Search Results for microhardness analysis

Quantitative image analysis has expanded the capabilities of surface analysis significantly with the use of computer technology. This article provides an overview of the quantitative image analysis and optical microscopy. It describes the various steps involved in surface preparation of samples prone to abrasion damage and artifacts for quantitative image analysis.

This article presents the different hardness test methods used to measure the effectiveness of surface carbon control in carburized parts of steel. Common test methods include Rockwell hardness measurements, superficial Rockwell 15N testing, and microhardness testing. The article provides information on the microscopic method used to detect smaller variations in carbon content, and reviews consecutive cuts analysis and spectrographic analysis that are used to accurately evaluate the carbon concentration profile of carburized parts. It describes procedures of and precautions to be undertaken during shim stock analysis, which is used to measure the atmosphere carbon potential. The article includes a discussion on the electromagnetic nondestructive tests that are used to evaluate the case depth of case-hardened parts.

Case depth is the normal distance from the surface of the steel to the start of the core. Measurement of case depth is highly sensitive to the type of case hardening, original steel composition, quenching condition, and even to the testing method. This article describes the various methods of measuring case depth in steels, including chemical methods such as the combustion analysis and spectrographic analysis, microhardness test method, macroscopic and microscopic visual methods, and nondestructive methods. It contains a table that provides approximate equivalent hardness numbers for steel.

This article uses metal and alloy powders as examples to briefly discuss how to perform the characterization of powders. It begins by reviewing some of the techniques involved in the sampling of powders to ensure accurate characterization. This is followed by a discussion on the important properties to characterize powders, namely the particle size, surface area, density, porosity, particle hardness, compressibility, green strength, and flowability. For characterization of powders, both individual particles and bulk powders are used to evaluate their physical and chemical properties. The article also discusses the important characteristics and compositions of powder as well as impurities that directly affect powder properties. It ends with a description of the ignition and dust-explosion characteristics of organic and metal powders.

This article describes the characterization of welds as a sequence of procedures, where each procedure is concerned with a finer scale of detail. The first level of characterization involves information that may be obtained by direct visual inspection and measurement of the weld. The article discusses nondestructive evaluation of welds by encompassing techniques that are used to characterize the locations and structure of internal and surface defects, including radiography, ultrasonic testing, and liquid penetrant inspection. It reviews the macrostructural characterization of a sectioned weld, including features such as number of passes; weld bead size, shape, and homogeneity; and the orientation of beads in a multipass weld. The article provides examples that describe how welds are characterized according to the procedures.

This article describes the two commonly used standardized tests for determining the mechanical properties of thermal spray coatings: hardness testing and tensile adhesion testing. It discusses the destructive and non-destructive methods of residual-stress measurement. Electrochemical testing methodologies include two distinctly different methods: direct and alternating current impedance techniques for assessing the corrosion resistance of coating attributes. The article also reviews the testing methods for determining thermomechanical and environmental stability of thermal barrier coatings. It discusses the wear testing methodologies that are standardized by ASTM, including the pin-on-disk, block-on-ring, dry sand/rubber wheel, erosion, metallographic apparatus abrasion, fretting wear, cavitation, reciprocating ball-on-flat, impact, and rolling contact fatigue test. The article concludes with a discussion on the methods of testing abradability and erosion resistance in abradable coatings.

Supercarburizing, also referred to as high-concentration carburizing, carbide-precipitation carburizing, and carbide dispersion, is a carburizing method that results in a large amount of dispersed particulate carbide, with carbon content as high as 2 to 3%, to obtain surfaces with high hardness and good wear resistance. This article briefly reviews the process of supercarburizing using conventional carburizing steel as well as steels developed for supercarburizing, including 20CrMnMo steel, 20Cr2Ni4 steel, 35Cr3SiMnMoV steel, and 20CrMnTi steel. In addition, it discusses supercarburized steel composition, carburizing characteristics, mechanical properties testing, and microstructure analysis of 35Cr3SiMnMoV steel.

Mechanical testing is an evaluative tool used by the failure analyst to collect data regarding the macro- and micromechanical properties of the materials being examined. This article provides information on a few important considerations regarding mechanical testing that the failure analyst must keep in mind. These considerations include the test location and orientation, the use of raw material certifications, the certifications potentially not representing the hardware, and the determination of valid test results. The article introduces the concepts of various mechanical testing techniques and discusses the advantages and limitations of each technique when used in failure analysis. The focus is on various types of static load testing, hardness testing, and impact testing. The testing types covered include uniaxial tension testing, uniaxial compression testing, bend testing, hardness testing, macroindentation hardness, microindentation hardness, and the impact toughness test.

This article reviews the failure analysis process with specific reference to the considerations that should be addressed when a casting has failed. It describes the failure analysis methodology for three failed cast components: an aluminum bracket, a bronze suction roll, and a steel automotive spindle. The article discusses failure analysis investigation by obtaining casting background information, planning the evaluation and selecting the appropriate casting for analysis, conducting a preliminary examination, conducting the proper material evaluations, and thoroughly evaluating the test data. It concludes with information on case studies that show how the methodology is adapted for differing materials, failure mechanisms, and failure circumstances.

Many metal failures involve fracture, and fractography is an essential activity in many, if not most, failure analysis (FA) investigations. This article introduces and illustrates the role of fractography in an FA investigation. Basic guidelines are briefly presented for investigating a failure and how fractography helps the FA investigator determine evidence. Examples are given throughout this article on how the examination of fracture surfaces discerns various sources of crack initiation and mechanisms of crack growth. The procedures for analyzing fractures also include several steps and techniques that involve photographic documentation, proper specimen handling, and visual or microscopic examination. The article also briefly describes the use of metallography in fracture analysis along with case studies as illustrative examples of various fracture mechanisms and modes.

This article describes a method for determining the dynamic indentation response of metals and ceramics. This method, based on split Hopkinson pressure bar testing, can determine rate-dependent characteristics of metals and ceramics at moderate strain rates. For example, dynamic indentation testing reveals a significant effect of loading rates on the hardness and the induced plastic zone size in metals and on the hardness and induced crack sizes of brittle materials. The article also explains the rebound and pendulum methods for dynamic hardness testing.

Thermal phenomena play a key role in the mechanics of surface finishing processes. This article provides information on the analysis and measurement of temperatures and associated thermal damage generated by finishing processes that are essential to the production of engineered components with controlled surface properties. Emphasis is placed on kinematically simple configurations of finishing processes, such as surface grinding, flat surface polishing, and lapping.

Quenching and partitioning (Q&P) steel is a term used to describe a series of C-Si-Mn, C-Si-Mn-Al, or other steels subjected to the quenching and partitioning heat treatment process. This article discusses the Q&P steel's chemical compositions and mechanical properties, and provides an overview of the important background and product characteristics with a focus on the automotive sheet steel application. It schematically represents the continuous annealing process, consequent phase-transformation behaviors, and forming-limit curves of Q&P steels. The article describes the parameters associated with resistance spot welding, laser welding, and metal active gas welding. It also provides useful information of retained austenite volume fraction measured by x-ray diffraction and electron backscatter diffraction. The article also examines microstructure evolution during tensile testing at different strain levels using electron backscatter diffraction.

Hardness testing is perhaps the simplest and the least expensive method of mechanically characterizing a material. This article provides an overview of the principles of hardness testing. It compares Brinell with Meyer hardness testing and hardness testing of fully cold worked metals with fully annealed metals. The article discusses the plastic deformation of ideal plastic metals under an indenter, by a flat punch, and by spherical indenters. The classification of the hardness tests using various criteria, including type of measurement, magnitude of indentation load, and nature of the test, is also provided.

Mechanical springs are used in mechanical components to exert force, provide flexibility, and absorb or store energy. This article provides an overview of the operating conditions of mechanical springs. Common failure mechanisms and processes involved in the examination of spring failures are also discussed. In addition, the article discusses common causes of failures and presents examples of specific spring failures, describes fatigue failures that resulted from these types of material defects, and demonstrates how improper fabrication can result in premature fatigue failure. It also covers failures of shape memory alloy springs and failures caused by corrosion and operating conditions.

The first part of this article focuses on two major forms of machining-related failures, namely machining workpiece (in-process) failures and machined part (in-service) failures. Discussion centers on machining conditions and metallurgical factors contributing to (in-process) workpiece failures, and undesired surface layers and metallurgical factors contributing to (in-service) machined part failures. The second part of the article discusses the effects of microstructure on machining failures and their preventive measures.

Induction hardening of steel components is the most common application of induction heat treatment of steel. This article provides a detailed account of electromagnetic and thermal aspects of metallurgy of induction hardening of steels. It describes induction hardening techniques, namely, scan hardening, progressive hardening, single-shot hardening, and static hardening. The article discusses the techniques used to control the heat pattern, and provides a brief review of quenching techniques used in the induction hardening. It provides guidelines for selecting the frequency and power for induction hardening, and describes common methods for measuring case depth, such as optical and microhardness, and surface hardness. It provides information on some complications and ambiguities associated with these measurements. The article also discusses the commonly used non-destructive testing methods, namely, magnetic particle testing, ultrasonic testing, and eddy current testing to evaluate induction-hardened components.

This article provides a detailed discussion on heat treatment of titanium alloys such as alpha alloys, alpha-beta alloys, and beta and near-beta alloys. Common processes include stress-relief, annealing, solution treating, aging, quenching, and age hardening. It provides information on the effects of alloying elements on alpha/beta transformation. The article also discusses the heat treating procedures, and the furnaces used for heat treating titanium and titanium alloys.

The ultrasonic additive manufacturing (UAM) process consists of building up solid metal objects by ultrasonically welding successive layers of metal tape into a three-dimensional shape with periodic machining operations to create detailed features of the resultant object. This article provides information on the materials, welding parameters, process consumables, procedures, and applications of the UAM. It describes the methods for determining metallurgical and mechanical properties of solid metal parts to assess the range of materials and applications for which the process is suited. These methods include peel testing, push-pin testing, and microhardness/nanohardness testing. The article also reviews the issues to be addressed in maintaining UAM fabrication quality.