This article focuses on the specimen preparation procedures of austenitic manganese steels: sectioning, mounting, and grinding. It provides information on macroexamination and microexamination of a fracture surface, the microstructure and special features of austenitic manganese steels, and the alloying elements used.

This article describes the fundamentals of titanium metallographic sample preparation. Representative micrographs are presented for each class of titanium alloys, including unalloyed titanium, alpha alloys, alpha-beta alloys, and beta titanium alloys. The article provides information on the macroexamination and microexamination for these alloys. It concludes with a discussion on the several metallographic techniques developed for specific purposes, such as recrystallization studies and microstructure/fracture topography correlations.

The two major types of beryllium-containing alloys are copper-berylliums and nickel-berylliums. The most widely used beryllium-containing alloys are wrought copper-berylliums, which provide good strength while retaining useful levels of electrical and thermal conductivity. This article provides information on the specimen preparation procedures, macroexamination, microexamination, and microstructures of beryllium, copper-beryllium alloys, as well as nickel-beryllium alloys. It also discusses health and safety measures associated with the specimen preparation of beryllium and beryllium-containing alloys.

Welding codes and standards usually require the qualification of welding procedures prior to being used in production. This is to ensure that welds will meet the minimum quality and mechanical property requirements for the application. This article provides an overview of the welding procedure qualification guidelines and test methods. It also reviews the codes, standards, and specifications that govern the design and fabrication of welded structures for the procedure qualification details that are appropriate for a given application.

Qualification of welding procedures and personnel is an important step to assure the quality and performance of any welded component or structure. This article summarizes common welding procedures, personnel qualification variables, and test methods. Welding procedure qualification tests can be categorized as either standard or special. The article discusses the purpose of qualifying a welding procedure to demonstrate that the resulting welds will meet prescribed quality standards and the qualification of the personnel.

This article focuses on the metallography and microstructures of wrought and cast aluminum and aluminum alloys. It describes the role of major alloying elements and their effect on phase formation and the morphologies of constituents formed by liquid-solid and/or solid-state transformations. The article also describes specimen preparation procedures and examines the microstructure of several alloy samples.

This article provides information on the microstructure of powder metal alloys and the special handling requirements of porous materials. It covers selection, sectioning, mounting, grinding, and polishing, and describes procedures, such as washing, liquid removal, and impregnation, meant to preserve pore structures and keep them open for analysis. The article compares and contrasts the microstructures of nearly 50 powder metal alloys, using them to illustrate the effect of consolidation and compaction methods as well as particle size, composition, and shape. It discusses imaging equipment and techniques and provides data on etchants and etching procedures.

Magnesium and its alloys are among the most difficult metals to prepare for metallographic examination. This article describes specimen preparation processes, including sectioning, mounting, grinding, and polishing. It discusses macro and microexamination techniques as well as related etching processes, including macroetching and color etching based on polarized light enhancement. The article concludes with an overview of the effects of alloying elements, including aluminum, beryllium, calcium, copper, iron, lithium, manganese, rare earth metals, silicon, silver, strontium, thorium, tin, zinc, and zirconium.

Fracture surfaces are fragile and subject to mechanical and environmental damage that can destroy microstructural features. This article discusses the importance of care and handling of fractures and the factors that need to be considered during the preliminary visual examination. It describes the procedures for sectioning a fracture and opening secondary cracks as well as the effect of nondestructive inspection on subsequent evaluation. The article provides information on the most common techniques for cleaning fracture surfaces. These techniques are dry air blast cleaning, replica stripping, organic-solvent cleaning, water-base detergent cleaning, cathodic cleaning, and chemical-etch cleaning.

This article describes various procedures used in the metallographic preparation of niobium, tantalum, molybdenum, and tungsten alloys. It provides information on sectioning, grinding, mounting, polishing, and electrolytic etching as well as alternate procedures that have been used on refractory metals. The article presents and analyzes several micrographs, provides etchant formulas for various materials, and discusses the unique characteristics of rhenium and its alloys.

This article describes the six fundamental factors that decide a tool's performance. These are mechanical design, grade of tool steel, machining procedure, heat treatment, grinding, and handling. A deficiency in any one of the factors can lead to a tool and die failure. The article presents a seven-step procedure to be followed when looking for the reason for a failure. A review of the results of the seven-point investigation may lead directly to the source of failure or narrow the field of investigation to permit the use of special tests.

This article discusses the principles of physical metallurgy and metallography of depleted uranium. It describes the techniques involved in the preparation of thin foils for transmission electron microscopy and illustrates the resulting microstructure of uranium and uranium alloys, with the aid of black and white images. The article also provides information on the applications of etching and examination of uranium alloys, at both macro and micro scales, in characterizing the grain structures, segregation patterns, inclusions, and the metal flow geometries produced by solidification and mechanical working processes.

This article describes the metallographic technique for nonferrous metals and special-purpose alloys. These include aluminum alloys, copper and copper alloys, lead and lead alloys, magnesium alloys, nickel and nickel alloys, magnetic alloys, tin and tin alloys, titanium and titanium alloys, refractory metals and alloys, zinc and zinc alloys, and wrought heat-resisting alloys. The preparation of specimens for metallographic technique includes operations such as sectioning, mounting, grinding, polishing, and etching of nonferrous metals and alloys. The article contains tables that list the etchants for macroscopic examination and microscopic examination of nonferrous metals and special-purpose alloys.

This article describes various evaluation techniques of fractography such as visual inspection, macroscopic and microscopic examinations that are used to resolve different aspects of failure. It gives a brief description and pictorial representation of various defects leading to fracture of metals, including laps, seams, cold shuts, cracks, inclusions, porosity, fatigue, and stress corrosion cracking.

This article contains tables that list standard reduction potentials for electrochemical reactions. The first table lists reactions alphabetically by element of interest. The second table is ranked by potential value. Potential is measured versus the Standard Hydrogen Electrode which has a value of 0.0000 V. Reactions with more than one voltage indicate that results have not been reconciled. Parenthetical materials not needed to balance reactions are catalysts.

This article focuses on the tests for evaluating the weldability, cracking susceptibility, weld pool shape, fluid flow, and weld penetration of base materials. These tests include different types of self-restraint tests, externally loaded tests for evaluating cracking susceptibility and weld penetration tests, weld pool shape tests, and Gleeble testing for evaluating weld pool shape, fluid flow, and weld penetration.

Proper sectioning of the surface to be examined is a very important step in preparing steel specimens. The first step in preventing damage to the metallurgical structure is to minimize the amount of sectioning that is done. This article discusses the various metallographic techniques, namely mounting, grinding, polishing, and etching involved in the microstructural analysis of carbon and alloy steels, case hardening steels, cast iron, ferrous powder metallurgy alloys, wrought and cast stainless steels, tool materials, steel castings, iron-chromium-nickel heat-resistant casting alloys and different product forms of steels.

Tool steels are prepared for metallographic examination in the same way as carbon steels with a few variations owing to hardness and alloying differences. This article explains what makes tool steels different and how to compensate for it when sectioning, mounting, grinding, polishing, and etching. It provides information and data on composition, hot working, austenitizing, tempering, and powder metal manufacturing and explains how it affects tool steel microstructure, using more than 100 detailed images.

Fracture surfaces can provide an important and indispensable record of many factors in simple or complex failures. Visual examination of fracture surfaces can reveal the type and direction of loading, with fracture-surface features often providing definitive evidence of torsion, tension, bending, and compressive loads. This article discusses tools and techniques of visual examination and characteristic features of fracture features. A brief review of ductile and brittle fracture-surface features is provided. The article also describes macroscopic features that can be used to identify fracture-initiation sites, locations of final overload, and the directions of crack propagation. In addition, the use of these features to characterize loading at the time of failure is also described.

This article provides information on the basic components of a light microscope, including the illumination system, collector lens, and optical and mechanical components. It describes optical performance in terms of image aberrations, resolution, and depth of field. The article discusses the examination of specimen surfaces using polarized light, phase contrast, oblique illumination, dark-field illumination, bright-field illumination, interference-contrast illumination, and phase contrast illumination. Special techniques and devices that may be used with the optical microscope, to obtain additional information, are also described. The article concludes with information on photomicroscopy and macrophotography.