This article reviews photographic principles, namely, visual examination, field photographic documentation, and laboratory photographic documentation, as applied to failure analysis and the specific techniques employed in both the field and laboratory. It provides information on the photographic equipment used in failure analysis and on film and digital photography. The article describes the basics of photography and the uses of different types of lighting in photography of a fractured surface. The article also addresses the techniques involved in macrophotography and microscopic photography as well as other special techniques.

This article discusses the preparation of photomacrographs of fracture surfaces. It provides useful information on the equipment used, such as view cameras, 35-mm single-lens-reflex cameras, and stereomicroscopes. The article describes the role of lenses, focusing, camera magnification, and selection of lens aperture in a microscopic system. It illustrates the lighting techniques employed in photography and highlights the use of different films. The article concludes with a list of auxiliary equipment used in fracture surface photography.

Failure analysis is generally defined as the investigation and analysis of parts or structures that have failed or appeared to have failed to perform their intended duty. Methods of field inspection and initial examination are also critical factors for both reconstruction analysts and materials failure analysts. This article focuses on the general methods and approaches from the perspective of a reconstruction analyst. It describes the elements of accident reconstruction, which have conceptual similarity with the principles for failure analysis of material incidents that are less complex than a large-scale accident. The approach presented is that the analysis and reconstruction is based on the physical evidence. The article provides a brief review of some general concepts on the use and limitations of advanced data acquisition tools and computer modeling. Legal implications of destructive testing are discussed in detail.

This article discusses the standard conduct of coating failure investigation. As each failure is different, a specific coating failure may require increased emphasis on a given step, or additional work and/or steps may be required. This article covers the following topics: obtaining and analyzing background information, preliminary determination of site conditions, inspection equipment requirements, coating failure site investigation, sampling techniques, sample chain of custody, coordination with the coatings laboratory, report preparation, and sample retention.

This article focuses on the general methods and approaches from the perspective of a reconstruction analyst and includes discussions relevant to materials failure analysts at the incident scene. The elements of accident reconstruction are described. These have conceptual similarity with the principles for failure analysis of material incidents that are less complex than a large-scale accident. The article provides a brief review of some general concepts on the use of modeling which can be a very powerful tool for information pertaining to the reconstruction of an accident where the model can be a physical, mathematical, or logical representation of a physical system or process.

This article describes the preliminary stages and general procedures, techniques, and precautions employed in the investigation and analysis of metallurgical failures that occur in service. The most common causes of failure characteristics are described for fracture, corrosion, and wear failures. The article provides information on the synthesis and interpretation of results from the investigation. Finally, it presents key guidelines for conducting a failure analysis.

Holography is basically a two-step process for creating a whole three dimensional image of a diffusely reflecting object having some arbitrary shape. This article discusses the advantages, disadvantages and applications of using the optical holography method in nondestructive evaluation. It also discusses the types of acoustical holography, including liquid-surface acoustical holography and scanning acoustical holography. The article concludes by comparing liquid-surface and scanning systems.

This article discusses the organization required at the outset of a failure investigation and provides a methodology with some organizational tools. It focuses on the use of problem-solving tools such as a fault tree analysis combined with critical thinking. The discussion covers nine steps to organize a good failure investigation. They are as follows: understand and negotiate goals of the investigation, obtain a clear understanding of the failure, identify all possible root causes, objectively evaluate the likelihood of each root cause, converge on the most likely root cause(s), objectively and clearly identify all possible corrective actions, objectively evaluate each corrective action, select optimal corrective action(s), and evaluate effectiveness of selected corrective action(s). Common problems detrimental to a failure investigation are also covered.

Photochemical machining (PCM), also known as chemical blanking, is a metal-etching process that uses a photoresist to define the locations where the metal will be etched. This article describes the major steps used in the PCM process, namely, the preparation of the phototool, selection of the metal, preparation of the workpiece, masking with photoresists, etching, and stripping and inspection. The article reviews various design considerations for the PCM process. These include dimensional limitations, tolerances, and edge quality. The article also discusses the advantages, disadvantages, and applications of the PCM process.

Selection of the process steps used, powder chosen, and lubricant choice have marked effects on the quality of a sintered component. This article describes the alloy composition, mechanical and structural properties, processing routes, and advantages of the common members of the copper alloy family, namely, pure copper, brass, and bronze, which all aid in the selection of the suitable material for structural and bearing applications. It outlines the structural applications of nickel silver alloys.

Rough grinding and polishing of specimens are required to prepare fiber-reinforced composite samples for optical analysis. This article discusses the consumables, process variables, and the equipment that influence the sample preparation procedure. It describes the hand and automated grinding methods. The article summarizes the rough and final polishing steps for both hand and automated techniques. Common artifacts that may be created during grinding and polishing steps of composite samples are reviewed. These include scratches, fiber pull-out, matrix smears, streaks, erosion of different phases, and fiber and sample edge rounding and relief.

The overall chemical composition of metals and alloys is most commonly determined by X-ray fluorescence (XRF) and optical emission spectroscopy (OES), and combustion and inert gas fusion analysis. This article provides information on the capabilities, uses, detection threshold and precision methods, and sample requirements. The amount of material that needs to be sampled, operating principles, and limitations of the stated methods are also discussed.

Ultrasonic inspection is a nondestructive method in which beams of high-frequency acoustic energy are introduced into a material to detect surface and subsurface flaws, to measure the thickness of the material, and to measure the distance to a flaw. This article provides a detailed account of ultrasonic flaw detectors, including ultrasonic transducers and types of search units and couplants. The article describes pulse-echo and transmission inspection methods and data interpretation. The general characteristics of ultrasonic waves and the factors influencing ultrasonic inspection are also addressed. The article concludes with a review of the advantages and disadvantages of ultrasonic inspection compared with other methods applications of the technique.

Failure analysis is an investigative process that uses visual observations of features present on a failed component fracture surface combined with component and environmental conditions to determine the root cause of a failure. The primary means of recording the conditions and features observed during a failure analysis investigation is photography. Failure analysis photographic imaging is a combination of both science and art; experience and proper imaging techniques are required to produce an accurate and meaningful fracture surface photograph. This article reviews photographic principles and techniques as applied to failure analysis, both in the field and in the laboratory. The discussion covers the processes involved in field and laboratory photographic documentations, provides a description of professional digital cameras, and gives information on photographic lighting and microscopic photography. Special techniques can be employed to deal with highly reflective conditions and are also described in this article.

Radiography is a nondestructive-inspection method that is based on the differential absorption of penetrating radiation by the part or test piece (object) being inspected. This article discusses the fundamentals and general applications of radiography, and describes the sources of radiation in radiographic inspection, including X-rays and gamma rays. It deals with the characteristics that differentiate neutron radiography from X-ray or gamma-ray radiography. The geometric principles of shadow formation, image conversion, variation of attenuation with test-piece thickness, and many other factors that govern the exposure and processing of a neutron radiograph are similar to those for radiography using X-rays or gamma rays.

This article reviews the most common reasons for failures and the purpose of a failure investigation. It discusses the nine steps for the organization of a good failure investigation. The three basic tools that are helpful in any failure investigation, namely, a fault tree, a failure mode assessment chart, and a technical plan for resolution chart, are reviewed. The article briefly describes failure investigation pitfalls and concludes with information on the other common tools used for failure investigation and root cause determination.

This article provides information on the basic components of a light microscope, including the illumination system, collector lens, and optical and mechanical components. It describes optical performance in terms of image aberrations, resolution, and depth of field. The article discusses the examination of specimen surfaces using polarized light, phase contrast, oblique illumination, dark-field illumination, bright-field illumination, interference-contrast illumination, and phase contrast illumination. Special techniques and devices that may be used with the optical microscope, to obtain additional information, are also described. The article concludes with information on photomicroscopy and macrophotography.

This article reviews the steps involved in presurface-preparation inspection: substrate replacement; removal of weld spatter, rounding of sharp edges, and grinding of slivers/laminations; and removal of rust scale, grease, oil, and chemical (soluble salt) contamination. It focuses on surface preparation methods that range from simple solvent cleaning to hand and power tool cleaning, dry and wet abrasive blast cleaning, centrifugal wheel blast cleaning, chemical stripping, and waterjetting for the application of the coating system. In addition, the article provides a description of the Society for Protective Coatings' (SSPC) standards and NACE International standards as well as the International Organization for Standardization (ISO) standards and International Concrete Repair Institute (ICRI) guidelines for surface cleanliness.

Fractography is the systematic study of fractures and fracture surfaces. It is a useful tool in failure analysis and provides a means for correlating the influence of microstructure on the fracture mode of a given material. This article discusses the preservation, preparation, and photography of fractured parts and surfaces, and describes some of the more common fractographic features revealed by light microscopy, including tensile-fracture surface marks in unnotched specimens, fatigue marks, and structural discontinuities within the metal. The article also explains how to interpret fracture information contained in optical and scanning-electron microscope fractographs.

Metal spinning is a term used to describe the forming of metal into seamless, axisymmetric shapes by a combination of rotational motion and force. This article describes two forming techniques, such as manual spinning and power spinning, for forming seamless metal components. The process technology, equipment, and tooling for both manual spinning and power spinning are also discussed.