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Image
Published: 01 January 1996
Fig. 9 Shapes of surface cracks, revealed by heat tinting before specimen fracture. The cracks were grown from (a) shallow and (b) deep notches
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Image
Published: 01 December 2004
Fig. 47 Zircaloy 4 as-cast ingot. Use of attack polishing, heat tinting (425 °C, or 800 °F), and differential interference contrast illumination reveals the basic crystal structure and the iron-chromium second phase. 200×. (P.E. Danielson)
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Image
Published: 01 January 1994
Fig. 3 Equipment for localized electrocleaning of heat tint from the surface of stainless steel. Source: Ref 5
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Image
Published: 01 December 2004
Fig. 51 Heat-tinted niobium alloy (C103) plate as viewed under differential interference contrast illumination. Some of the grains exhibit a second phase (note small, particle-like features) due to alloying additions. 65×. (P.E. Danielson)
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Image
Published: 01 December 2004
Fig. 62 Microstructure of as-cast Ti-6Al-4V heat tinted on a laboratory hot plate, and viewed with polarized light plus sensitive tint to reveal the coarse alpha-beta basketweave matrix structure. Magnification bar is 100 μm long.
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Image
in Metallography and Microstructures of Zirconium, Hafnium, and Their Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 3 Zircaloy 4 as-cast ingot. (a) Center section. Attack polished, heat tinted, etchant procedure No. 6, and viewed with differential interference contrast illumination. (b) Midthickness. Attack polished, heat tinted, and viewed with differential interference contrast illumination
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Image
in Metallography and Microstructures of Zirconium, Hafnium, and Their Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 5 Zircaloy 4 hot-worked plate, longitudinal. Attack polished, heat tinted, and viewed with polarized light illumination. This micrograph shows a hot-worked and annealed structure. Original magnification: 100×.
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Image
in Metallography and Microstructures of Zirconium, Hafnium, and Their Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 12 Zirconium crystal bar. Attack polished, heat tinted, and viewed with polarized light illumination. This micrograph shows large as-cast grains in zirconium crystal bar. Original magnification: 50×.
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Image
in Metallography and Microstructures of Zirconium, Hafnium, and Their Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 15 Zr702 plate, transverse. Attack polished, heat tinted, and viewed with polarized light illumination. These micrographs show an equiaxed alpha structure comparing the difference as viewed in (a) color and (b) monochromatic. Original magnification: 200×.
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Image
in Metallography and Microstructures of Zirconium, Hafnium, and Their Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 38 Zirconium sheet. (a) Attack polished, heat tinted, and viewed with polarized light illumination. (b) Attack polished, etchant procedure No. 2, anodized at 108 V, and viewed with bright-field illumination. These micrographs show the advantages certain preparation procedures offer
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Image
in Metallography and Microstructures of Zirconium, Hafnium, and Their Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 48 Hafnium crystal bar, longitudinal. Attack polished, heat tinted, and viewed with polarized light illumination. This micrograph shows the twinning in hafnium grains. Original magnification: 50×.
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Book Chapter
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003749
EISBN: 978-1-62708-177-1
... and describes several methods for film formation, namely, heat tinting, color etching, anodizing, potentiostatic etching, vapor deposition, and film deposition by sputtering. It provides information on the general procedures and precautions for etchants and reagents used in metallographic microetching...
Abstract
Metallographic contrasting methods include various electrochemical, optical, and physical etching techniques, which in turn are enhanced by the formation of a thin transparent film on the specimen surface. This article primarily discusses etching in conjunction with light microscopy and describes several methods for film formation, namely, heat tinting, color etching, anodizing, potentiostatic etching, vapor deposition, and film deposition by sputtering. It provides information on the general procedures and precautions for etchants and reagents used in metallographic microetching, macroetching, electropolishing, chemical polishing, and other similar operations.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003771
EISBN: 978-1-62708-177-1
... Abstract This article describes the metallurgy and microstructure of high-performance cobalt-base alloys. It discusses metallographic preparation procedures, including sectioning, mounting, grinding, polishing, etching, staining, and heat tinting. It examines the microstructure of cobalt alloys...
Abstract
This article describes the metallurgy and microstructure of high-performance cobalt-base alloys. It discusses metallographic preparation procedures, including sectioning, mounting, grinding, polishing, etching, staining, and heat tinting. It examines the microstructure of cobalt alloys in cast, wrought, and powder metal forms, including magnetic alloys as well as several cobalt-base superalloys.
Book Chapter
Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003622
EISBN: 978-1-62708-182-5
.... The effects of gas-tungsten arc weld shielding gas composition and heat-tint oxides on corrosion resistance are also discussed. The article explains microbiological corrosion of butt welds in water tanks with the examples. In addition, it provides information on corrosion of ferritic stainless steel weldments...
Abstract
This article reviews the metallurgical factors associated with welding. It provides a discussion on the preferential attack associated with weld metal precipitates in austenitic stainless steels. The article describes the corrosion associated with postweld and weld backing rings. The effects of gas-tungsten arc weld shielding gas composition and heat-tint oxides on corrosion resistance are also discussed. The article explains microbiological corrosion of butt welds in water tanks with the examples. In addition, it provides information on corrosion of ferritic stainless steel weldments and duplex stainless steel weldments.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003782
EISBN: 978-1-62708-177-1
... on zirconium alloy structures was that of Vogel and Tonn in 1931. The zirconium samples were prepared using an electropolishing process in nitric acid and subsequent heat tinting revealing a β-quenched structure in zirconium ( Ref 2 ). In 1948, Roth described a procedure involving mechanical polishing...
Abstract
Zirconium, hafnium, and their alloys are reactive metals used in a variety of nuclear and chemical processing applications. This article describes various specimen preparation procedures for these materials, including sectioning, mounting, grinding, polishing, and etching. It reviews some examples of the microstructure and examination for zircaloy alloys, hafnium, zirconium, and bimetallic forms.
Image
Published: 01 December 2004
Fig. 61 Microstructure of commercially pure titanium (ASTM F 67, grade 4) (transverse plane, specimen was annealed) heat tinted on a laboratory hot plate, and viewed with polarized light plus sensitive tint to reveal the grain structure.
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Image
Published: 01 June 2016
Fig. 1 Micrograph of an α alloy. Microstructure of commercially pure titanium, ASTM F67, grade 4 (transverse plane, specimen was annealed) prepared using the three-step method, heat tinted on a laboratory hot plate, and viewed with polarized light plus sensitive tint to reveal the grain
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Image
Published: 01 December 1998
) Austenitic AISI 304, welded. Structure: delta ferrite and austenite (dark). Heat tinted; 500×. (d) Duplex alloy, as cast and annealed. Structure: austenite and ferrite (dark). Tint etched; 200×
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Image
in Metallography and Microstructures of Zirconium, Hafnium, and Their Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 2 Zircaloy 4 welded sheet. (a) Parent metal. (b) Heat-affected zone. (c) Weld metal. Attack polished, heat tinted, and viewed with polarized light illumination. The parent metal is an equiaxed alpha structure, an acicular alpha heat-affected zone, with a Widmanstätten structure
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Image
in Metallography and Microstructures of Zirconium, Hafnium, and Their Alloys
> Metallography and Microstructures
Published: 01 December 2004
Fig. 33 Zr705 plate weld area, longitudinal. (a) Parent metal. (b) Heat-affected zone. (c) Weld metal, attack polished, heat tinted, polarized light. These micrographs show the appearance of the parent metal and weld zones. Original magnification: 1000×
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