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liquid nitrocarburizing
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Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005776
EISBN: 978-1-62708-165-8
... procedures, as well as the equipment used (salt bath furnaces) and safety precautions to be undertaken during the liquid nitriding process. It describes the different types of liquid nitriding process, namely, liquid pressure nitriding, aerated bath nitriding, and liquid nitrocarburizing. Environmental...
Abstract
The liquid nitriding process has several proprietary modifications and is applied to a wide variety of carbon steels, low-alloy steels, tool steels, stainless steels, and cast irons. This article discusses the applications, subclassifications, operating procedures, and maintenance procedures, as well as the equipment used (salt bath furnaces) and safety precautions to be undertaken during the liquid nitriding process. It describes the different types of liquid nitriding process, namely, liquid pressure nitriding, aerated bath nitriding, and liquid nitrocarburizing. Environmental considerations and the increased cost of detoxification of cyanide-containing effluents have led to the development of low-cyanide salt bath nitrocarburizing treatments. The article reviews the wear and antiscuffing characteristics of the compound zone produced in salt baths with the help of Falex scuff test.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003197
EISBN: 978-1-62708-199-3
..., carbon and hardness gradients, and process procedures of different types of case hardening methods: carburizing (gas, pack, liquid, vacuum, and plasma), nitriding (gas, liquid, plasma), carbonitriding, cyaniding and ferritic nitrocarburizing. An accurate and repeatable method of measuring case depth...
Abstract
Case hardening is defined as a process by which a ferrous material is hardened in such a manner that the surface layer, known as the case, becomes substantially harder than the remaining material, known as the core. This article discusses the equipment required, process variables, carbon and hardness gradients, and process procedures of different types of case hardening methods: carburizing (gas, pack, liquid, vacuum, and plasma), nitriding (gas, liquid, plasma), carbonitriding, cyaniding and ferritic nitrocarburizing. An accurate and repeatable method of measuring case depth is essential for quality control of the case hardening process and for evaluation of workpieces for conformance with specifications. The article also discusses various case depth measurement methods, including chemical, mechanical, visual, and nondestructive methods.
Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005929
EISBN: 978-1-62708-166-5
... Carburizing and Cyaniding of Steels” and “Liquid Nitriding of Steels” in ASM Handbook , Volume 4A. In addition, some variations include carbo-austempering and salt bath nitrocarburizing, as described subsequently. At one time, the use of cyanide-based carburizing salts was once an important procedure...
Abstract
This article provides information on the salt baths used for a variety of heat treatments, including heating, quenching, interrupted quenching (austempering and martempering), case hardening, and tempering. It describes two general types of salt bath systems for steel hardening: the first type uses atmosphere austenitizing followed by salt quench and the second type employs austenitizing salt baths with rapid transfer to the quench salt. The article provides a detailed account on the construction, advantages and disadvantages, and limitations of isothermal quenching furnaces, submerged-electrode furnaces, immersed-electrode furnaces, and externally heated furnaces. It discusses the important applications of various furnace designs, including the austempering of ductile iron, the hardening of tool steels, and the isothermal annealing of high-alloy steels.
Series: ASM Handbook
Volume: 18
Publisher: ASM International
Published: 31 December 2017
DOI: 10.31399/asm.hb.v18.a0006355
EISBN: 978-1-62708-192-4
... the coefficient of friction with a compound layer Increasing the fatigue strength of the components The methods of introducing atomic nitrogen, or both atomic nitrogen and atomic carbon, into the surface include the following: Gas nitriding and gas nitrocarburizing Liquid nitriding with salt...
Abstract
The surface of irons and steels can be hardened by introducing nitrogen (nitriding), nitrogen and carbon (nitrocarburizing), or nitrogen and sulfur (sulfonitriding) into the surface. This article lists the principal reasons for nitriding and nitrocarburizing, and summarizes the typical characteristics of nitriding processes along with a general comparison of carburizing processes in a table. It describes the two most common nitriding methods: gas nitriding and ion (plasma) nitriding. The article discusses the wear behavior of nitrided layers and the wear resistance of selected steels. Rolling-contact fatigue (RCF) occurs in rolling contacts such as bearings, rolls, and gears. The article provides a discussion on rolling-contact fatigue of nitrided steels for aerospace bearing components.
Series: ASM Handbook
Volume: 4D
Publisher: ASM International
Published: 01 October 2014
DOI: 10.31399/asm.hb.v04d.a0005959
EISBN: 978-1-62708-168-9
... by a discussion on physical metallurgy, including crystallographic identity, thermal stability and decomposition, nitrogen and carbon solubility in expanded austenite, and diffusion kinetics of interstitials. It provides a description of low-temperature nitriding and nitrocarburizing processes for primarily...
Abstract
Low-temperature surface hardening is mostly applied to austenitic stainless steels when a combination of excellent corrosion performance and wear performance is required. This article provides a brief history of low-temperature surface hardening of stainless steel, followed by a discussion on physical metallurgy, including crystallographic identity, thermal stability and decomposition, nitrogen and carbon solubility in expanded austenite, and diffusion kinetics of interstitials. It provides a description of low-temperature nitriding and nitrocarburizing processes for primarily austenitic and, to a lesser extent, other types of stainless steels along with practical examples and industrial applications of these steels.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005806
EISBN: 978-1-62708-165-8
... Abstract This article summarizes the terminology for gas reactions, and discusses low-temperature nitriding and nitrocarburizing of stainless steels. It describes the various nitriding processes, namely, high- and low-pressure nitriding, oxynitriding, sulfonitriding, oxysulfonitriding, ferritic...
Abstract
This article summarizes the terminology for gas reactions, and discusses low-temperature nitriding and nitrocarburizing of stainless steels. It describes the various nitriding processes, namely, high- and low-pressure nitriding, oxynitriding, sulfonitriding, oxysulfonitriding, ferritic nitrocarburizing and austenitic nitrocarburizing. The article includes a discussion on the difficulties in specimen cleaning, importance of furnace purge, uses of pre and post oxidation, depassivation, or activation, and requirements for perfect nucleation in nitriding process. In nitriding, the successful atmosphere control depends on various potentials. The article summarizes the methods of measuring potentials in nitriding and nitrocarburizing, provides useful information on the furnaces used, and the safety precautions to be followed in the nitriding process. It also describes the sample preparation procedures and testing methods to ensure the quality of the sample.
Series: ASM Handbook
Volume: 4D
Publisher: ASM International
Published: 01 October 2014
DOI: 10.31399/asm.hb.v04d.a0005958
EISBN: 978-1-62708-168-9
... and nitrocarburizing processes and the equipment required for heat treating tool steels to improve hardness, wear resistance, and thermal fatigue. The various nitriding and nitrocarburizing processes covered are salt bath nitrocarburizing, gas nitriding and nitrocarburizing, and plasma nitriding and nitrocarburizing...
Abstract
This article provides a detailed discussion on the heating equipment used for austenitizing, quenching, and tempering tool steels. These include salt bath furnaces, controlled atmosphere furnaces, fluidized-bed furnaces, and vacuum furnaces. The article discusses the types of nitriding and nitrocarburizing processes and the equipment required for heat treating tool steels to improve hardness, wear resistance, and thermal fatigue. The various nitriding and nitrocarburizing processes covered are salt bath nitrocarburizing, gas nitriding and nitrocarburizing, and plasma nitriding and nitrocarburizing.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005771
EISBN: 978-1-62708-165-8
... case than carburizing; gas control critical Liquid (cyaniding) Diffused carbon and nitrogen 760–870 1400–1600 2.5–125 μm (0.1–5 mils) 50–65 (a) Low-carbon steels Good for thin cases on noncritical parts; batch process; salt disposal problems Ferritic nitrocarburizing Diffused carbon...
Abstract
Surface hardening improves the wear resistance of steel parts. This article focuses exclusively on the methods that involve surface and subsurface modification without any intentional buildup or increase in part dimensions. These include diffusion methods, such as carburizing, nitriding, carbonitriding, and austenitic and ferritic nitrocarburizing, as well as selective-hardening methods, such as laser transformation hardening, electron beam hardening, ion implantation, selective carburizing, and surface hardening with arc lamps. The article also discusses the factors affecting the choice of these surface-hardening methods.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005818
EISBN: 978-1-62708-165-8
... Nitrocarburizing of Steels” ) Salt (cyanate-cyanide) baths (see “Liquid Nitriding of Steels” ) Plasmas (ionized gases, as, for example, based on N 2 -H 2 gas mixtures) (see “Plasma (Ion) Nitriding and Nitrocarburizing of Steels” ) Powder media (based on CaCN 2 , calcium-cyanamide, which delivers NH...
Abstract
The nitriding process typically involves the introduction of nitrogen into the surface-adjacent zone of a component, usually at a temperature between 500 and 580 deg C. This article provides an overview of the essential aspects of the thermodynamics and kinetics of nitriding and nitrocarburizing of iron-base materials with gaseous processes. It describes nitriding potentials and the Lehrer diagram, carburizing potentials, controlled nitriding and nitrocarburizing, and the microstructural evolution of the compound layer and the diffusion zone.
Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005927
EISBN: 978-1-62708-166-5
... and decarburizing atmosphere; nitrocarburizing and nitriding atmosphere; carburizing and carbonitriding atmosphere; and chemical vapor deposition atmosphere. External resistance heating, external combustion heating, internal resistance heating, direct resistance heating, submerged combustion heating, and internal...
Abstract
This article discusses the important characteristics of fluidized beds. The total space occupied by a fluidized bed can be divided into three zones: grid zone, main zone, and above-bed zone. The article discusses the various types of atmospheres of fluidized beds, such as oxidizing and decarburizing atmosphere; nitrocarburizing and nitriding atmosphere; carburizing and carbonitriding atmosphere; and chemical vapor deposition atmosphere. External resistance heating, external combustion heating, internal resistance heating, direct resistance heating, submerged combustion heating, and internal combustion heating can be used to achieve the heat input for a fluidized bed. The article also describes the operations, design considerations, and applications of fluidized-bed furnaces in heat treating. Thermochemical surface treatments, such as carburizing, carbonitriding, nitriding, and nitrocarburizing, are also discussed. Finally, the article reviews the principles and applications of fluidized-bed heat treatment.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.9781627081658
EISBN: 978-1-62708-165-8
Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001306
EISBN: 978-1-62708-170-2
... deburring may be unnecessary. However, for intricate parts such as those shown in Fig. 1 , separate deburring operations generally are required. The use of liquid deburring methods is not usually suitable, especially if such liquids are corrosive. Thus, acid pickling is not recommended, because acid...
Abstract
Specialty steels encompass a broad range of ferrous alloys noted for their special processing characteristics (powder metallurgy alloys), corrosion resistance (stainless steels), wear resistance and toughness (tool steels), high strength (maraging steels), or magnetic properties (electrical steels). This article provides a detailed discussion on the various surface treatments, including cleaning, nitriding, carburizing, coating, and plating, performed on specialty steels.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005762
EISBN: 978-1-62708-165-8
..., and others ( Ref 4 , 5 ). The nitriding process of nitrocarburizing also has been improperly used as reference to the carbonitriding process. Part of this confusion is that the term carbonitriding seems to imply a nitriding process. However, carbonitriding is a modified form of carburizing, while...
Abstract
Carbonitriding is a modified form of carburizing that involves the introduction and diffusion of atomic nitrogen into the surface steel during carburization. This article discusses the composition, depth, and hardenability of a carburized case, and demonstrates how to control atmosphere in batch and continuous furnaces. It discusses the most important considerations in the selection of carbonitriding temperature. The article also describes the processing factors for minimizing retained austenite in the carbonitrided case. Hardness testing and carbonitriding of powder metallurgy parts, quenching and tempering of carbonitrided steel parts, and applications of carbonitriding are also covered in the article.
Series: ASM Handbook
Volume: 4D
Publisher: ASM International
Published: 01 October 2014
DOI: 10.31399/asm.hb.v04d.a0005977
EISBN: 978-1-62708-168-9
... Micrograph of nitrocarburized AISI 316 (673 K for 4 h) showing the S-phase layer above the austenitic matrix. Source: Ref 14 Fig. 16 Micrograph of nitrided AISI 316 (773 K for 22 h) showing the S-phase layer above the austenitic matrix with the nitride layer at the top. Source: Ref 14...
Abstract
Stainless steels are essential for the modern industrial civilization because of their corrosion resistance, especially in the chemical, petrochemical, and food industries. This article discusses the classification of the various types of stainless steels, including martensitic, ferritic, austenitic, duplex (ferritic-austenitic), and precipitation-hardening stainless steels. It presents a checklist of characteristics to be considered in selecting the proper type of stainless steel for a specific application. The article also outlines the need to promote the formation of an effective protective passive layer in stainless steels. It discusses hardness, fatigue and fretting properties, tribological properties, wear resistance, and corrosion-wear process of the S-phase layer. The article describes two thermochemical nitriding techniques of stainless steels: plasma-assisted nitriding techniques and non-plasma assisted nitriding processes. It also describes the difficulties in stainless steel nitriding/carburizing.
Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005956
EISBN: 978-1-62708-166-5
... significantly defines the behavior of the final distortion. With this static influence of the carbon depth profile, and the characteristics of the quenchant and the geometry, especially for liquids such as in oil- or water-based systems, a superposition occurs with the local incident flow. All of these factors...
Abstract
The process of case hardening of steel includes three consecutive steps of heat treatment: heating; the thermochemical process with the enrichment of the surface area during the carburizing or carbonitriding stage with carbon and nitrogen; and the subsequent quenching process for hardening. This article provides a model-based description of the development of residual stresses during case hardening. It also describes the influence and effects of residual stresses and distortion in hardening, carburizing, and nitriding processes of the steel.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005784
EISBN: 978-1-62708-165-8
.... The article also describes the usage of stop-off paints in different heat treating processes, namely, carburizing and carbonitriding, deep carburizing, vacuum carburizing, nitriding and nitrocarburizing, and plasma nitriding. The article concludes by reviewing the application methods of stop-off paints...
Abstract
A wide variety of stop-off technologies for heat treatment are used to selectively prevent the diffusion of carbon and/or nitrogen during atmosphere carburizing, carbonitriding, vacuum carburizing, and various forms of nitriding. In addition to selective stop-off, technologies are also available for scale prevention in open-fired furnaces. This article describes two stop-off technologies, mechanical masking and copper plating, along with stop-off paints/compounds. Prior to the application of stop-off paints, the part surface of the furnaces should be properly cleaned and dried. The article also describes the usage of stop-off paints in different heat treating processes, namely, carburizing and carbonitriding, deep carburizing, vacuum carburizing, nitriding and nitrocarburizing, and plasma nitriding. The article concludes by reviewing the application methods of stop-off paints: brushing, dipping, dispensing, spraying and stamping.
Series: ASM Handbook
Volume: 22B
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.hb.v22b.a0005536
EISBN: 978-1-62708-197-9
... Evolution of the experimental and calculated carbon profiles of three samples of the Fe-13Cr-5Co-3Ni-2Mo-0.07C grade, carburized in the same conditions during 23, 53, and 145 min at 955 °C (1750 °F). Source: Ref 19 Gas Nitriding and Nitrocarburizing Nitriding and nitrocarburizing...
Abstract
This article focuses on the modeling and simulation of diffusion-controlled processes related to both materials processing such as heat treatments, and materials degradation from a practical perspective by using the one-dimensional (1-D) sharp interface approach. It describes various diffusion simulation models, such as one-phase simulations, moving phase-boundary simulations, and dispersed system simulations. The article presents case studies that illustrate some examples where diffusion simulations have been applied to industrial-based problems, with an emphasis on the approaches used and the lessons learned from performing such simulations.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003762
EISBN: 978-1-62708-177-1
... Liquid (cyaniding) 760–870 (1400–1600) 2.5–125 μm (0.1–5 mils) 50–65 Low-carbon steels Good for thin cases on noncritical parts, batch process, salt disposal problems Ferritic nitrocarburizing 565–675 (1050–1250) 2.5–25 μm (0.1–1 mil) 40–60 Low-carbon steels Low-distortion process for thin...
Book
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.9781627081702
EISBN: 978-1-62708-170-2
Book Chapter
Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0005585
EISBN: 978-1-62708-170-2
... transfer between the two surfaces or loss from either surface. Compare with abrasive wear. adsorption. The adhesion of the molecules of gases, dissolved substances, or liquids to the Glossary of Terms I 945 surfaces of solids or liquids with which they are in contact. aerated bath nitriding. A type...
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