Plasma (ion) nitriding is a method of surface hardening using glow-discharge technology to introduce nascent (elemental) nitrogen to the surface of a metal part for subsequent diffusion into the material. This article describes the procedures and applications of plasma nitriding methods of steel. These methods include direct-current plasma nitriding, pulsed-current plasma nitriding, and active-screen plasma nitriding. The article reviews cold-walled and hot-walled furnaces used for plasma nitriding. It provides information on the importance of controlling three process parameters: atmosphere, pressure, and part temperature. The article includes a discussion on the influence of nitrogen concentration on case structure formation on nitrided steel, and explains the significance of microstructure, hardness, and fatigue strength on nitrided case. It also discusses processing, laboratory studies, and applications of nitrocarburizing of steel.

Laser-beam welding (LBW) uses a moving high-density coherent optical energy source, called laser, as the source of heat. This article discusses the advantages and limitations of LBW and tabulates energy consumption and efficiency of LBW relative to other selected welding processes. It provides information on the applications of microwelding with pulsed solid-state lasers. The article describes the modes of laser welding such as conduction-mode welding and deep-penetration-mode welding, as well as major independent process variables for laser welding, such as laser-beam power, laser-beam diameter, absorptivity, and traverse speed. It concludes with information on various hazards associated with LBW, including electrical hazards, eye hazards, and chemical hazards.

Laser-ultrasonics is a particular implementation of ultrasonic nondestructive inspection in which ultrasound is generated and detected by lasers. This article discusses the various mechanisms that ensure ultrasound generation and explains the possibility to get the equivalent of phase-array by numerical processing of an array of previously acquired laser-ultrasonic signals. The article describes the ultrasound generation by thermoelastic mechanism and ablation or vaporization. It illustrates the principle of optical detection of ultrasound with confocal Fabry-Perot interferometer and photorefractive two-wave mixing interferometer. The article concludes with information on the industrial applications of laser-ultrasonics, including thickness measurement, flaw detection, and material characterization.

The gas tungsten arc welding (GTAW) process derives the heat for welding from an electric arc established between a tungsten electrode and the part to be welded. This article provides a discussion on the basic operation principles, advantages, disadvantages, limitations, and applications of the process. It describes the equipment used for GTAW, namely, power supplies, torch construction and electrodes, shielding gases, and filler metals as well as the GTAW welding procedures. The article concludes with a review of the safety precautions to avoid possible hazards during the GTAW process: electrical shock, fumes and gases, arc radiation, and fire and explosion.

This article provides a detailed discussion on the heating equipment used for austenitizing, quenching, and tempering tool steels. These include salt bath furnaces, controlled atmosphere furnaces, fluidized-bed furnaces, and vacuum furnaces. The article discusses the types of nitriding and nitrocarburizing processes and the equipment required for heat treating tool steels to improve hardness, wear resistance, and thermal fatigue. The various nitriding and nitrocarburizing processes covered are salt bath nitrocarburizing, gas nitriding and nitrocarburizing, and plasma nitriding and nitrocarburizing.

The hazards associated with thermal spray deposition processes include ultraviolet and infrared radiation; acoustical noise; and by-product production in the forms of nitrous oxides, ozone, fumes, and dust. The most important consideration in health and safety is to use the engineered controls of hazards. This article provides a brief description of the spray booth, the most commonly used engineering tool to separate the operator from the thermal spray process and confine the associated hazards. It also presents guidelines on the proper and safe handling of industrial gases and ventilation and heat exhaust. The article provides information on the personal protective equipment for eyes and skin from radiation, and ears from noise. It also discusses other potential safety hazards associated with thermal spraying, namely, magnetic fields and infrasound.

Sputtering is a nonthermal vaporization process in which the surface atoms are physically ejected from a surface by momentum transfer from an energetic bombarding species of atomic/molecular size. It uses a glow discharge or an ion beam to generate a flux of ions incident on the target surface. This article provides an overview of the advantages and limitations of sputter deposition. It focuses on the most common sputtering techniques, namely, diode sputtering, radio-frequency sputtering, triode sputtering, magnetron sputtering, and unbalanced magnetron sputtering. The article discusses the fundamentals of plasma formation and the interactions on the target surface. A comparison of reactive and nonreactive sputtering is also provided. The article concludes with a discussion on the several methods of process control and the applications of sputtered films.

This article emphasizes the traits that are common to high-velocity forming operations. It describes general principles on how metal forming is accomplished and analyzed when inertial forces are large. The article discusses the principal methods of high-velocity forming, such as explosive forming, electrohydraulic forming, and electromagnetic forming. It provides examples that illustrate how these methods can be practically applied. The article concludes with information on the status and development potential for the technology.

Magnetically soft materials are characterized by their low coercivity, an essential requirement for irons and steels selected for any application involving electromagnetic induction cycling. This article provides information on ferromagnetic material properties and how they are affected by impurities, alloying additions, heat treatment, residual stress, and grain size. It also describes classification and testing methods for magnetically soft materials such as high-purity iron, low-carbon steels, silicon steels, iron-aluminum alloys, nickel-iron alloys, iron-cobalt alloys, ferrites, and stainless steels. The article also addresses corrosion resistance and provides insights on the selection of alloys for power generation applications, including motors, generators, and transformers. A short note on the design and fabrication of magnetic cores is also included.

Coatings and other surface modifications are used for a variety of functional, economic, and aesthetic purposes. Two major applications of thermal spray coatings are for wear resistance and corrosion resistance. This article discusses thermal (surface hardening) and thermochemical (carburizing, nitriding, and boriding) surface modifications, electrochemical treatments (electroplating, and anodizing), chemical treatments (electroless plating, phosphating, and hot dip coating), hardfacing, and thermal spray processes. It provides information on chemical and physical vapor deposition techniques such as conventional CVD, laser-assisted CVD, cathodic arc deposition, molecular beam epitaxy, ion plating, and sputtering.

This article discusses the basic principles of inductively coupled plasma mass spectrometry (ICP-MS), covering different instruments used for performing ICP-MS analysis. The instruments covered include the sample-introduction system, ICP ion source, mass analyzer, and ion detector. Emphasis is placed on ICP-MS applications in the semiconductor, photovoltaic, materials science, and other electronics and high-technology areas.

Adhesive-bonded joints are extensively used in aircraft components and assemblies where structural integrity is critical. This article addresses the problem of how to inspect bonded assemblies so that all discrepancies are identified. It describes several inspection techniques and presents drawbacks and limitations of these techniques. Generic flaw types and flaw-producing mechanisms are listed in a table. The article discusses metal-to-metal defects, adherend defects, honeycomb sandwich defects, repair defects, and in-service defects. It reviews the methods applicable to the inspection of bonded structures, including visual inspection, ultrasonic inspection, X-ray radiography, and neutron radiography. The evaluation and correlation of inspection results are also discussed. The article concludes with information on the effects of ultrasonic wave interference in the ultrasonic inspection of adhesive-bonded joints.

Projection welding is a variation of resistance welding in which current flow is concentrated at the point of contact with a local geometric extension of one (or both) of the parts being welded. This article focuses on the process fundamentals, advantages, and limitations of projection welding and reviews the equipment used in the process. It discusses projection welding of copper and copper alloys, aluminum and aluminum alloys, and steels. The article provides several specifications and recommended weld schedules and practices for projection welding. It describes the embossed-projection welding of heavy-, intermediate-, and thin-gage sheet mild steel as well as the welds between dissimilar thickness joints. The article also considers the solid-projection welding of steels: annular, nut, and cross-wire projection configurations. It also details the various tests that can be used to validate projection weld quality.

This article discusses the failure analysis of several steel transmission pipeline failures, describes the causes and characteristics of specific pipeline failure modes, and introduces pipeline failure prevention and integrity management practices and methodologies. In addition, it covers the use of transmission pipeline in North America, discusses the procedures in pipeline failure analysis investigation, and provides a brief background on the most commonly observed pipeline flaws and degradation mechanisms. A case study related to hydrogen cracking and a hard spot is also presented.

This article discusses the equipment design, procedures, experimental considerations, and interpretation of the torsion tests used to establish workability. It describes the application of torsion testing to obtain flow-stress data and to gage fracture-controlled workability and flow-localization-controlled failure. The article discusses the torsion test used to establish the processing parameters that are required to produce the desired microstructures.