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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003754
EISBN: 978-1-62708-177-1
... discusses the examination of specimen surfaces using polarized light, phase contrast, oblique illumination, dark-field illumination, bright-field illumination, interference-contrast illumination, and phase contrast illumination. Special techniques and devices that may be used with the optical microscope...
Abstract
This article provides information on the basic components of a light microscope, including the illumination system, collector lens, and optical and mechanical components. It describes optical performance in terms of image aberrations, resolution, and depth of field. The article discusses the examination of specimen surfaces using polarized light, phase contrast, oblique illumination, dark-field illumination, bright-field illumination, interference-contrast illumination, and phase contrast illumination. Special techniques and devices that may be used with the optical microscope, to obtain additional information, are also described. The article concludes with information on photomicroscopy and macrophotography.
Image
Published: 01 January 1987
in a mixture of perchloric acid, ethanol, butyl cellusolve, and water and observed under phase-contrast illumination. SEM, 200× (R.E. Ricker, University of Notre Dame, and D.J. Duquette, Rensselaer Polytechnic Institute)
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009075
EISBN: 978-1-62708-177-1
...-field illumination, dark-field illumination, polarized-light microscopy, interference and contrast microscopy, and fluorescence microscopy. The article also provides a discussion of sample preparation materials such as dyes, etchants, and stains for the analysis of composite materials using optical...
Abstract
The analysis of composite materials using optical microscopy is a process that can be made easy and efficient with only a few contrast methods and preparation techniques. This article is intended to provide information that will help an investigator select the appropriate microscopy technique for the specific analysis objectives with a given composite material. The article opens with a discussion of macrophotography and microscope alignment, and then goes on to describe various illumination techniques that are useful for specific analysis requirements. These techniques include bright-field illumination, dark-field illumination, polarized-light microscopy, interference and contrast microscopy, and fluorescence microscopy. The article also provides a discussion of sample preparation materials such as dyes, etchants, and stains for the analysis of composite materials using optical microscopy.
Image
Published: 01 December 2004
Fig. 25 Lighting effects to enhance contrast between phase constituents in an unetched specimen of Al-Si-Cu-Ni alloy. (a) Bright-field illumination with silicon (A, dark gray), α-Al(FeMn)Si (B, light gray), and Al 2 Cu (C, beige). (b) Dark-field illumination with phase boundaries revealed. (c
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Image
Published: 01 December 2004
Fig. 26 Lighting effects to reveal contrast of crystal orientation in an etched aluminum-copper specimen. (a) Bright-field illumination with α-Al (light gray) and Al 2 Cu (gray). (b) Dark-field illumination with phase boundaries revealed. (c) Cross-pole mode of observation revealing Al 2 Cu
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003782
EISBN: 978-1-62708-177-1
... of the specimen may require two to three charges of the acid/abrasive solution. This final-polishing step can last from 3 to 5 min. When polishing is complete, a slight indication of second-phase structure would be visible using bright field illumination. Polarized light also works well for checking the progress...
Abstract
Zirconium, hafnium, and their alloys are reactive metals used in a variety of nuclear and chemical processing applications. This article describes various specimen preparation procedures for these materials, including sectioning, mounting, grinding, polishing, and etching. It reviews some examples of the microstructure and examination for zircaloy alloys, hafnium, zirconium, and bimetallic forms.
Image
Published: 01 December 2004
Fig. 2 Composite materials made from different types of fibers. (a) Woven glass fiber fabric composite revealing a multiphase-matrix morphology. Ultrathin section, transmitted-light phase contrast, 20× objective. (b) Kevlar (E.I. du Pont de Nemours and Company) fabric composite cross section
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Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001237
EISBN: 978-1-62708-170-2
... and the porosity of the sample can be examined. In DIC illumination, the different phases of silicon and silicon carbide become very apparent. Fig. 3 (a) Bright-field image of SiSiC. 200×. (b) Dark-field image of SiSiC. 200×. (c) Differential interference contrast illumination image of SiSiC. 200...
Abstract
Quantitative image analysis has expanded the capabilities of surface analysis significantly with the use of computer technology. This article provides an overview of the quantitative image analysis and optical microscopy. It describes the various steps involved in surface preparation of samples prone to abrasion damage and artifacts for quantitative image analysis.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009071
EISBN: 978-1-62708-177-1
..., 5× objective, montage Fig. 2 Composite materials made from different types of fibers. (a) Woven glass fiber fabric composite revealing a multiphase-matrix morphology. Ultrathin section, transmitted-light phase contrast, 20× objective. (b) Kevlar (E.I. du Pont de Nemours and Company) fabric...
Abstract
This article illustrates the polymer matrices used for composite materials. It describes the use of prepeg materials in manufacturing high-performance composites. The article discusses the various infusion processes for the development of fiber-reinforced composites, namely, resin transfer molding, vacuum-assisted resin transfer molding, and resin film infusion. It explains the composite- and matrix-toughening methods for fiber-reinforced composites, such as dispersed-phase toughening and interlayer toughening. The article concludes with information on optical microscopy, which provides an insight into the micro- and macrostructure of fiber-reinforced composites.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.9781627081771
EISBN: 978-1-62708-177-1
Image
Published: 01 December 2004
Fig. 9 Higher-magnification views of the composite cross section shown in Fig. 8 . (a) Reflected light, phase contrast, 25× objective. (b) Bright-field illumination, 50× objective
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Image
Published: 01 January 2000
Fig. 21 Knoop indents in ferrite (dark) and austenite (white) grains in a dual-phase stainless steel (differential interference contrast illumination, aqueous 20% nitric acid, 3 V dc). 500×
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Image
Published: 01 December 2004
Fig. 47 Zircaloy 4 as-cast ingot. Use of attack polishing, heat tinting (425 °C, or 800 °F), and differential interference contrast illumination reveals the basic crystal structure and the iron-chromium second phase. 200×. (P.E. Danielson)
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Image
Published: 01 December 2004
Fig. 51 Heat-tinted niobium alloy (C103) plate as viewed under differential interference contrast illumination. Some of the grains exhibit a second phase (note small, particle-like features) due to alloying additions. 65×. (P.E. Danielson)
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Image
Published: 15 January 2021
Fig. 27 Comparison of (a) bright-field, (b) differential interference contrast, and (c) dark-field illumination for viewing a partially fractured (by impact) specimen of AISI type 312 weld metal containing substantial sigma phase. Original magnification: all 240×
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Book Chapter
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003800
EISBN: 978-1-62708-177-1
..., the illumination of an altered from the original composition, (b) that of propagation. The amount of energy trans- object so that it appears on a bright back- appears dark when etched, or (c) that has a mitted along an optical path through a crystal ground. higher hardness value than the core. Contrast...
Abstract
This article is a compilation of definitions of terms related to metallography and microstructures.
Image
Published: 01 January 2000
Fig. 24 Vickers indents (50 gf) in the matrix (dark) and in the intergranular beta (white) phase in as-cast beryllium copper (C 82500) that was burnt in solution annealing (differential interference contrast illumination, aqueous 3% ammonium persulfate and 1% ammonium hydroxide). 500×
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Image
Published: 01 January 2000
Fig. 25 Vickers indents (100 gf) in the matrix (dark) and in the intergranular beta (white) phase in an age-hardened as-cast beryllium copper (C 82500) that was burnt in solution annealing (differential interference contrast illumination, aqueous 3% ammonium persulfate and 1% ammonium
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Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003464
EISBN: 978-1-62708-195-5
... remain hidden when using standard bulk metallographic preparation techniques and reflected illumination. Because most polymeric materials are inert to metallographic etchants, they can be best observed with transmitted polarized light and various contrast media to enhance the differences in refractive...
Abstract
Microscopy is a valuable tool in materials investigations related to problem solving, failure analysis, advanced materials development, and quality control. This article describes the sample preparation techniques of composite materials. These techniques include mounting, rough grinding, and polishing. The preparation techniques of ultrathin sections are also summarized. The article explains the illumination methods used by reflected light microscopy to view a specimen. These consist of epi-bright-field illumination, epi-dark-field illumination, epi-polarized light, and epi-fluorescence. The article also provides information on transmitted light microscopy.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006684
EISBN: 978-1-62708-213-6
... if they have a much different hardness and polishing rate than the surrounding metal. They will either stand above or below the matrix phase and can be easily observed, particularly if differential interference contrast illumination (DIC) is used. However, bright-field illumination is the starting point...
Abstract
The reflected light microscope is the most commonly used tool to study the microstructure of metals, composites, ceramics, minerals, and polymers. For the study of the microstructure of metals and alloys, light microscopy is employed in the reflected-light mode using either bright-field illumination, dark-field illumination, polarized light illumination, or differential interference contract, generally by the Nomarski technique. This article concentrates on how to reveal microstructure properly to enable the proper identification of the phases and constituents and, if needed, measuring the amount, size, and spacing of constituents, using the light optical microscope. The discussion covers the examination of microstructures using different illumination methods and includes a comparison between light optical images and scanning electron microscopy images of microstructure.
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