Autoclave molding is a process used to impart a controlled heat and pressure cycle cure to a layup. This article describes the materials used for preparing a layup, including peel ply, separator, bleeder, barrier, breather, dam, and vacuum bag. It describes the major elements and functions of an autoclave system, including pressure vessel, gas stream heating and circulation sources, gas stream pressurizing systems, vacuum systems, control systems, and loading systems. The article includes information about modified autoclaves for specialized applications and safety practices in autoclave molding. It also describes the tooling configuration and type of tooling which includes aluminum and steel tooling, electroformed nickel tooling, graphite-epoxy tooling, and elastomeric tooling.

Thermomechanical are used to gain insight into the causes of problems that arise during a given thermomechanical process. This article provides examples to demonstrate how significant the parameters were selected for specific tests. It examines the types of problems that can occur during a thermomechanical process. The article provides information on the thermophysical properties, which include specific heat, coefficient of thermal expansion, thermal conductivity/diffusivity, and density. It concludes with examples that illustrate how the various considerations in testing are successfully used to solve practical thermomechanical processing problems.

A cylindrical specimen compressed with friction at the die surfaces does not remain cylindrical in shape but becomes bulged or barreled. Tensile stresses associated with the bulging surface make the upset test a candidate for workability testing. This article discusses test-specimen geometry and friction conditions; strain measurements; crack detection; and material inhomogeneities, which are to be considered for performing cold upset testing. It describes test characteristics in terms of deformation, free-surface strains, and stress states for performing cylindrical compression tests. The article illustrates the fracture loci in cylindrical, tapered, and flanged upset-test specimens of aluminum alloy and type 1045 cold-finished steel.

Optical testing of plastics includes characterization of materials and analysis of optical components. This article focuses on procedures for testing various characteristics of optical components, including transmission and haze, yellowness, refractive index, birefringence, as well as surface irregularity, contamination, gloss, and color. It provides a short note on ad hoc testing, which is beneficial for practical applications in which lenses, prisms, and light pipes are being used and tested, as other test instruments are often not available.

Independent verification of coating system performance can be based on laboratory testing and/or field exposure. Qualification testing is a critical component to coating system selection. This article focuses on performance evaluations that are used to prequalify coating systems, namely, facility-specific, industry-specific, coating-type-specific, or a combination of these. It describes the standard laboratory tests used to generate performance data, namely, physical, compositional, chemical exposure, and application characteristics tests. The pros and cons of using manufacturer-generated data versus independently generated data are discussed. The article provides information on accelerated corrosion/weathering testing and nuclear level 1/level 2 service coatings qualification. It also describes the procedures for establishing minimum performance requirements and for determining when requalification testing may be required.

This article introduces the principal methodologies and some advanced technologies that are being applied for nondestructive evaluation (NDE) of fiber-reinforced polymer-matrix composites. These include acoustic emission, ultrasonic, eddy-current, computed tomography, electromagnetic acoustic transducer, radiography, thermography, and low-frequency vibration methods. The article also provides information on NDE methods commonly used for metal-matrix composites.

Elastomers belong to a group of materials known as polymers that acquire their properties and strength from their molecular weight, chain entanglements, and crystalline regions. This article focuses on the use of elastomers as seals and describes its performance capabilities from the point of a sealant. The important technical concepts that define the performance capabilities of the elastomeric part include polymer architecture (molecular building blocks), compounding (the ingredients within the polymer), and vulcanization of the elastomer shape. The article discusses the aggressiveness of the chemical environment, temperature, and minor constituents in the environment and in the material itself that affect the chemical resistance of the elastomer. It provides a discussion on performance evaluation methods, namely, immersion testing and application specific testing that are determined using ISO and ASTM standards. The article concludes with information on elastomer failure modes and failure analysis.

Relatively limited effort has gone into developing repair processes and materials for composites, in contrast to the significant labor and expense that has gone into the development of these materials for numerous critical applications. As composites gain wider acceptance as aerospace materials, there is a need to understand the requirements of the end users regarding repair of these advanced materials. This article focuses on the repair of graphite-epoxy structures designed in a variety of forms for a wide range of load intensities. Five repair concepts developed for generic laminate repair have been validated in this article through the required environmental and load condition tests. These include bonded-scarf joint flush repair, double-scarf joint flush repair, blind-side banded-scarf repair, blind-side sandwich repair, and bonded external patch repair. A brief note on thermoplastic repair concepts is also provided in this article.

This article discusses the concepts of quality control (QC) and quality assurance (QA), and clarifies the differences and similarities in the roles and responsibilities of QC and QA personnel. It describes the inspection procedures used to verify proper surface preparation and installation of the protective coating/lining system. Prior to beginning surface-preparation operations, many specifications will require a presurface-preparation inspection to verify the correction of fabrication defects and removal of surface contamination such as grease, oil, cutting compounds, lubricants, and chemical contaminants. When inspecting concrete prior to coating installation, three areas of concern exist: surface roughness, moisture content in concrete, and acidity/alkalinity of the surface. The article provides information on the industry standards for assessing surface cleanliness. It details postcoating application quality requirements, including measuring of dry-film thickness, assessing intercoat cleanliness, verifying minimum and maximum recoat intervals, performing holiday/pinhole detection, conducting cure/hardness testing, and assessing adhesion of the applied coating system.

The process of coating plastics with metals for functional purposes is called metallizing of plastics. This article discusses the metallizing of plastics, provides information on its history, and gives a short note on applications and adhesion properties of metallic coatings. It also discusses the selection of plastics for plating. This article also describes metallizing techniques, including plating (electrolytic or electroplating), vacuum metallizing and thermal spraying, and environmental considerations. The article discusses the quality assurance procedures for metallized plastic parts which include tests that assess the quality of the finish, coating thickness, adhesion, and corrosion resistance, and gives a short note on service performance, which includes service condition classifications.

Honeycomb is a product consisting of very thin sheets attached to form connecting cells. This article briefly explains the construction, core characteristics, properties, and testing methods of the honeycomb structures. It discusses the special processes used to custom fit the shape of core to fit customer’s specific needs. The article provides information on sandwich structures, including material selection, design guidelines, and structural efficiency.

Workability is the ability of the workpiece metal to undergo extrusion or drawing without fracture or defect development. This article describes the limits of workability in extrusion and drawing in terms of fracture and flaw development and presents some comments on fracture mechanisms. It discusses the empirical projections of absolute workability from various mechanical tests. The article concludes with a discussion on extrusion and drawing process design implications.

This article examines the deformation processes in metal-forming operations and considers the effects introduced by scale factors when microforming. It discusses the process parameters and variables affecting surface interactions, including temperature, speed, reduction, stiffness, and dynamic response of equipment. The article reviews the determination of friction coefficient using laboratory monitoring methods, indirect measurements, and the inverse method. It considers the determination of the interface heat-transfer coefficient by using the ring test and computer simulations. The article describes the behavior of oxide scale on the surface of hot metal undergoing thermomechanical processing. It concludes with information on the effects of process and material parameters on interfacial phenomena.

This article discusses the classification of the attachment and joining methods in plastics, including mechanical fastening, adhesive bonding, solvent bonding, and welding. It describes the mechanical fastening techniques used to join both similar and dissimilar materials with machine screws or bolts, nuts and washers, molded-in threads, self-threading screws, rivets, spring-steel fasteners, press fits, and snap fits. The article explains solvent bonding used for thermoplastic parts, and tabulates the solvent types used with various plastics. It also describes the surface preparation of plastics, chemical treatment for adhesion, and tabulates the adhesive types for bonding plastics to plastics and plastics to nonplastics. The article briefly describes the welding processes of thermoplastics, including fusion welding (hot-tool, hot gas, extrusion, and focused infrared), friction welding (vibration, spin, and ultrasonic), and electromagnetic welding (resistance, induction, dielectric, and microwave). It concludes with the evaluation of welds using destructive and nondestructive testing.

This article describes the methods and equipments involved in the preparation of specimens for examination by light optical microscopy, scanning electron microscopy, electron microprobe analysis for microindentation hardness testing, and for quantification of microstructural parameters, either manually or by the use of image analyzers. Preparation of metallographic specimens generally requires five major operations: sectioning, mounting, grinding, chemical polishing, and etching. The article provides information on the principles of technique selection in mechanical polishing, and describes the procedures, advantages, and disadvantages of electrolytic and chemical polishing. It also provides a detailed account of procedures, precautions, and composition for preparation and handling of etchants.

This article presents examples of the visual fracture examination that illustrate the procedure as it applies to failure analysis and quality determination. It describes the techniques and procedures for the visual and light microscopic examination of fracture surfaces with illustrations. The article also describes microscopic and macroscopic features of the different fracture mechanisms with illustrations with emphasis on visual and light microscopy examination. The types of fractures considered include ductile fractures, tensile-test fractures, brittle fractures, fatigue fractures, and high-temperature fractures.

This article identifies the coatings applied to many substrates for both beautification and protection, and the inherent conflicts that exist between the coatings and the buildings they are designed to protect; emphasis is placed on masonry walls. It provides information on the purposes of the coatings in the commercial buildings. The article briefly describes some of the most common types of substrates found in buildings and the coatings commonly associated with each substrate. The selection of the coating system depends on the substrate and service expectations. The article addresses the primary causes of masonry coating problems and also provides a detailed discussion on the wall design considerations, moisture considerations, and coating system challenges in the masonry buildings.

Visual examination, using the unaided eye or a low-power optical magnifier, is typically one of the first steps in a failure investigation. This article presents the guidelines for selecting samples for scanning electron microscope examination and optical metallography and for cleaning fracture surfaces. It discusses damage characterization of metals, covering various factors that influence the damage, namely stress, aggressive environment, temperature, and discontinuities.

The structural efficiency of a composite structure is established by its joints and assembly. Adhesive bonding, mechanical fastening, and fusion bonding are three types of joining methods for polymer-matrix composites. This article provides information on surface treatment and the applications of adhesive bonding. It discusses the types of adhesives, namely, epoxy adhesives, epoxy-phenolic adhesives, condensation-reaction PI adhesives, addition-reaction PI adhesives, bismaleimide adhesives, and structural adhesives. The article provides information on fastener selection considerations, including corrosion compatibility, fastener materials and strength, head configurations, importance of clamp-up, interference fit fasteners, lightning strike protection, blind fastening, and sensitivity to hole quality. Types of fusion bonding are presented, namely, thermal welding, friction welding, electromagnetic welding, and polymer-coated material welding.