This article provides guidelines for the assessment of model quality in materials science and engineering. It discusses the fundamentals of model quality assessment and the calibration of mechanistic material models. The article reviews the considerations for the model verification during software implementation planning to identify suitable programs, software components, and programming languages. It describes the validity tests used in model validation, including boundary-value tests, degenerate problem tests, sensitivity tests, and benchmarking. The article also presents an example of model calibration, verification, and validation for the prediction of martensite start temperature of steels.

This article provides a practical reference guide for instrumented indentation testing (IIT). It summarizes the various types of indenters used in IIT and parameters describing their geometries. The article discusses the physical principles and models used to determine hardness and elastic modulus from indentation load displacement data. Indentation deformation can be time-dependent, with the extent and nature of the time dependence strongly influenced by temperature. The article examines the methods for probing and characterizing the time-dependent phenomena. It also emphasizes the better-developed measurement techniques and procedures and calibrations required to obtain accurate and meaningful measurements.

Simulated service testing is the most reliable predictor of corrosion behavior that is important for specific objectives. These include materials selection, predicting the probable service life of a product or structure, evaluating new commercial alloys and processes, and calibrating laboratory corrosion tests in short of in-plant tests and actual service experience. This article provides a detailed discussion on the types of atmospheres used in simulated service testing. It describes the specifics of atmospheric-corrosion test that include equipment, test arrangement, and test specimen; factors affecting atmospheric corrosion; and evaluation of exposed atmospheric-corrosion panels. The article concludes with a discussion on the empirical model used for analyzing the atmospheric-corrosion measurements for estimating the service life of the part being evaluated.

Probability of detection (POD) assesses the performance of a non-destructive evaluation (NDE)-based inspection, which is a method used to determine the capability of an inspection as a function of defect type and defect size. This article provides an overview of the concept of POD, why it is needed, the history behind the development of POD, how POD assessments are performed, and how modeling and simulation can be integrated into the execution of a POD assessment. It describes the methods by which POD is determined. This includes detail on the experimental process to acquire the needed data, the mathematical methods to obtain a POD curve, and techniques to assess uncertainty in the POD curve as it is obtained from a limited data set. The concept of model-assisted POD (MAPOD) is introduced, with additional details and representative examples of MAPOD.

Miscellaneous hardness tests encompass a number of test methods that have been developed for specific applications. These include dynamic, or "rebound," hardness tests using a Leeb tester or a Scleroscope; static indentation tests on rubber or plastic products using the durometer or IRHD testers; scratch hardness tests; and ultrasonic microindentation testing. This article reviews the procedures, equipment, and applications associated with these alternate hardness test methods.

A key aspect of solidification process modeling is the treatment of the interface between the solidifying casting and the mold in which it is contained. This article begins with information on casting-mold interface heat-transfer phenomena. It describes practical considerations and methods for incorporating interface heat-transfer coefficient into models and for quantifying the heat transfer coefficient experimentally. The article concludes with information on the selection of the heat transfer coefficient for a given casting configuration.

The purpose of accreditation is to evaluate and assure high-quality results from suppliers of products or services without incurring the costs associated with auditing each supplier. This article describes laboratory accreditation based on the general requirements of International Organization for Standardization/International Electrotechnical Commission (ISO/IEC) Guide 25, "General Requirements for the Competence of Calibration and Testing Laboratories." The Guide 25 is a balanced standard that addresses quality system requirements of ISO 9000 and the technical requirements needed to perform testing or calibration. The article describes an accreditation process that would enhance the international acceptance of test data for mechanical testing laboratories.

This article provides a detailed overview of the thermomechanical modeling of additive manufacturing (AM) process. It begins with information on a basic understanding of the formation of residual stress during AM processing followed by a discussion on models commonly applied in AM modeling, such as heat-input models, material models, and material activation models. Information on experimental setup for validation and simulation of directed-energy deposition model is then included. The article also provides information on moving-source and part-scale analyses to simulate the laser powder-bed fusion AM process.

One of the key attributes of continuous fiber-reinforced ceramic composites (CFCCs) is their ability to undergo inelastic straining upon mechanical loading. This article reviews the mechanics of inelastic deformation and fracture of CFCCs, as needed for the development of damage-tolerant failure prediction methodologies for use in engineering design. It outlines a general framework for the description of fracture in structural materials in the presence of notches and cracks. The article describes the common classes of fracture behavior of CFCCs and presents the constitutive laws needed to describe crack-tip inelasticity. It demonstrates the effects of inelasticity on crack-tip stress fields and addresses the environmental degradation effects on damage tolerance.

This article examines how cellular automaton (CA) can be applied to the simulation of static and dynamic recrystallization. It describes the steps involved in the CA simulation of recrystallization. These include defining the CA framework, generating the initial microstructure, distributing nuclei of recrystallized grains, growing the recrystallized grains, and updating the dislocation density. The article concludes with information on the developments in CA simulations.

Thermoelastic stress analysis (TSA) an increasingly popular infrared (IR)-based technique for measuring stress on the surface of a part subjected to time-varying loads. This article begins by providing a theoretical and historical background of thermoelastic stress analysis. It then describes infrared detectors, such as quantum detectors and thermal/nonquantum detectors, for thermoelastic stress analysis. The article discusses the theoretical aspects for producing thermoelastic stress analysis data and the applications amenable to thermoelastic stress analysis. It concludes with information on the qualitative applications of thermoelastic stress analysis.

This article discusses a set of experimental and computational studies aimed at understanding the effect of various processing parameters on the extent of burr and other defect formation during sheet edge-shearing and slitting processes. It describes the development of experimentally validated finite-element models for analyzing the classes of shearing processes. The article also discusses the use of microstructural characterization with stereology to render three-dimensional volumetric parameters. It concludes with information on the numerical simulation of an edge-shearing process, along with sensitivity studies with respect to process and tool parameters.

Bioprinting has been advancing in the field of tissue engineering as the process for fabricating scaffolds, making use of additive manufacturing technologies. In situ bioprinting (also termed intraoperative bioprinting) is a promising solution to address the limitations of conventional bioprinting approaches. This article discusses the main approaches and technologies for in situ bioprinting. It provides a brief overview of the bioprinting pipeline, highlighting possible solutions to improve currently used approaches. Additionally, case studies of in situ bioprinting are provided and in situ bioprinting future perspectives are discussed.

Understanding fatigue crack growth is critical for the safe operation of many structural components. This article reviews the standard fracture mechanics and methods to determine the crack growth rate for a material and loading condition experimentally. It also addresses the two most important aspects of crack-growth modeling: loading environment and crack geometry.

This article discusses the inspection/reference standards that are absolutely critical for proper application of ultrasonic inspection systems. Many of the standards and specifications for ultrasonic inspection require the use of standard reference blocks. The article lists the variables that should be considered when selecting standard reference blocks and describes the three types of standard blocks ordinarily used for calibration or reference: area-amplitude blocks, distance-amplitude blocks, and blocks of the type sanctioned by the International Institute of Welding. It reviews the determination of area-amplitude and distance-amplitude curves of a straight-beam pulse-echo ultrasonic inspection system. The article discusses the three principal conventional manual ultrasonic sizing techniques: 6 dB drop technique, maximum-amplitude technique, and 20 dB drop technique. It provides information on the dimension-measurement applications of ultrasonic inspection methods.

Ultrasonic inspection is a nondestructive technique that is useful in both quality control and research applications for flaw detection in fiber-reinforced composite materials. This article describes ultrasonic nondestructive analysis by outlining its three basic types of scans. It reviews the important quality control techniques used during the manufacture of composite components by analyzing tooling control, material control, pattern orientation control, and in-process control.

Detailed analyses and test correlations are typically required to support design development, structural sizing, and certification. This article addresses issues concerning building block levels ranging from design-allowables coupons up through subcomponents, as these levels exhibit a wide variety of test-analysis correlation objectives. At these levels, enhanced analysis capability can be used most effectively in minimizing test complexity and cost while also reducing design weight and risk. The article discusses the examples of tests for which good correlative capability has shown significant benefit. These include notched (open and/or filled hole) tension and compression, inter/intralaminar shear and tension, and pin bearing.

This article describes the phenomena of crack initiation and early growth. It examines specimen design and preparation as well as the apparatus used in crack initiation testing. The article provides descriptions of the various commercially available fatigue testing machines: axial fatigue testing machines and bending fatigue machines. Load cells, grips and alignment devices, extensometry and strain measuring devices, environmental chambers, graphic recorders, furnaces, and heating systems of ancillary equipment are discussed. The article presents technologies available to accomplish closed loop control of materials testing systems in performing standard materials tests and for the development of custom testing applications. It explores the advanced software tools for materials testing. The article includes a description of baseline isothermal fatigue testing, creep-fatigue interaction, and thermomechanical fatigue. The effects of various variables on fatigue resistance and guidelines for fatigue testing are also presented.

The article provides an overview of the various types of testing machines: gear-driven or screw-driven machines and servohydraulic machines. It examines force application systems, force measurement, and strain measurement. The article discusses important instrument considerations and describes gripping techniques of test specimens. It analyzes test diagnostics and reviews the use of computers for gathering and reducing data. Emphasis is placed on universal testing machines with separate discussions of equipment factors for tensile testing and compressing testing. The influence of the machine stiffness on the test results is also described, along with a general assessment of test accuracy, precision, and repeatability of modern equipment.