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Published: 01 December 2004
Fig. 12 Ultrathin section of a particle-modified interlayer-toughened composite material. Transmitted-light Hoffman modulation contrast, 20× objective
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Image
in Viewing Composite Specimens Using Reflected Light Microscopy[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 8 Cross section of a polished interlayer-toughened composite that was lightly etched showing height differences on the sample surface using reflected-light differential interference contrast. 10× objective
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Image
in Viewing Composite Specimens Using Reflected Light Microscopy[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 9 Cross sections of an interlayer-toughened composite material. (a) Bright-field illumination, 25× objective. (b) Same view but after the addition of a solvent-based laser dye (Magnaflux Zyglo, Magnaflux Corp.) to the sample surface. The laser dye is preferentially absorbed
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Image
Published: 01 December 2004
Fig. 15 Microcracks in the intraply region of an interlayer-toughened carbon fiber composite material that terminated at the interlayer region. Epi-fluorescence, 390–440 nm excitation, 25× objective
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Published: 01 December 2004
Fig. 8 Large view of a cross section of an interlayer-toughened composite showing multiple plies and interlayer regions. Bright-field illumination, 10× objective
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Published: 01 December 2004
Fig. 12 Fracture morphology in a particle interlayer-toughened thermoset-matrix composite. (a) Strain birefringence in the interlayer particles. Transmitted polarized light, 20× objective. (b) Some of the particles are found to bridge the formed cracks, and some particles are torn. Transmitted
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Published: 01 December 2004
Fig. 13 Fiber-matrix interfacial failure in an interlayer-toughened thermoset-matrix composite. Transmitted polarized light, full wave plate, 20× objective
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009071
EISBN: 978-1-62708-177-1
... transfer molding, vacuum-assisted resin transfer molding, and resin film infusion. It explains the composite- and matrix-toughening methods for fiber-reinforced composites, such as dispersed-phase toughening and interlayer toughening. The article concludes with information on optical microscopy, which...
Abstract
This article illustrates the polymer matrices used for composite materials. It describes the use of prepeg materials in manufacturing high-performance composites. The article discusses the various infusion processes for the development of fiber-reinforced composites, namely, resin transfer molding, vacuum-assisted resin transfer molding, and resin film infusion. It explains the composite- and matrix-toughening methods for fiber-reinforced composites, such as dispersed-phase toughening and interlayer toughening. The article concludes with information on optical microscopy, which provides an insight into the micro- and macrostructure of fiber-reinforced composites.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009081
EISBN: 978-1-62708-177-1
... interlayer-toughened composite failure mechanisms. aircraft industry brittle-matrix composite failures composite design composites c-scan methods dispersed-phase thermoset-matrix composite failures impact parameters impact response impact-damaged composites material characteristics optical...
Abstract
This article describes methods for analyzing impact-damaged composites in the aircraft industry. These include C-scan and x-radiography methods and optical microscopy. The article reviews brittle-matrix composite and tough-matrix composite failures. It explains the different types of composite failure mechanisms such as thermoplastic-matrix composite failure mechanisms, untoughened thermoset-matrix composite failure mechanisms, toughened thermoset-matrix composite failure mechanisms, dispersed-phase and rubber-toughened thermoset-matrix composite failure mechanisms, and particle interlayer-toughened composite failure mechanisms.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009080
EISBN: 978-1-62708-177-1
... impregnation material quality microstructure morphology particle interlayer toughening prepregs reflected-light optical microscopy single-pass impregnation thermoplastic materials thermoset-matrix composites THE PERFORMANCE of fiber-reinforced composite systems has evolved in response to new...
Abstract
This article describes the dispersed-phase toughening of thermoset matrices by the development of multiphase-structure thermosetting matrices using rubber and/or thermoplastic materials. It discusses two main methods for manufacturing prepregs, namely, single-pass impregnation and double-pass impregnation. The article illustrates reflected-light optical microscopy techniques to evaluate the morphology of thermoplastic materials for determining the material quality and correlating key microstructural features with material performance.
Image
Published: 01 December 2004
Fig. 9 Interlayer strain and fracture after impact of a toughened thermo-setting-matrix composite. Transmitted polarized light, full wave plate, 40× objective
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Image
Published: 01 December 2004
region (i.e., light-gray circles). Slightly uncrossed polarized light, 50× objective. (b) Ultrathin section developed from a particle-modified toughened interlayer composite that was sectioned through the thickness. Transmitted light, Hoffman modulation contrast, 40× objective. (c) Ultrathin section
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009079
EISBN: 978-1-62708-177-1
... the cracked area, it can be seen that many of the carbon fibers were separated from the matrix as a result of the crack propagation. In this material, the microcracks were found to not propagate into the particle-toughened interlayer region of the composite. Fig. 15 Microcracks in the intraply region...
Abstract
This article describes the microcrack analysis of composite materials using bright-field illumination, polarized light, dyes, dark-field illumination, and epi-fluorescence.
Image
Published: 01 December 2004
Fig. 3 Dispersed-phase-toughened carbon fiber composite material that was sectioned at an oblique angle to obtain a larger view of the interlayer region. Large, irregular ases, with some phases spherical and hollow, were found in the interlayer area and extended into the intraply area
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Image
Published: 01 December 2004
Fig. 10 Fracture morphology of a primary-phase-toughened matrix composite after impact. (a) Onset of hackle formation and strain in front of the crack tip. Transmitted polarized light, full wave plate, 40× objective. (b) Hackles in the interlayer region of the composite. Transmitted polarized
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Image
Published: 01 December 2004
Fig. 5 Impact damage of a carbon fiber composite material that has a toughened matrix. (a) Montage of the impact area. Epi-fluorescence, 390–440 nm excitation, 5× objective. (b) Wide crack formation in the 45° plies and mainly cohesive failure in the interlayer. Epi-fluorescence, 390–440 nm
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Image
Published: 01 December 2004
Fig. 4 Dispersed-phase-toughened carbon fiber composite material that was sectioned at an oblique angle to obtain a larger view of the interlayer region. A complex morphology was revealed, which was also present in the intraply area. Ultrathin section. Transmitted light, differential
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009075
EISBN: 978-1-62708-177-1
... interlayer-toughened composite that was lightly etched showing height differences on the sample surface using reflected-light differential interference contrast. 10× objective Another technique that is worth mentioning but is rarely used for enhancing the contrast of composite specimens is reflected...
Abstract
The analysis of composite materials using optical microscopy is a process that can be made easy and efficient with only a few contrast methods and preparation techniques. This article is intended to provide information that will help an investigator select the appropriate microscopy technique for the specific analysis objectives with a given composite material. The article opens with a discussion of macrophotography and microscope alignment, and then goes on to describe various illumination techniques that are useful for specific analysis requirements. These techniques include bright-field illumination, dark-field illumination, polarized-light microscopy, interference and contrast microscopy, and fluorescence microscopy. The article also provides a discussion of sample preparation materials such as dyes, etchants, and stains for the analysis of composite materials using optical microscopy.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003056
EISBN: 978-1-62708-200-6
Abstract
Many applications of ceramics and glasses require them to be joined to each other or to other materials such as metals. This article focuses on ceramic joining technologies, including glass-metal sealing, glass-ceramic/metal joining, ceramic-metal joining, ceramic-ceramic joining, and the more advanced joining of nonoxide ceramics. It also discusses metallizing, brazing, diffusion bonding, and chemical bonding.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003380
EISBN: 978-1-62708-195-5
... Volume , ASTM , April 1989 , p 251 – 269 15. Kageyama K. , Kimpara I. , Ohsawa I. , Hojo M. , and Kabashima S. , “Mode I and Mode II Delamination Growth of Interlayer Toughened Carbon/Epoxy Composite System,” STP 1230 , Composite Materials: Fatigue and Fracture...
Abstract
Delamination is one of the most commonly observed failure modes in composite materials. This article describes the three fundamental fracture failure modes of composite delamination, namely, opening, in-plane shearing, and tearing or scissoring shearing modes. It discusses the characterization and analysis of delamination. The article also reviews the prediction of delamination factors, such as flexbeam fatigue life, and skin/stiffener pull-off strength and life.
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