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Brian S. Hayes, Luther M. Gammon
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George F. Vander Voort
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George F. Vander Voort
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Janina M. Radzikowska, George Vander Voort
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Book Chapter
Mounting of Specimens
Available to PurchaseSeries: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003786
EISBN: 978-1-62708-177-1
... Abstract Mounting of the specimen is often desirable or necessary for handling and metallographic polishing after the specimen is cut into an appropriate size. This article illustrates the different mechanical clamps used in mounting small specimens. It provides useful information...
Abstract
Mounting of the specimen is often desirable or necessary for handling and metallographic polishing after the specimen is cut into an appropriate size. This article illustrates the different mechanical clamps used in mounting small specimens. It provides useful information on compression molded mounts, which are molded with thermoplastic and thermosetting resins. The article reviews several resins and their key factors, which help in the selection of the most appropriate mounting method and resin. It also discusses the characteristics of plastic mounting materials. The article provides information on the molds and resins used for castable mounts, vacuum treatment of mounts, special mount arrangements, and mount marking and storage.
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in Thin Section Preparation and Transmitted Light Microscopy for Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
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in Thin Section Preparation and Transmitted Light Microscopy for Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
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Published: 31 October 2011
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Typical specimen-mounting method for the single-filament fiber tension test...
Available to Purchase
in Mechanical Testing and Properties of Plastics—An Introduction
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
Fig. 24 Typical specimen-mounting method for the single-filament fiber tension test (ASTM D 3379)
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Typical galvanic-corrosion test specimen using a threaded rod for mounting ...
Available to PurchasePublished: 01 January 2003
Fig. 4 Typical galvanic-corrosion test specimen using a threaded rod for mounting and electrical connection
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Schematic of taper sectioning (mounting), as applied to a coated specimen. ...
Available to PurchasePublished: 01 December 1998
Fig. 3 Schematic of taper sectioning (mounting), as applied to a coated specimen. Taper magnification equals the cosecant of taper angle, α.
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Method of (a) cutting a test specimen from a test button and (b) mounting t...
Available to PurchasePublished: 01 December 1998
Fig. 2 Method of (a) cutting a test specimen from a test button and (b) mounting the test specimen to retain flatness for metallographic examination. Dimensions are in inches.
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Schematic showing typical specimen-mounting method for the single-filament ...
Available to PurchasePublished: 01 January 2000
Fig. 26 Schematic showing typical specimen-mounting method for the single-filament fiber tension test (ASTM D 3379)
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Schematic showing typical specimen-mounting method for determining single-f...
Available to PurchasePublished: 01 January 2001
Fig. 2 Schematic showing typical specimen-mounting method for determining single-filament tensile strength
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Book Chapter
Sample Preparation and Mounting for Fiber-Reinforced Composites
Available to PurchaseSeries: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009072
EISBN: 978-1-62708-177-1
... Abstract This article describes how composite specimens are sectioned, documented, and labeled during sample preparation. The mounting procedures for the specimen are summarized. The article explains sample clamping, which involves not mounting the specimens using an adhesive or casting resin...
Abstract
This article describes how composite specimens are sectioned, documented, and labeled during sample preparation. The mounting procedures for the specimen are summarized. The article explains sample clamping, which involves not mounting the specimens using an adhesive or casting resin and corresponds to clamped samples used in automated polishing heads. It details that cavity molds involve mounting the composite specimens using a casting resin in a preset mold. The article also discusses the mounting of composite materials for hand polishing.
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(a) Automated polishing head containing circular sample openings. Notice th...
Available to Purchase
in Sample Preparation and Mounting for Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 15 (a) Automated polishing head containing circular sample openings. Notice the smaller sample length in the circular mounts. Also, circular cavities cannot accommodate unmounted composite specimens. The samples in this mount have been made with different mounting resins, which result
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Preparation steps for the development of a manual polishing mount. (a) Back...
Available to PurchasePublished: 01 January 2001
Fig. 2 Preparation steps for the development of a manual polishing mount. (a) Backup sides and three specimens. (b) The mount before bonding with epoxy. (c) Mold with taped ends for retaining mounting resin and holding samples while curing. (d) Mounted specimens ready to polish. (e) Manual
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Preparation steps for the development of a manual polishing mount. (a) Back...
Available to Purchase
in Sample Preparation and Mounting for Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 16 Preparation steps for the development of a manual polishing mount. (a) Backup sides with three specimens in the center. (b) Mount before bonding with epoxy. (c) Mold with taped ends for retaining the bonding resin and holding samples while curing. (d) Mounted specimens ready
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Effect of special techniques for improving edge retention of steel specimen...
Available to PurchasePublished: 01 December 2004
Fig. 25 Effect of special techniques for improving edge retention of steel specimens mounted in an epoxy resin. (a) Steel shot incorporated in the mount; specimen finish polished by a standard technique. (b) Edge protected by an electrodeposited coating of nickel; specimen finish polished
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Book: Composites
Series: ASM Handbook Archive
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003464
EISBN: 978-1-62708-195-5
... that it is not destroyed during the removal process or distorted. For thin materials, the specimen must be mounted first to resist deformation and then ground down to size. This grinding operation should also be done with ample cooling water so that the temperature is not increased. Before mounting the specimens...
Abstract
Microscopy is a valuable tool in materials investigations related to problem solving, failure analysis, advanced materials development, and quality control. This article describes the sample preparation techniques of composite materials. These techniques include mounting, rough grinding, and polishing. The preparation techniques of ultrathin sections are also summarized. The article explains the illumination methods used by reflected light microscopy to view a specimen. These consist of epi-bright-field illumination, epi-dark-field illumination, epi-polarized light, and epi-fluorescence. The article also provides information on transmitted light microscopy.
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Steps in the preparation of a taper section. (a) First mount, using an incl...
Available to PurchasePublished: 01 December 2004
Fig. 5 Steps in the preparation of a taper section. (a) First mount, using an inclined-surface plug. (b) Second mount, using a straight plug. (c) Mounted specimen before turning and grinding. (d) Mounted taper section after turning and grinding. See text for more information.
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Book Chapter
Metallographic Techniques in Failure Analysis
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003532
EISBN: 978-1-62708-180-1
... Abstract This article provides a discussion on the metallographic techniques used for failure analysis, and on fracture examination in materials, with illustrations. It discusses various metallographic specimen preparation techniques, namely, sectioning, mounting, grinding, polishing...
Abstract
This article provides a discussion on the metallographic techniques used for failure analysis, and on fracture examination in materials, with illustrations. It discusses various metallographic specimen preparation techniques, namely, sectioning, mounting, grinding, polishing, and electrolytic polishing. The article also describes the microstructure examination of various materials, with emphasis on failure analysis, and concludes with information on the examination of replicas with light microscopy.
Book Chapter
Metallographic Techniques in Failure Analysis
Available to PurchaseSeries: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006765
EISBN: 978-1-62708-295-2
... be performed with the scanning electron microscope (SEM) over the same magnification range as the LM, but examination with the latter is more efficient. This article describes the major operations in the preparation of metallographic specimens, namely sectioning, mounting, grinding, polishing, and etching...
Abstract
Metallographic examination is one of the most important procedures used by metallurgists in failure analysis. Typically, the light microscope (LM) is used to assess the nature of the material microstructure and its influence on the failure mechanism. Microstructural examination can be performed with the scanning electron microscope (SEM) over the same magnification range as the LM, but examination with the latter is more efficient. This article describes the major operations in the preparation of metallographic specimens, namely sectioning, mounting, grinding, polishing, and etching. The influence of microstructures on the failure of a material is discussed and examples of such work are given to illustrate the value of light microscopy. In addition, information on heat-treatment-related failures, fabrication-/machining-related failures, and service failures is provided, with examples created using light microscopy.
Book Chapter
Metallography and Microstructures of Cast Iron
Available to PurchaseSeries: ASM Handbook
Volume: 1A
Publisher: ASM International
Published: 31 August 2017
DOI: 10.31399/asm.hb.v01a.a0006342
EISBN: 978-1-62708-179-5
... Abstract The metallographic specimen preparation process for microstructural investigations of cast iron specimens usually consists of five stages: sampling, cold or hot mounting, grinding, polishing, and etching with a suitable etchant to reveal the microstructure. This article describes...
Abstract
The metallographic specimen preparation process for microstructural investigations of cast iron specimens usually consists of five stages: sampling, cold or hot mounting, grinding, polishing, and etching with a suitable etchant to reveal the microstructure. This article describes the general preparation of metallographic specimens and the methods of macroscopic and microscopic examination. Usually, gray-scale (black-and-white) metallography is sufficient for microstructural analysis of cast irons. The article discusses the use of color metallography of gray irons and ductile irons. It also presents application examples of color metallography.
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