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Book: Fractography
Series: ASM Handbook
Volume: 12
Publisher: ASM International
Published: 01 June 2024
DOI: 10.31399/asm.hb.v12.a0007028
EISBN: 978-1-62708-387-4
... Abstract This article focuses on the fractography of Nitinol, a shape memory alloy of nickel and titanium, in superelastic biomedical applications, which primarily comprise drawn and/or laser-cut wire and tube components. Overload fracture, hydrogen embrittlement fracture, and fatigue fracture...
Abstract
This article focuses on the fractography of Nitinol, a shape memory alloy of nickel and titanium, in superelastic biomedical applications, which primarily comprise drawn and/or laser-cut wire and tube components. Overload fracture, hydrogen embrittlement fracture, and fatigue fracture are discussed in detail.
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in Failure Analysis of Medical Devices
> Analysis and Prevention of Component and Equipment Failures
Published: 30 August 2021
Fig. 24 Scanning electron microscopy micrographs showing (a) nitinol stent strut cracking and (b) fatigue fracture surface after prolonged ultrasonic cleaning
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in Failure Analysis of Medical Devices
> Analysis and Prevention of Component and Equipment Failures
Published: 30 August 2021
Fig. 26 Scanning electron microscopy images of fractured low-strength nitinol wire device. (a) Overview of fractured wire showing secondary cracks at the compressive side of the sharp shape-set bends, as marked by white arrows. (b) High-magnification view of fracture surface exhibiting
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Published: 30 August 2021
Fig. 26 (a) Nitinol wires. (b) General view of the fracture surface showing surface defects and massive corrosion, magnification 150×. (c) Detail of the fracture surface showing a ductile fracture, magnification 3500×. (d) Acicular microstructure and the progression of lateral cracking. (e
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Published: 30 August 2021
Fig. 29 SEM image of cracks from other locations on the nitinol stent
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Published: 30 August 2021
Fig. 30 SEM image showing a nitinol wire in compression with cracks at the intrados and no cracking at the extrados
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Published: 30 August 2021
Fig. 32 SEM image of compression-induced cracks in a nitinol wire sample subjected to 50% strain
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Published: 30 August 2021
Fig. 33 SEM image of slip lines and cracks in a compression-damaged nitinol wire sample subjected to 31% strain
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Published: 30 August 2021
Fig. 34 Metallographic image of intrados cracks in compressed and released nitinol wire sample. Cracks initiate in shear during compression and grow in tension upon release
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Published: 15 December 2019
Fig. 37 Martensite in nitinol (Ni-50at.%Ti) shape memory alloy revealed by etching using equal parts HNO 3 , acetic acid, and hydrofluoric acid, and viewed using bright field (a) and Nomarski DIC (b). Nomarski DIC reveals more detail compared with bright field.
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Published: 01 June 2012
Fig. 5 Elastic strain characteristics of Nitinol. Adapted from Ref 43
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Published: 01 June 2012
Fig. 18 Laser-welded microforceps made from Nitinol. Source: Ref 1
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Published: 01 June 2012
Fig. 7 Typical stress-strain curve for Nitinol deformed to fracture above its M d temperature, where it can no longer transform to martensite. In this case, the specimen is 50.8 at.% Ni wire, and the test temperature is 160 °C (320 °F).
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Published: 01 June 2012
Fig. 10 Schematic map of apparent yield stress of Nitinol showing three distinct regions. Below M s , yielding is governed by the resistance to twin-boundary movement (solid line). Above M d , dislocation slip in the austenitic phase controls yielding (dashed line). Between M s and M d
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Published: 01 June 2012
Fig. 15 Traditional S - N curves for two fully annealed binary Nitinol alloys, one with M s = −30 °C (22 °F) and the other with M s = 70 °C (160 °F), representing typical stress-controlled fatigue. The reported stress is the total cyclic stress (σ max − σ min ), or two times the amplitude
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Published: 01 June 2012
Fig. 2 Ductile torsion fracture in Nitinol wire. Fracture surface is parallel to maximum shear stress.
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Published: 01 June 2012
Fig. 4 SEM image of microvoid coalescence in Nitinol from uniaxial tensile loading
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Published: 01 June 2012
Fig. 6 SEM image of directional microvoid coalescence in a Nitinol wire that fractured in bending (arrow identifies the crack growth direction)
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