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Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003644
EISBN: 978-1-62708-182-5
... available for laboratory studies of corrosion phenomena. The techniques and tests include no-applied-signal tests, small-signal polarization tests, large-signal polarization tests, scanning electrode techniques, and miscellaneous techniques. electrochemical corrosion electrochemical test...
Abstract
This article reviews the fundamentals of electrochemical corrosion test methods. The features and requirements of the instrumentation needed for an electrochemical test are briefly discussed. The article provides a discussion on the various electrochemical techniques and tests available for laboratory studies of corrosion phenomena. The techniques and tests include no-applied-signal tests, small-signal polarization tests, large-signal polarization tests, scanning electrode techniques, and miscellaneous techniques.
Book Chapter
Basic Inspection Methods (Pulse-Echo and Transmission Methods)
Available to PurchaseSeries: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006469
EISBN: 978-1-62708-190-0
...), and, to a certain degree, the shape and orientation of large flaws ( Fig. 9 ). C-scans: This format provides a semiquantitative or quantitative display of signal amplitudes obtained over an area of the test piece surface. This information can be used to map out the position of flaws on a plan view of the test...
Abstract
This article considers the two primary methods used for ultrasonic inspection: pulse-echo and the transmission methods. Pulse-echo inspection can be accomplished with longitudinal, shear, surface (Rayleigh), or Lamb (plate) waves using a diverse range of transducers. The article discusses the principles of each of these inspection methods. It describes the applications and the basic data formats for single-element transducer-based systems, including A-scans, B-scans, and C-scans. The article provides information on electronic equipment used for ultrasonic inspection. It also describes how specific material conditions produce and modify A-scan indications. The article provides information on the controls and their functions for the display unit of the electronic equipment. It describes the techniques used for the identification and characterization of flaws, namely, surface (Rayleigh) wave and ultrasonic polar scan techniques.
Book Chapter
Microwave- and Millimeter-Wave Inspection
Available to PurchaseSeries: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006475
EISBN: 978-1-62708-190-0
... Abstract Electromagnetic signals at microwave and millimeter-wave frequencies are well suited for inspecting dielectric materials and composite structures in many critical applications. This article presents a partial list of reported nondestructive testing (NDT) application areas...
Abstract
Electromagnetic signals at microwave and millimeter-wave frequencies are well suited for inspecting dielectric materials and composite structures in many critical applications. This article presents a partial list of reported nondestructive testing (NDT) application areas for microwaves. It discusses the advantages and limitations of inspection with microwaves. The article discusses the physical principles, including reflection and refraction, absorption and dispersion, scattering, and standing waves. It provides a discussion on terahertz (THz) imaging for nondestructive evaluation (NDE). The article concludes with information on ground-penetration radar (GPR) that uses electromagnetic radiation and detects the reflected signals from subsurface structures.
Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003659
EISBN: 978-1-62708-182-5
... of corrosion testing. corrosion-monitoring method electrical-resistance probe side-stream loop electrochemical noise hydrogen-probe corrosion rate ultrasonic thickness polarization-resistance corrosion potential alternating current data analysis IN-SERVICE MONITORING of industrial...
Abstract
This article describes the criteria for selecting a corrosion-monitoring method used in industrial plants. It provides a detailed discussion on the design, advantages, and disadvantages of plant corrosion-testing program. The basic types of racks used to support and insulate the coupons are also discussed. The analysis of electrical-resistance probes, sentry holes, side-stream loop, electrochemical noise, hydrogen-probe, and process streams are used to monitor and estimate corrosion rates. The corrosion rates can also be estimated by ultrasonic thickness measurements, polarization-resistance measurements, corrosion potential measurements, and alternating current impedance measurements. Corrosion monitoring strategies, such as locations, data analysis, redundancy, and other issues, are discussed. The article concludes with information on the interpretation and reporting of corrosion testing.
Book Chapter
Microbiologically Influenced Corrosion Testing
Available to PurchaseSeries: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003647
EISBN: 978-1-62708-182-5
... values of 1 or less due to accumulation of H 2 SO 4 . Total corrosion loss determined from integrated R p data was less for the control sample than for the flushed sample. Large Signal Polarization Large signal polarization is applied to obtain potentiostatic or potentiodynamic polarization...
Abstract
Corrosion resulting from the presence and activities of microbes on metals and metal alloys is generally referred to as microbiologically influenced corrosion (MIC). This article describes the biofilm formation and structure and microbial processes influencing corrosion. It also discusses the electrochemical techniques used to study and monitor MIC and presents examples of their applications to MIC.
Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003656
EISBN: 978-1-62708-182-5
...-corrosion cracking. Because localized corrosion is isolated to certain areas and often has small lateral dimensions compared with its depth, detection methods that measure response over a large surface area, such as the widely used electrical resistance and linear polarization methods ( Ref 1 , 2 , 3 , 4...
Abstract
This article provides a discussion on the operation of various methods and sensors that have been used or have the potential to be used for on-line, real-time monitoring of localized corrosion. These include the electrochemical noise (ECN) method, nonelectrochemical methods, the galvanically coupled differential flow cell, galvanically coupled crevice cell, coupled multielectrode sensor, and electrochemical biofilm activity sensor.
Book Chapter
Corrosion Testing of Coatings
Available to PurchaseBook: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001296
EISBN: 978-1-62708-170-2
... of measuring polarization resistance is that only a very small potential range has to be scanned, and thus the measurements take less time. On the other hand, a charge transfer-controlled condition can be reached with very low scan rates without a large increase in total measuring time. Impedance...
Abstract
This article focuses on the testing and typical corrosion behavior of coating-substrate systems in aqueous solutions and humid aggressive atmospheres. It includes a short review of the fundamentals of corrosion, followed by a discussion of specific system behavior, electrochemical and laboratory accelerated tests, and simulated service tests. The article also contains examples of different types of corrosion damage and presents guidelines for improving corrosion resistance.
Book Chapter
Methods for Determining Aqueous Corrosion Reaction Rates
Available to PurchaseSeries: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003586
EISBN: 978-1-62708-182-5
... for corrosion testing ( Ref 1 , 2 , 3 , 4 , 5 , 6 , 7 , 8 , 9 , 10 , 11 , 12 , 13 , 14 , 15 , 16 ). This article highlights many of the commonly used laboratory methods used to determine instantaneous corrosion rates as well as methods that characterize corrosion thresholds that signal conditions...
Abstract
This article addresses electrochemical methods for instantaneous rate determination and threshold determination as well as nonelectrochemical methods that can determine incremental or cumulative rates of corrosion. Electrochemical methods for the study of galvanic corrosion rates and localized corrosion and evaluation of corrosion rates under paints are also discussed. The article describes nonelectrochemical methods that can determine incremental or cumulative rates of corrosion. Methods presented include polarization methods, polarization resistance methods, electrochemical impedance methods, frequency modulation methods, electrochemical noise resistance, potential probe methods, cyclic potentiodynamic polarization methods, potentiostatic and galvanostatic methods, electrochemical noise (EN) methods, scratch-repassivation method, and electrochemical impedance spectroscopy (EIS) techniques. Gravimetric determination of mass loss, electrical-resistance methods, magnetic methods, quartz crystal microbalance method, solution analysis methods, and metrological methods are nonelectrochemical methods. The article presents an electrochemical test that examines the susceptibility of stainless steel alloys to intergranular corrosion.
Book Chapter
Cure Monitoring and Control
Available to PurchaseBook: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003435
EISBN: 978-1-62708-195-5
... C b . If this situation is avoided, then the sample behaves as a simple dielectric. However, if this situation occurs, for example, for highly conductive resins, then charging of the electrodes through R masks other circuit responses. When 1/ R becomes large, electrode polarization becomes...
Abstract
This article discusses the attempts made by the industry to create sensing approaches for modeling a process, part, and chemistry and kinetics. It reviews microwave curing of thick-section composites and the resin cure sensors that are used for resin cure monitoring. These include dielectric cure sensors, fiberoptics-based resin cure sensors, ultrasonics-based resin cure sensors, and dosimetry-based resin cure sensors. The article provides information on the resin cure control flow sensing, flow modeling, flow mapping, and resin flow. It addresses some practical issues in sensing resin cure and flow.
Book Chapter
Electromagnetic Acoustic Transducers for Nondestructive Evaluation
Available to PurchaseSeries: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006458
EISBN: 978-1-62708-190-0
... electromagnetic acoustic transducer (EMAT) for generating shear waves propagating normally away from the test block front surface and polarized predominantly perpendicular to the coil wires nearest to the test block surface. (b) Small spiral coil, radial shear-wave permanent magnet (PM) EMAT approximately 25 mm...
Abstract
This article describes the basic features of electromagnetic acoustic transducers (EMATs) and discusses their existing and some potential uses within the field of ultrasonic nondestructive evaluation (UNDE). It provides sufficient basic and practical information to make an informed choice when considering the transducer to be used for any particular UNDE application. The article describes how different types of EMATs operate and presents their fundamental and some practical limitations. It summarizes the representative literature for electromagnetic acoustic transducer UNDE applications. Some successful uses of EMATs are mentioned to illustrate the depth, range, and potential of commercial EMAT applications. The article concludes with information on the commercial sources for EMAT systems and components.
Book Chapter
Corrosion Testing of Implantable Medical Devices
Available to PurchaseSeries: ASM Handbook
Volume: 23
Publisher: ASM International
Published: 01 June 2012
DOI: 10.31399/asm.hb.v23.a0005683
EISBN: 978-1-62708-198-6
... current density determination by Tafel extrapolation, potentiodynamic measurement of the polarization resistance, electrochemical impedance measurement, and potentiostatic deaeration. Tests combining corrosion and mechanical forces, such as fretting corrosion tests, environment-assisted cracking tests...
Abstract
The interaction of an implant with the human body environment may result in degradation of the implant, called corrosion. This article discusses the corrosion testing of metallic implants and implant materials. The corrosion environments for medical implants are the extracellular human body fluids, very complex solutions containing electrolytes and nonelectrolytes, inorganic and organic constituents, and gases. The article describes the fundamentals of electrochemical corrosion testing and provides a brief discussion on various types of corrosion tests. It illustrates corrosion current density determination by Tafel extrapolation, potentiodynamic measurement of the polarization resistance, electrochemical impedance measurement, and potentiostatic deaeration. Tests combining corrosion and mechanical forces, such as fretting corrosion tests, environment-assisted cracking tests, and ion-leaching tests are also discussed.
Book Chapter
Nondestructive Testing of Composites (Polymer- and Metal-Matrix Composites)
Available to PurchaseSeries: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006478
EISBN: 978-1-62708-190-0
... under test, typically has a wide dynamic range (>120 dB on some systems), and easily detects problems in multilayered structures. By comparing TT signal loss in adjacent good areas, porosity, unbonds, wrinkles, delaminations, and most inclusions can be detected. In the case of porosity, the signal...
Abstract
This article introduces the principal methodologies and some advanced technologies that are being applied for nondestructive evaluation (NDE) of fiber-reinforced polymer-matrix composites. These include acoustic emission, ultrasonic, eddy-current, computed tomography, electromagnetic acoustic transducer, radiography, thermography, and low-frequency vibration methods. The article also provides information on NDE methods commonly used for metal-matrix composites.
Book
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.9781627081900
EISBN: 978-1-62708-190-0
Book Chapter
Nondestructive Testing
Available to PurchaseBook: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003436
EISBN: 978-1-62708-195-5
... test, typically has a wide dynamic range (>120 dB on some systems), and easily detects problems in multilayered structures. By comparing TT signal loss in adjacent good areas, porosity, unbonds, wrinkles, delaminations, and most inclusions can be detected. In the case of porosity, the signal loss...
Abstract
This article introduces the principal methodologies and some technologies that are being applied for nondestructive evaluation of composite materials. These include ultrasonic testing (UT), air-coupled UT, laser UT, ultrasonic spectroscopy, leaky lamb wave method, acousto-ultrasonics, radiography, X-ray computed tomography, thermography, low-frequency vibration methods, acoustic emission, eddy current testing, optical holography, and shearography. The article presents some examples are for fiber-reinforced polymer-matrix composites. Many of the techniques have general applicability to other types of composites such as metal-matrix composites and ceramic-matrix composites.
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006451
EISBN: 978-1-62708-190-0
... a small decrease in temperature. From a practical standpoint, TSA entails correlating a representative signal (e.g., load or displacement) from a mechanical test (either fatigue or impulse loading) to the output of a sensitive IR detector in order to extract the temperature change due to the thermoelastic...
Abstract
Thermoelastic stress analysis (TSA) an increasingly popular infrared (IR)-based technique for measuring stress on the surface of a part subjected to time-varying loads. This article begins by providing a theoretical and historical background of thermoelastic stress analysis. It then describes infrared detectors, such as quantum detectors and thermal/nonquantum detectors, for thermoelastic stress analysis. The article discusses the theoretical aspects for producing thermoelastic stress analysis data and the applications amenable to thermoelastic stress analysis. It concludes with information on the qualitative applications of thermoelastic stress analysis.
Book Chapter
In-Service Techniques—Damage Detection and Monitoring
Available to PurchaseSeries: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003653
EISBN: 978-1-62708-182-5
...-optic technology fluorescence method BECAUSE OF THE MAGNITUDE of the corrosion problem, its economic impact, and human safety factors, new methods for detecting and monitoring corrosion are being developed. Past efforts have resulted in new methods being used in the field or being tested...
Abstract
This article focuses on the methods that are being developed for detecting and monitoring corrosion: electrochemical methods, electromagnetic or sound wave methods, fiber-optic technology, fluorescence methods, and the Diffracto Sight method. It reviews the importance of data management and the Corrosion Expert System. It concludes with information on the simulation and modeling for incorporating the mechanisms of corrosion prevention into military hardware systems design and operation.
Book Chapter
Electrical Testing of Polymers
Available to PurchaseSeries: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003026
EISBN: 978-1-62708-200-6
... of frequency over which important dielectric relaxations may take place. Testing techniques can be divided into two broad categories. The first category contains techniques used for low (<10 8 Hz) frequencies, in which the wavelength of the electric field is large compared to sample dimensions...
Abstract
In terms of their electrical properties, plastics can be divided into thermosetting and thermoplastic materials, some of which are conductive or semiconductive. This article provides detailed information on factors that affect the property of plastics. It discusses the major test methods used to determine the following dielectric properties of plastics: dielectric breakdown voltage, dielectric strength, dielectric constant, dissipation factor, arc tracking resistance, insulation resistance, volume, and surface resistivity or conductivity. The test specifications and conditions, recommended by several U.S. and foreign testing organizations for characterizing the electrical properties of plastic materials are listed. The article describes the influence of these properties on selection of plastics for insulation application. An outline of the electromagnetic shielding and testing methods of electromagnetic interference are also provided. Designations, electrical properties, and applications of elastomers are tabulated.
Book Chapter
Well Casing External Corrosion and Cathodic Protection
Available to PurchaseSeries: ASM Handbook
Volume: 13C
Publisher: ASM International
Published: 01 January 2006
DOI: 10.31399/asm.hb.v13c.a0004114
EISBN: 978-1-62708-184-9
.... These include the determination of cathodic protection current by the casing polarization and CPP tests or by mathematical models; calculation of casing-to-anode separation; isolation of the casing from other facilities; consideration of stray current interference from other dc power sources; and determination...
Abstract
This article describes two principal methods for detecting well casing corrosion, namely, metal-loss tools and casing current measurement, as well as their limitations and advantages. It discusses the factors to be considered in designing well casing cathodic protection systems. These include the determination of cathodic protection current by the casing polarization and CPP tests or by mathematical models; calculation of casing-to-anode separation; isolation of the casing from other facilities; consideration of stray current interference from other dc power sources; and determination of the size and the location of the anode bed for effective current output for the desired life of the anode bed. The article concludes with a discussion on the commissioning and monitoring of cathodic protection systems.
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006454
EISBN: 978-1-62708-190-0
... nondestructive testing (NDT) methods in two key respects. The signal originates in the material itself, not in an external source, and AE detects movement, while most other methods detect existing geometrical discontinuities. Characteristics of AE inspection compared with other inspection methods include...
Abstract
Acoustic emission is the generation of stress waves by sudden movement in stressed materials. This article begins with a comparison of acoustic emission from most other nondestructive testing (NDT) methods, and discusses the range of applicability of acoustic emission. It describes the instrumentation principles of acoustic emission and reviews the role of acoustic emission in materials studies. The article illustrates the testing of metal-matrix composites (MMCs) using acoustic emission and the use of acoustic emission inspection in production quality control. It concludes with information on the structural test applications of acoustic emission inspection to find defects and to assess or ensure structural integrity.
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006471
EISBN: 978-1-62708-190-0
... ultrasonic waves; some examples are shown in Fig. 1 ( Ref 1 , 2 ). Conventional technologies most commonly have used single-element piezoelectric-based transducers that couple energy into a part using a couplant. This couplant can be a grease or gel in contact testing, or a large volume of fluid, commonly...
Abstract
This article discusses the advantages, disadvantages, applications, and selection criteria of various technologies and transduction modalities that can generate and detect ultrasonic waves. These include piezoelectric transducers, electromagnetic acoustic transducers (EMATs), laser ultrasound phased array transducers, magnetostriction transducers, and couplants. The article discusses four basic types of search units with piezoelectric transducers. These include the straight-beam contact type, the angle-beam contact type, the dual-element contact type, and the immersion type. The article concludes with information on immersion or contact type focused search units.
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