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interference-contrast illumination
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Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006684
EISBN: 978-1-62708-213-6
... illumination (not common today), and differential interference contrast, generally by the Nomarski technique. Bright-field illumination is usually the starting point for examination of microstructures, which should start before etching to detect nonmetallic inclusions, nitrides, carbides, and possibly voids...
Abstract
The reflected light microscope is the most commonly used tool to study the microstructure of metals, composites, ceramics, minerals, and polymers. For the study of the microstructure of metals and alloys, light microscopy is employed in the reflected-light mode using either bright-field illumination, dark-field illumination, polarized light illumination, or differential interference contract, generally by the Nomarski technique. This article concentrates on how to reveal microstructure properly to enable the proper identification of the phases and constituents and, if needed, measuring the amount, size, and spacing of constituents, using the light optical microscope. The discussion covers the examination of microstructures using different illumination methods and includes a comparison between light optical images and scanning electron microscopy images of microstructure.
Book: Fractography
Series: ASM Handbook
Volume: 12
Publisher: ASM International
Published: 01 January 1987
DOI: 10.31399/asm.hb.v12.a0001835
EISBN: 978-1-62708-181-8
... 120 s) are used to improve the signal-to-noise ratio. Contrast and brightness are modulated by the operator of the scanning electron microscope. A good micrograph exhibits a range of gray levels; as the number of gray levels increases, so does the information content of the micrograph. The operating...
Abstract
Scanning electron microscopy (SEM) has unique capabilities for analyzing fracture surfaces. This article discusses the basic principles and practice of SEM, with an emphasis on its applications in fractography. The topics include an introduction to SEM instrumentation, imaging and analytical capabilities, specimen preparation, and the interpretation of fracture features. SEM can be subdivided into four systems, namely, illuminating/imaging, information, display, and vacuum systems. The article also describes the major criteria and techniques of SEM specimen preparation, and the general features of ductile and brittle fracture modes.
Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001237
EISBN: 978-1-62708-170-2
... that requires a three-dimensional appearance. It uses low-angle illumination, so higher magnifications are limited. Polarized light is especially useful for analyzing optically anisotropic metals, such as beryllium, α-titanium, and zirconium. Differential interference contrast (DIC...
Abstract
Quantitative image analysis has expanded the capabilities of surface analysis significantly with the use of computer technology. This article provides an overview of the quantitative image analysis and optical microscopy. It describes the various steps involved in surface preparation of samples prone to abrasion damage and artifacts for quantitative image analysis.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006765
EISBN: 978-1-62708-295-2
... specimen edge (revealed using Nomarski differential interference contrast illumination) and the water stains (arrows on the aluminum specimen). Fig. 6 Light micrograph showing stain (arrows pointing up) from the etchant (Vilella’s reagent) that seeped from the shrinkage gap (wide arrows pointing...
Abstract
Metallographic examination is one of the most important procedures used by metallurgists in failure analysis. Typically, the light microscope (LM) is used to assess the nature of the material microstructure and its influence on the failure mechanism. Microstructural examination can be performed with the scanning electron microscope (SEM) over the same magnification range as the LM, but examination with the latter is more efficient. This article describes the major operations in the preparation of metallographic specimens, namely sectioning, mounting, grinding, polishing, and etching. The influence of microstructures on the failure of a material is discussed and examples of such work are given to illustrate the value of light microscopy. In addition, information on heat-treatment-related failures, fabrication-/machining-related failures, and service failures is provided, with examples created using light microscopy.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003230
EISBN: 978-1-62708-199-3
... lenses combined with convex lenses to relay the image. A larger light guide bundle is used, which provides higher illumination and a larger image with a higher degree of contrast. Hybrid borescopes are up to 990 mm (39 in.) long, and 5.5 to 12 mm (0.216 to 0.47 in.) in diameter. All hybrid borescopes...
Abstract
Visual inspection is a nondestructive testing technique that provides a means to detect and examine a variety of surface flaws, such as corrosion, contamination, surface finish, and surface discontinuities. This article discusses the equipment used to aid visual inspection, including borescopes (rigid and flexible), optical sensors, and magnifying systems. The article discusses the special features of borescopes, the factors that influence the choice of a flexible or rigid borescope for use in a specific application, and some of the image sensors used in visual inspection.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003244
EISBN: 978-1-62708-199-3
... cotton that will not scratch the polished surface. Etch time varies with etch strength and can only be determined by experience. In general, for high magnification examination, the etch should be shallower, while for low magnification examination a deeper etch yields better image contrast. Some etchants...
Abstract
This article describes the methods and equipments involved in the preparation of specimens for examination by light optical microscopy, scanning electron microscopy, electron microprobe analysis for microindentation hardness testing, and for quantification of microstructural parameters, either manually or by the use of image analyzers. Preparation of metallographic specimens generally requires five major operations: sectioning, mounting, grinding, chemical polishing, and etching. The article provides information on the principles of technique selection in mechanical polishing, and describes the procedures, advantages, and disadvantages of electrolytic and chemical polishing. It also provides a detailed account of procedures, precautions, and composition for preparation and handling of etchants.
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006447
EISBN: 978-1-62708-190-0
... acuity and contrast sensitivity. The Illuminating Engineering Society provides recommendations for lighting conditions, but the applicable code and standard according to the task usually addresses these values. Illumination should be not less than 350 lux and not more than 1000 lux and is measured...
Abstract
Visual inspection (VI) is the oldest inspection technique man has used as a quality-control tool to evaluate products, assess their final form in terms of fabrication accuracy and external features based on experience, and decide on their acceptance or rejection. This article discusses the basic principles of visual inspection in terms of direct visual examination and indirect visual examination as well as advantages and limitations of visual inspection. It reviews the factors affecting the effectiveness of VI as a nondestructive testing (NDT): lighting conditions of observation, condition of surface under inspection, physical state/condition of inspector, proper training of personnel and level of expertise, and knowledge of applicable standards. The article provides schematic illustrations of rigid borescopes, fiberscopes, and videoscopes. It concludes with a discussion on automated optical inspection systems.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003240
EISBN: 978-1-62708-199-3
... reconstruction. The real-time feature makes the liquid-surface system suitable for rapid inspection of large amounts of material on a continuous basis. In contrast, inspection with the scanning system is relatively slow. Photographic or videotape records for later study may be made with either system. The...
Abstract
Holography is basically a two-step process for creating a whole three dimensional image of a diffusely reflecting object having some arbitrary shape. This article discusses the advantages, disadvantages and applications of using the optical holography method in nondestructive evaluation. It also discusses the types of acoustical holography, including liquid-surface acoustical holography and scanning acoustical holography. The article concludes by comparing liquid-surface and scanning systems.
Book Chapter
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006474
EISBN: 978-1-62708-190-0
... provided by the scanning system requires reconstruction. The real-time feature makes the liquid-surface system suitable for the rapid inspection of large amounts of material on a continuous basis. In contrast, inspection with the scanning system is relatively slow. The prominent feature of the scanning...
Abstract
Acoustical holography is the extension of holography into the ultrasonic domain. The basic systems for acoustical holography are the liquid-surface type and the scanning type. This article discusses the applications for acoustical holography, including inspection of large composite parts, through-transmission breast imaging system, inspection of welds in thick materials, and inspection of sleeve-bearing stock. It describes the basic system for liquid-surface acoustical holography and scanning acoustical holography. A comparison between these techniques is also provided.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006681
EISBN: 978-1-62708-213-6
... micrometers; the halide grains transform to silver when electrons interact with them. The transformation to silver creates contrast in the film. The film is very sensitive to electrons and has a high detector quantum efficiency (DQE), which is the ratio of input/output signal-to-noise ratios, and indicates...
Abstract
Transmission electron microscopy (TEM) approach enables essentially simultaneous examination of microstructural features through imaging from lower magnifications to atomic resolution and the acquisition of chemical and crystallographic information from small regions of the thin specimen. This article discusses fundamentals of the technique, especially for solving materials problems. Background information is provided to help understand basic operations and principles, including instrumentation, the physics of signal generation and detection, image formation, electron diffraction, and spectrometry techniques with data analysis.
Series: ASM Handbook
Volume: 23
Publisher: ASM International
Published: 01 June 2012
DOI: 10.31399/asm.hb.v23.a0005685
EISBN: 978-1-62708-198-6
... objective lenses and eyepieces ( Fig. 1 , 2 ). The minimum feature resolution is approximately 0.2 μm. However, smaller features—as small as approximately 0.05 μm—can be detected by image contrast enhancement with polarized light, interference contrast, or dark-field illuminations. Fig. 1 Light...
Abstract
This article focuses on the modes of operation, physical basis, sample requirements, properties characterized, advantages, and limitations of common characterization methods that are used to evaluate the physical morphology and chemical properties of component surfaces for medical devices. The methods include light microscopy, scanning electron microscopy, atomic force microscopy, energy-dispersive x-ray spectroscopy, Auger electron spectroscopy, secondary ion mass spectrometry, x-ray photoelectron spectroscopy, Fourier transform infrared spectroscopy, and Raman spectroscopy.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006644
EISBN: 978-1-62708-213-6
... large cross section with thickness ranging from hundreds of micrometers to several millimeters. Different imperfections are identified through interpretation of contrast using well-established kinematical and dynamical theories of x-ray diffraction. The capability of in situ characterization during...
Abstract
X-ray topography is the general term for a family of x-ray diffraction imaging techniques capable of providing information on the nature and distribution of imperfections. This article provides a detailed account of x-ray topography techniques, providing information on the historical background and development trends in x-ray diffraction topography. The discussion covers the general principles, components of systems, and applications of x-ray topography techniques, namely conventional X-ray topographic techniques and synchrotron x-ray topographic techniques.
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006466
EISBN: 978-1-62708-190-0
... its very high-magnification mode and is employed as a counterpart to conventional optical and electron microscopy, that is, to see fine detail at and near surfaces. The scanning acoustic microscope, like the other acoustic microscopy methods, produces image contrast, which is a function of the elastic...
Abstract
This article discusses the fundamentals and operating principles of the following acoustic microscopy methods: scanning laser acoustic microscopy, C-mode scanning acoustic microscopy, and scanning acoustic microscopy. It describes the applications of acoustic microscopy for detecting defects in metals, ceramics, glasses, polymers, and composites with examples.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006653
EISBN: 978-1-62708-213-6
... spectra to only that of the element of interest and the associated fill gas (i.e., neon or argon). Consequently, subsequent wavelength-isolation components (monochromator or interference filter) were only required to isolate the selected resonance transition wavelength. This is contrasted with high...
Abstract
This article focuses on some of the factors pertinent to atomic absorption spectroscopy (AAS). It begins by describing the working principle, critical components, and construction of flame atomic absorption instrumentation. This is followed by sections discussing various types of interferences in AAS, namely vaporization, ionization, matrix interferences, and background correction. Some of the methods for the analysis of microliter-sized samples and methods of standard additions to the sample solution for generating calibration standards are then reviewed. The article concludes with a section on processes involved in matrix matching.
Book Chapter
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006457
EISBN: 978-1-62708-190-0
..., some adhesives, such as AF-55 and FM-400, are x-ray opaque, which yields a much higher contrast among voids, porosity, and solid adhesive ( Fig. 16 ). Disbonds (separation between adhesive and adherend) are best detected by ultrasonic techniques. Fig. 16 Positive print from neutron radiograph...
Abstract
Adhesive-bonded joints are extensively used in aircraft components and assemblies where structural integrity is critical. This article addresses the problem of how to inspect bonded assemblies so that all discrepancies are identified. It describes several inspection techniques and presents drawbacks and limitations of these techniques. Generic flaw types and flaw-producing mechanisms are listed in a table. The article discusses metal-to-metal defects, adherend defects, honeycomb sandwich defects, repair defects, and in-service defects. It reviews the methods applicable to the inspection of bonded structures, including visual inspection, ultrasonic inspection, X-ray radiography, and neutron radiography. The evaluation and correlation of inspection results are also discussed. The article concludes with information on the effects of ultrasonic wave interference in the ultrasonic inspection of adhesive-bonded joints.
Book Chapter
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006671
EISBN: 978-1-62708-213-6
... microscopy, x-ray photoelectron spectroscopy, secondary ion mass spectroscopy, and ion-scattering spectroscopy can be used to show what is on or within the first few atomic layers of the surface. These techniques yield specific chemical bonding information and identify the elements present and, in contrast...
Abstract
The characterization, testing, and nondestructive evaluation of ceramics and glasses are vital to manufacturing control, property improvement, failure prevention, and quality assurance. This article provides a broad overview of characterization methods and their relationship to property control, both in the production and use of ceramics and glasses. Important aspects covered include the means for characterizing ceramics and glasses, the corresponding rationale behind them, and relationship of chemistry, phases, and microconstituents to engineering properties. The article also describes the effects that the structure of raw ceramic materials and green products and processing parameters have on the ultimate structure and properties of the processed piece. The effects that trace chemistry and processing parameters have on glass properties are discussed. The article describes mechanical tests and failure analysis techniques used for ceramics.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006764
EISBN: 978-1-62708-295-2
... available. Sometimes, a white coating is applied to the surface prior to conducting visible-particle tests (dry or wet) to enhance contrast and improve detection. Benefits and limitations of both types of particles/indications are similar to those for visible and fluorescent dye penetrants. The method can...
Abstract
Nondestructive testing (NDT), also known as nondestructive evaluation (NDE), includes various techniques to characterize materials without damage. This article focuses on the typical NDE techniques that may be considered when conducting a failure investigation. The article begins with discussion about the concept of the probability of detection (POD), on which the statistical reliability of crack detection is based. The coverage includes the various methods of surface inspection, including visual-examination tools, scanning technology in dimensional metrology, and the common methods of detecting surface discontinuities by magnetic-particle inspection, liquid penetrant inspection, and eddy-current testing. The major NDE methods for internal (volumetric) inspection in failure analysis also are described.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003232
EISBN: 978-1-62708-199-3
... ferrites (Ni x Fe 2 O 4 ), and some nickel alloys. Important particle characteristics include magnetic properties, size, shape, density, mobility, and degree of visibility and contrast. A mercury-vapor lamp is a convenient source of ultraviolet light, emitting a light...
Abstract
Magnetic-particle inspection is a nondestructive testing technique used to locate surface and subsurface discontinuities in ferromagnetic materials. Beginning with an overview of the applications, advantages, and limitations of magnetic-particle inspection, this article provides a detailed account of the portable power sources available for magnetization, and the different ways of generating magnetic fields using yokes, coils, central conductors, prod contacts, direct-contact, and induced current. In addition, the article discusses the characteristics and classification, and properties of magnetic particles and suspended liquids. Finally, the article outlines the types of discontinuities (surface and subsurface) that can be identified by magnetic-particle inspection and the importance of demagnetization after inspection.
Series: ASM Handbook
Volume: 2
Publisher: ASM International
Published: 01 January 1990
DOI: 10.31399/asm.hb.v02.9781627081627
EISBN: 978-1-62708-162-7
Book: Fractography
Series: ASM Handbook
Volume: 12
Publisher: ASM International
Published: 01 January 1987
DOI: 10.31399/asm.hb.v12.a0001834
EISBN: 978-1-62708-181-8
... rewarded with improved results and ease of correct interpretation. Errors in interpretation are made when specimens are not properly prepared. As-polished samples should be examined first with bright-field illumination and then with dark-filled illumination, differential interference contrast (DIC) or...
Abstract
This article presents examples of the visual fracture examination that illustrate the procedure as it applies to failure analysis and quality determination. It describes the techniques and procedures for the visual and light microscopic examination of fracture surfaces with illustrations. The article also describes microscopic and macroscopic features of the different fracture mechanisms with illustrations with emphasis on visual and light microscopy examination. The types of fractures considered include ductile fractures, tensile-test fractures, brittle fractures, fatigue fractures, and high-temperature fractures.