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particle interlayer toughening
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Published: 01 December 2004
Fig. 12 Fracture morphology in a particle interlayer-toughened thermoset-matrix composite. (a) Strain birefringence in the interlayer particles. Transmitted polarized light, 20× objective. (b) Some of the particles are found to bridge the formed cracks, and some particles are torn. Transmitted
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009081
EISBN: 978-1-62708-177-1
... microscopy particle interlayer-toughened composite failures rubber-toughened thermoset-matrix composite failures thermoplastic-matrix composite failures toughened thermoset-matrix composite failures tough-matrix composite failures untoughened thermoset-matrix composite failures X-radiography methods...
Abstract
This article describes methods for analyzing impact-damaged composites in the aircraft industry. These include C-scan and x-radiography methods and optical microscopy. The article reviews brittle-matrix composite and tough-matrix composite failures. It explains the different types of composite failure mechanisms such as thermoplastic-matrix composite failure mechanisms, untoughened thermoset-matrix composite failure mechanisms, toughened thermoset-matrix composite failure mechanisms, dispersed-phase and rubber-toughened thermoset-matrix composite failure mechanisms, and particle interlayer-toughened composite failure mechanisms.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009080
EISBN: 978-1-62708-177-1
... impregnation material quality microstructure morphology particle interlayer toughening prepregs reflected-light optical microscopy single-pass impregnation thermoplastic materials thermoset-matrix composites THE PERFORMANCE of fiber-reinforced composite systems has evolved in response to new...
Abstract
This article describes the dispersed-phase toughening of thermoset matrices by the development of multiphase-structure thermosetting matrices using rubber and/or thermoplastic materials. It discusses two main methods for manufacturing prepregs, namely, single-pass impregnation and double-pass impregnation. The article illustrates reflected-light optical microscopy techniques to evaluate the morphology of thermoplastic materials for determining the material quality and correlating key microstructural features with material performance.
Image
Published: 01 December 2004
Fig. 12 Ultrathin section of a particle-modified interlayer-toughened composite material. Transmitted-light Hoffman modulation contrast, 20× objective
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009071
EISBN: 978-1-62708-177-1
... that the particles remain in the composite interlayer and do not penetrate the fiber tows ( Ref 20 ). The most common method of interlayer toughening is through adding preformed particle-modified resin on the surface of the prepreg, which, when consolidated and cured, results in an interlayer-toughened composite...
Abstract
This article illustrates the polymer matrices used for composite materials. It describes the use of prepeg materials in manufacturing high-performance composites. The article discusses the various infusion processes for the development of fiber-reinforced composites, namely, resin transfer molding, vacuum-assisted resin transfer molding, and resin film infusion. It explains the composite- and matrix-toughening methods for fiber-reinforced composites, such as dispersed-phase toughening and interlayer toughening. The article concludes with information on optical microscopy, which provides an insight into the micro- and macrostructure of fiber-reinforced composites.
Image
Published: 01 December 2004
region (i.e., light-gray circles). Slightly uncrossed polarized light, 50× objective. (b) Ultrathin section developed from a particle-modified toughened interlayer composite that was sectioned through the thickness. Transmitted light, Hoffman modulation contrast, 40× objective. (c) Ultrathin section
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Image
in Viewing Composite Specimens Using Reflected Light Microscopy[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 9 Cross sections of an interlayer-toughened composite material. (a) Bright-field illumination, 25× objective. (b) Same view but after the addition of a solvent-based laser dye (Magnaflux Zyglo, Magnaflux Corp.) to the sample surface. The laser dye is preferentially absorbed
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009079
EISBN: 978-1-62708-177-1
... the cracked area, it can be seen that many of the carbon fibers were separated from the matrix as a result of the crack propagation. In this material, the microcracks were found to not propagate into the particle-toughened interlayer region of the composite. Fig. 15 Microcracks in the intraply region...
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003056
EISBN: 978-1-62708-200-6
... techniques Mechanism Processes Limitations Condensation of atoms onto ceramic substrate Plating, evaporation, plasma sputtering, chemical vapor deposition Annealing may be required to remove residual stress Deposition of particles in organic medium or in liquid state Screen printing...
Abstract
Many applications of ceramics and glasses require them to be joined to each other or to other materials such as metals. This article focuses on ceramic joining technologies, including glass-metal sealing, glass-ceramic/metal joining, ceramic-metal joining, ceramic-ceramic joining, and the more advanced joining of nonoxide ceramics. It also discusses metallizing, brazing, diffusion bonding, and chemical bonding.
Series: ASM Handbook
Volume: 6
Publisher: ASM International
Published: 01 January 1993
DOI: 10.31399/asm.hb.v06.a0001457
EISBN: 978-1-62708-173-3
... are changing rapidly, with a major emphasis on structural applications. Furthermore, these materials are becoming more complex, in terms of being strengthened and toughened by transformation processes, the addition of other ceramic or metallic materials, or the development of performance-enhancing...
Abstract
This article is intended to assist the development of procedures for the brazing of ceramic-to-ceramic or ceramic-to-metal joints for service under elevated temperatures, mechanical or thermal stresses, or corrosive atmospheres. It describes the factors considered in preparing a procedure for the brazing of graphitic materials.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009075
EISBN: 978-1-62708-177-1
... interlayer-toughened composite that was lightly etched showing height differences on the sample surface using reflected-light differential interference contrast. 10× objective Another technique that is worth mentioning but is rarely used for enhancing the contrast of composite specimens is reflected...
Abstract
The analysis of composite materials using optical microscopy is a process that can be made easy and efficient with only a few contrast methods and preparation techniques. This article is intended to provide information that will help an investigator select the appropriate microscopy technique for the specific analysis objectives with a given composite material. The article opens with a discussion of macrophotography and microscope alignment, and then goes on to describe various illumination techniques that are useful for specific analysis requirements. These techniques include bright-field illumination, dark-field illumination, polarized-light microscopy, interference and contrast microscopy, and fluorescence microscopy. The article also provides a discussion of sample preparation materials such as dyes, etchants, and stains for the analysis of composite materials using optical microscopy.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009076
EISBN: 978-1-62708-177-1
..., and short fibers embedded in a matrix or adhesive. A common feature of interest is a toughening phase or particle either dispersed throughout the matrix or in the interlayer region. Large, complex structures with an array of different materials. Frequently, there are zones with intermingled phases...
Abstract
This article describes the various aspects relating to the selection and preparation of ultrathin-section specimens of fiber-reinforced polymeric composites for examination by transmitted light microscopy. It provides information on the contrast-enhancement methods used by transmitted-light microscopy and optimization of microscope conditions. Examples of composite ultrathin sections analyzed using transmitted-light microscopy contrast methods are also presented.
Book Chapter
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003422
EISBN: 978-1-62708-195-5
..., or dipping. The liquid can be water or volatile organics with organic binders in solution, inorganic or organic sols or solutions that form oxides, or thermosetting preceramic polymers or polymer solutions ( Ref 66 , 67 ). Hardening produces a coating composed of powder particles, bound together...
Abstract
This article describes the manufacture, post-processing, fabrication, and properties of carbon-carbon composites (CCCs). Manufacturing techniques with respect to the processibility of different geometries of two-directional and multiaxial carbon fibers are listed in a table. The article discusses matrix precursor impregnants, liquid impregnation, and chemical vapor infiltration (CVI) for densification of CCCs. It presents various coating approaches for protecting CCCs, including pack cementation, chemical vapor deposition, and slurry coating. Practical limitations of coatings are also discussed. The article concludes with information on the mechanical properties of CCCs.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003448
EISBN: 978-1-62708-195-5
...) are a diverse class of materials that consist of a metallic alloy matrix typically reinforced with a ceramic phase in the form of particles, platelets, whiskers, short fibers, and continuously aligned fibers (Ref 1 , 2 , and 3 ). Metal-matrix composites are used in structural applications...
Abstract
Metal-matrix composites (MMCs) are used in structural applications, and in applications requiring wear resistance, thermal management, and weight savings. This article summarizes the mechanical and thermal properties of discontinuously reinforced aluminum MMCs, laminated metallic composites, and continuously aligned fiber reinforced MMCs.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003047
EISBN: 978-1-62708-200-6
... fillers, adhesion promoters, tackifiers, and tougheners. It gives a short note on functions of primers and primerless bonding. Applications of adhesives in automotive, aerospace, electronics, electrical, medical, sports, and construction sectors are also described. Finally, the article describes the steps...
Abstract
This article begins with an overview of the fundamentals of adhesive technology, including functions, limitations, adhesive joint types, and the key factors in the selection of adhesives, including application, type of joint, process limitation, mechanical requirement, and service conditions. It then focuses on the characteristics, types, and properties of the five groups of adhesives, such as structural, hot melt, pressure sensitive, water based, ultraviolet, and electron beam cured adhesives. The article also discusses the functions and applications of adhesive modifiers, including fillers, adhesion promoters, tackifiers, and tougheners. It gives a short note on functions of primers and primerless bonding. Applications of adhesives in automotive, aerospace, electronics, electrical, medical, sports, and construction sectors are also described. Finally, the article describes the steps in adhesive bonding, including storage and handling of adhesives, bonding preparation, adhesive application, tooling, and curing.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003067
EISBN: 978-1-62708-200-6
... in the event of a fire and prevent the passage of smoke and flames. Laminated glasses with intumescent interlayers offer the same or better fire ratings without the presence of the wire grid. Regulation of Heat and Light The control of heat loss through windows has advanced so much that the thermal...
Abstract
This article reviews the applications of traditional glasses in architecture, transportation, construction, houseware, containers, and fibers. It also describes uses of specialty glasses for aerospace and military applications, biomedical and dental applications, chemical-resistant applications, lighting, information display, electronic processing and electronic devices, optical and ophthalmic products, and communications equipment.
Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001320
EISBN: 978-1-62708-170-2
... toughness by a transformation toughening or crack deflection mechanism ( Ref 4 , 5 ), but it decreases the thermal conductivity and hardness of the tool. Additions of up to 30 vol% TiC to Al 2 O 3 make the inserts black and improve the thermal conductivity, hardness, and toughness of the tools without...
Abstract
The classes of tool materials for machining operations are high-speed tool steels, carbides, cermets, ceramics, polycrystalline cubic boron nitrides, and polycrystalline diamonds. This article discusses the expanding role of surface engineering in increasing the manufacturing productivity of carbide, cermet, and ceramic cutting tool materials used in machining operations. The useful life of cutting tools may be limited by a variety of wear processes, such as crater wear, flank wear or abrasive wear, builtup edge, depth-of-cut notching, and thermal cracks. The article provides information on the applicable methods for surface engineering of cutting tools, namely, chemical vapor deposited (CVD) coatings, physical vapor deposited coatings, plasma-assisted CVD coatings, diamond coatings, and ion implantation.
Series: ASM Handbook
Volume: 24
Publisher: ASM International
Published: 15 June 2020
DOI: 10.31399/asm.hb.v24.a0006559
EISBN: 978-1-62708-290-7
... between ceramic particles in the traditional sintering process and obtain a clean and high-strength bonding interface by sharing atoms ( Ref 5 ). As a result, the long-range-ordered crystal structure can be maintained to a higher temperature, and the MGC can have high-temperature strength...
Abstract
Directed-energy deposition (DED) is a kind of additive manufacturing (AM) technology based on synchronous powder feeding or wire feeding. This article provides a comprehensive coverage of DED for ceramic AM, beginning with an overview of DED equipment setup, followed by a discussion on DED materials and the DED deposition process. The bulk of the article is devoted to the discussion on the microstructure and properties of oxide ceramics, namely alumina and zirconia ceramics.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003059
EISBN: 978-1-62708-200-6
Abstract
This article provides crystallographic and engineering data for single oxide ceramics, zirconia, silicates, mullite, spinels, perovskites, borides, carbides, silicon carbide, boron carbide, tungsten carbide, silicon-nitride ceramics, diamond, and graphite. It includes data on crystal structure, density, mechanical properties, physical properties, electrical properties, thermal properties, and magnetic properties.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003064
EISBN: 978-1-62708-200-6
Abstract
Carbon-carbon composites (CCCs) are introduced in fields that require their high specific strength and stiffness, in combination with their thermoshock resistance, chemical resistance, and fracture toughness, especially at high temperatures. The use of CCCs has expanded as the price of carbon fibers has dropped and their mechanical properties have increased. This article begins with an overview of the carbon conversion processes, fiber properties and microstructures, and interfacial bonding and environmental interaction of carbon fibers, followed by a detailed discussion on the various techniques available for processing CCCs for specific applications, including preform fabrication (fiber weaving), densification, application of protective coatings, and joining. The article closes with a description of the mechanical and physical properties and applications of CCCs. The main applications of CCCs, in terms of money and mass, are in the military, space, and aircraft industries.
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