This article describes the microcrack analysis of composite materials using bright-field illumination, polarized light, dyes, dark-field illumination, and epi-fluorescence.

The analysis of composite materials using optical microscopy is a process that can be made easy and efficient with only a few contrast methods and preparation techniques. This article is intended to provide information that will help an investigator select the appropriate microscopy technique for the specific analysis objectives with a given composite material. The article opens with a discussion of macrophotography and microscope alignment, and then goes on to describe various illumination techniques that are useful for specific analysis requirements. These techniques include bright-field illumination, dark-field illumination, polarized-light microscopy, interference and contrast microscopy, and fluorescence microscopy. The article also provides a discussion of sample preparation materials such as dyes, etchants, and stains for the analysis of composite materials using optical microscopy.

This article is an atlas of fractographs that helps in understanding the causes and mechanisms of fracture of cobalt alloys (cast Vitallium and cast ASTM F75 alloys) and in identifying and interpreting the morphology of fracture surfaces. The fractographs illustrate the fatigue fracture, microcrack, and stair-step fracture surface of these alloys.

Lightning damage in polymer composites is manifested by damage at both the macroscopic or visual level and within the material microstructure. This article illustrates the effects of the laboratory-generated lightning strikes on polymeric composites.

Split-Hopkinson pressure bar (SHPB) testing is traditionally used for determining the plastic properties of metals (which are softer than the pressure bar material) at high strain rates. However, the use of this method for testing ceramic has various limitations. This article provides a discussion on the operational principle of the traditional SHPB technique and the relevant assumptions in the derivation of the stress-strain relationship. It describes the inherent limitations on the validity of these assumptions in testing ceramics and discusses the necessary modifications in SHPB design and test procedure for evaluating high-strength brittle ceramics. The article includes information on the maximum strain rate that can be obtained in ceramics using an SHPB and the necessity of incident pulse shaping. It also reviews the specimen design considerations, interpretation of experimental results obtained from SHPB testing of ceramics, and effectiveness of the proposed modifications.

This article presents an overview of fatigue crack nucleation from the point of view of the material microstructure and its evolution during cycling. It describes the sites of microcrack nucleation at the free surfaces. The article discusses the relation of dislocation structures and surface relief and reviews the mechanisms of crack nucleation. The damage of material due to crack nucleation, the extent (in terms of the number of cycles) of the nucleation stage, and the factors influencing crack nucleation are discussed.

This article summarizes fatigue phenomena in metallic materials. It discusses fatigue under variable-amplitude (VA) loading, with emphasis on crack growth. The article presents the prediction models of crack initiation and crack growth under VA loading. It concludes with a discussion on the conditions associated with engineering applications of VA loading.

Fatigue damage in metals is caused by the simultaneous action of cyclic stress, tensile stress, and plastic strain. This article details the fundamental aspects of the stages of the fatigue failure process. These include cyclic plastic deformation prior to fatigue crack initiation, initiation of one or more microcracks, propagation or coalescence of microcracks to form one or more microcracks, and propagation of one or more macrocracks.

Thermal phenomena play a key role in the mechanics of surface finishing processes. This article provides information on the analysis and measurement of temperatures and associated thermal damage generated by finishing processes that are essential to the production of engineered components with controlled surface properties. Emphasis is placed on kinematically simple configurations of finishing processes, such as surface grinding, flat surface polishing, and lapping.

This article describes the microstructure, properties, and performance of carburized steels, and elucidates the microstructural gradients associated with carbon and hardness gradients. It provides information on case depth measurement, the factors affecting case depth, and the formation and causes of microcracks. The article discusses the effects of alloying elements on hardenability, the effects of excessive retained austenite and massive carbides on fatigue resistance, the effects of residual stresses and internal oxidation on fatigue performance of carburized steels. In addition, the causes of intergranular fracture at austenite grain boundaries and their prevention methods are explored. The article also describes the major mechanisms of bending fatigue crack initiation in carburized steels.

This article reviews the mechanical behavior and fracture characteristics that discriminate structural polymers from metals, including plastic deformation. It provides overviews of crack propagation and fractography. The article presents the distinction between ductile and brittle fracture modes. Several case studies of field failure in various polymers are also presented to illustrate the applicability of available analytical tools in conjunction with an understanding of failure mechanisms.

This article reviews the mechanical behavior and fracture characteristics that discriminate structural polymers from metals. It provides information on deformation, fracture, and crack propagation as well as the fractography involving the examination and interpretation of fracture surfaces, to determine the cause of failure. The fracture modes such as ductile fractures and brittle fractures are reviewed. The article also presents a detailed account of various fracture surface features. It concludes with several cases of field failure in various polymers that illustrate the applicability of available analytical tools in conjunction with an understanding of failure mechanisms.

Honeycomb-cored sandwich panels increase part stiffness at a lower weight than monolithic composite materials. This article illustrates an area of a honeycomb-cored sandwich structure composite cross section that is viewed using transmitted polarized light. This area shows the differences in the constituents and resin intermingling. The article discusses the factors that govern the honeycomb core movement and honeycomb core crush, with illustrations. Some common tests performed on honeycomb composites to characterize the skin-to-core bond strength are the climbing drum peel and flatwise tensile tests. The article concludes with a description on the reasons for core failure, which are analyzed after these tests.

Microscopy is a valuable tool in materials investigations related to problem solving, failure analysis, advanced materials development, and quality control. This article describes the sample preparation techniques of composite materials. These techniques include mounting, rough grinding, and polishing. The preparation techniques of ultrathin sections are also summarized. The article explains the illumination methods used by reflected light microscopy to view a specimen. These consist of epi-bright-field illumination, epi-dark-field illumination, epi-polarized light, and epi-fluorescence. The article also provides information on transmitted light microscopy.

The objective of quantitative metallography/stereology is to describe the geometric characteristics of the features. This article discusses the geometric attributes of microstructural features that can be divided into: the numerical extents and the number density of microstructural features; derived microstructural properties; feature specific size, shape, and orientation distributions; and descriptors of microstructural spatial clustering and correlations. It emphasizes on the practical aspects of the measurement techniques and applications. The article also provides information on the quantitative metallographic methods for estimation of volume fraction, total surface area per unit volume, and total length of per unit volume.

This article provides a summary of the concepts discussed in the articles under the Section “Failure Analysis” in ASM Handbook, Volume 21: Composites. Most of the information in this Section is geared toward organic-matrix composites, although there is some information on failure analysis and fractography of ceramic- and metal-matrix composites.

The design of structural components with nominally brittle materials is largely determined by their elastic moduli, density, and tensile strength. This article discusses some of the factors involved in the design and reliability through considerations of toughness and ductility of nominally brittle materials. It describes toughening by various bridging mechanisms, as well as process zone effects and their interaction with the bridging rupture zone. The article explains the phenomena that give rise to exceptional toughness and notch-insensitive mechanical behavior. It provides a schematic illustration of a basic cell model to characterize the inelastic strains that occur in ceramic-matrix composites and their dependence on the interface friction.

This article summarizes the understanding of the mechanisms and mechanical effects of fatigue processes in highly brittle materials, with particular emphasis on ceramics. It provides a discussion on room-temperature fatigue crack growth in monolithic ceramics, transformation-toughened ceramics, and ceramic composites under cyclic compression. The cyclic damage zones ahead of tensile fatigue cracks, crack propagation under cyclic tension or tension-compression loads, and elevated-temperature fatigue crack growth in monotonic and composite ceramics, are discussed. The article presents ceramic fatigue data for fatigue crack growth testing and concludes with a discussion on life prediction for ceramics or ceramic-matrix composites.

Cyanate ester resins are a family of high-temperature thermosetting resins that bridge the gap in thermal performance between engineering epoxy and high-temperature polyimides. This article discusses the chemistry, properties and characteristics of the cyanate ester resins. It describes the processing procedures for the cyanate ester resins and provides information on properties for selected applications, such as space applications, radomes, and printed circuit boards.

Interpretation of failures of ceramic-matrix composites, and in particular continuous fiber reinforced ceramic-matrix composites is complicated by the complex structure of the composite material. This article describes the failure characteristics and evidence of failure mechanisms of these composites, with illustrations.