The objective of quantitative metallography/stereology is to describe the geometric characteristics of the features. This article discusses the geometric attributes of microstructural features that can be divided into: the numerical extents and the number density of microstructural features; derived microstructural properties; feature specific size, shape, and orientation distributions; and descriptors of microstructural spatial clustering and correlations. It emphasizes on the practical aspects of the measurement techniques and applications. The article also provides information on the quantitative metallographic methods for estimation of volume fraction, total surface area per unit volume, and total length of per unit volume.

This article focuses specifically on material modeling applied to structure-property predictions. It provides general guidelines and considerations in terms of modeling the salient material features that ultimately impact the mechanical performance of parts produced by additive manufacturing (AM). Two of the primary ingredients needed to predict structure-property relationships via material modeling include a geometrical representation of the microstructural features of interest (e.g., grain structure and void defects) and a suitable constitutive model describing the material behavior, both of which can be scale and resource dependent. The article also presents modeling challenges to predict various aspects of (process-) structure-property relationships in AM.

The microstructure that develops during the solidification stage of cast iron largely influences the subsequent solid-state transformations and mechanical properties of the cast components. This article provides a brief introduction of methods that can be used for simulating the solidification microstructure of cast iron. Analytical as well as numerical models describing solidification phenomena at both macroscopic and microscopic scales are presented. The article introduces macroscopic transport equations and presents analytical microscopic models for solidification. These models include the dendrite growth models and the cooperative eutectic growth models. The article provides some solutions using numerical models to simulate the kinetics of microstructure formation in cast iron. It concludes with a discussion on cellular automaton (CA) technique that can handle complex topology changes and reproduce most of the solidification microstructure features observed experimentally.

The systematic study of microstructural evolution during deformation under hot working conditions is important in controlling processing variables to achieve dimensional accuracy. This article explains the microstructural features that need to be modeled and provides an outline of the principles and achievements of each of the various microstructural models, including black-box modeling, gray-box modeling, white-box modeling, and hybrid modeling.

Steel sheet is widely used for industrial and consumer products, partly because it is relatively strong, easily joined, and readily available at moderate cost. This article discusses the mechanical properties and formability of steel sheet, the use of circle grid analysis to identify the properties of complicated shapes, and various simulative forming tests. The mechanical properties of steel sheet that influence its forming characteristics, either directly or indirectly, can be measured by uniaxial tension testing. The article covers the effects of steel composition, steelmaking practices, and metallic coatings, as well as the correlation between microstructure and formability. A guide to the selection of steel sheet is also included. The formability of steel sheet is related to various microstructural features of the sheet. The article describes some of the forming characteristics of the more commonly used formable grades. It also lists the typical mechanical properties for common grades of hot-rolled and cold-rolled steel sheets.

This article describes metallographic preparation and examination techniques for stainless steels and maraging steels. It presents a series of micrographs demonstrating microstructural features of these alloys. Procedures used to prepare stainless steels for macroscopic and microscopic examination are similar to those used for carbon, alloy, and tool steels. Cutting and grinding must be carefully executed to minimize deformation because the austenitic grades work harden readily. The high-hardness martensitic grades that contain substantial undissolved chromium carbide are difficult to polish while fully retaining the carbides. Unlike carbon, alloy, and tool steels, etching techniques are more difficult due to the high corrosion resistance of stainless steels and the various second phases that may be encountered. The microstructures of stainless steels can be quite complex. Matrix structures vary according to the type of steel, such as ferritic, austenitic, martensitic, precipitation hardenable, or duplex.

Microstructural analysis is the combined characterization of the morphology, elemental composition, and crystallography of microstructural features through the use of a microscope. This article reviews three types of the most commonly used electron microscopies in metallurgical studies, namely scanning electron microscopy, electron probe microanalysis, and transmission electron microscopy. It briefly describes the operating principles, instrumentation which includes energy dispersive X-ray detectors, spatial resolution, typical use of the techniques, elemental analysis detection threshold and precision, limitations, sample requirements, and the capabilities of related techniques.

This article describes the effects of cyclic fatigue properties on aluminum alloys. It provides a discussion on strain-control fatigue and the effects of two microstructural features on the strain life of aluminum alloys: shearable precipitates and precipitate-free zones. The article discusses various models of fatigue crack growth (FCG) and the effects of alloy microstructure and composition on FCG.

Aluminum casting alloys are the most versatile of all common foundry alloys and generally have the highest castability ratings. This article discusses the designation and classification of aluminum casting alloys based on their composition and the factors influencing alloy selection. Alloys discussed include rotor alloys, commercial duralumin alloys, premium casting alloys, piston and elevated-temperature alloys, general-purpose alloys, magnesium alloys, aluminum-zinc-magnesium alloys, and bearing alloys. Six basic types of aluminum alloys developed for casting include aluminum-copper, aluminum-copper-silicon, aluminum-silicon, aluminum-magnesium, aluminum-zinc-magnesium, and aluminum-tin. The article also describes the main casting processes for aluminum alloys, which include die casting, permanent mold casting, sand casting (green sand and dry sand), plaster casting, and investment casting. In addition, the article discusses factors affecting the mechanical and physical properties, microstructural features that affect mechanical properties, the effects of alloying, and major applications of aluminum casting alloys.

This article explains how to prepare precious metal test samples for metallographic examination. It discusses cutting, mounting, grinding, polishing, and etching and addresses some of the challenges of working with small, relatively soft specimens. It includes dozens of example micrographs, comparing and contrasting the microstructural features of gold, platinum, iridium, palladium, and ruthenium-base alloys. It examines pure gold, intermetallic gold compounds, gold and platinum jewelry alloys, platinum-containing shape memory alloys, and alloys consisting of platinum, aluminum, and copper.

This article describes the dispersed-phase toughening of thermoset matrices by the development of multiphase-structure thermosetting matrices using rubber and/or thermoplastic materials. It discusses two main methods for manufacturing prepregs, namely, single-pass impregnation and double-pass impregnation. The article illustrates reflected-light optical microscopy techniques to evaluate the morphology of thermoplastic materials for determining the material quality and correlating key microstructural features with material performance.

Plastic deformation can occur in metals from various mechanisms, such as slip, twinning, diffusion creep, grain-boundary sliding, grain rotation, and deformation-induced phase transformations. This article emphasizes on the mechanism of slip and twinning under cold working conditions. It discusses the factors on which the structures developed during plastic deformation depend. These factors include crystal structure, amount of deformation, composition, deformation mode, and deformation temperature and rate. The article illustrates the microstructural features that appear after substantial deformation when revealed through metallographic investigation.

This article introduces the different types, distinctions, and grades of commercially pure titanium and titanium alloys. It describes three types of alloying elements: alpha stabilizers, beta stabilizers, and neutral additions. The article discusses the basic categories of titanium alloys, namely, alpha and near-alpha titanium alloys, beta and near-beta titanium alloys, and alpha-beta titanium alloys. It also describes the general microstructural features of titanium alloys.

Of the various thermal processing methods for steel, heat treating has the greatest overall impact on control of residual stress and on dimensional control. This article provides an overview of the effects of material- and process-related parameters on the various types of failures observed during and after heat treating of quenched and tempered steels. It describes phase transformations of steels during heating, cooling of steel with and without metallurgical transformation, and the formation of high-temperature transformation products on the surface of a carburized part. The article illustrates the use of carbon restoration on decarburized spring steels. Different geometric models for carbide formation are shown schematically. The article also describes the different microstructural features such as grain size, microcracks, microsegregation, and banding.