in titanium P/M technology.

This article briefly reviews the subject of copper-base powder-metallurgy (P/M) products in terms of powder production methods (atomization, oxide reduction, electrolysis, and hydrometallurgy) and the product properties/consolidation practices of the major applications. Of the four major methods for making copper and copper alloy powders, atomization and oxide reduction are presently practiced on a large scale in North America. The article provides information on the mechanism, production, properties, composition and applications of different types of copper-base P/M products, including self-lubricating sintered bearings, structural parts, oxide-dispersion-strengthened copper, sintered metal friction materials, and porous filters.

This article discusses the applications of high-strength aluminum powder metallurgy (P/M) alloys, detailing the advantages, properties, and the various steps involved in P/M technology, including powder production, powder processing, and degassing and consolidation. Three areas of design efforts to push the inherent advantages of aluminum alloys to new limits are also covered: high ambient-temperature strength with improved corrosion and stress corrosion cracking resistance; improved elevated-temperature properties so aluminum alloys can more effectively compete with titanium alloys; and increased stiffness and/or reduced density for aluminum alloys to compete with organic composites. An appendix provides a detailed account of the properties, processing, and applications of conventionally pressed and sintered aluminum P/M alloys.

Powder metallurgy (PM) processes include press and sinter hardening, metal injection molding, powder forging, hot isostatic pressing, powder rolling, and spray forming. This article provides an overview of PM processing methods and general considerations of heat treatment of PM parts that are case-hardened to obtain higher hardness, wear, fatigue, and impact properties. It describes the effects of porosity on heat treatment, alloy content on PM hardenability, and starting material on homogenization of PM steels. The article describes the properties, following heat treatment, of low-alloy steels tempered at 175 ºC for one hour, and lists recommended quench and temper parameters to achieve good wear resistance and core strength based on different ranges of porosity.

This article focuses on various heat-treating practices, namely, normalizing, annealing, stress relieving, preheating, austenitizing, quenching, tempering, and nitriding for cold-work tool steels. The cold-work tool steels include medium-alloy air-hardening tool steels, high-carbon high-chromium tool steels, and high-vanadium-powder metallurgy tool steels. The article also describes the properties, types, nominal compositions and designations of these cold-work tool steels.

Powder metallurgy (PM) has been called a lost art. Long before furnaces were developed that could approach the melting point of metal, PM principles were used. This article provides an overview of the major historical developments of various methods of platinum powder production. The development of production methods took place in various phases starting from prehistoric time, post-war period, to recent and commercial period. The article discusses the powder metallurgy of platinum, as well as the commercial and post-war developments of PM. Literature and trade associations are also discussed.

The technology to fabricate lower-density, porous powdered metal materials provides unique engineering solutions for many applications. This article summarizes the characteristics and applications of porous powder metallurgy technology, as well as the fabrication methods employed.

This article describes the physical properties of powder metallurgy (PM) stainless steels. These include thermal diffusivity, conductivity, thermal expansion coefficient, Poisson's ratio, and elastic modulus. The article contains a table that lists the characteristics of various grades of PM stainless steels. It discusses the applications of various PM stainless steels such as rearview mirror brackets, anti-lock brake system sensor rings, and automotive exhaust flanges and sensor bosses.

The organizations that are most active in the development of standards for powder metallurgy (PM) are the American Society for Testing and Materials (ASTM), Metal Powder Industries Federation (MPIF), and International Standards Organization (ISO). This article presents the test method standards, materials standards, and material designation codes for PM materials. It provides information on the codes for structural parts, PM soft magnetic materials, PM self-lubricating bearings, metal injection molded materials, and powder forged materials.