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Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006770
EISBN: 978-1-62708-295-2
... on the operating principles and applications of detectors for x-ray spectroscopy, namely energy-dispersive spectrometers, wavelength-dispersive spectrometers, and handheld x-ray fluorescence systems. The processes involved in x-ray analysis in the SEM and handheld x-ray fluorescence analysis are then covered...
Abstract
X-ray spectroscopy is generally accepted as the most useful ancillary technique that can be added to any scanning electron microscope (SEM), even to the point of being considered a necessity by most operators. While “stand-alone” x-ray detection systems are used less frequently in failure analysis than the more exact instrumentation employed in SEMs, the technology is advancing and is worthy of note due to its capability for nondestructive analysis and application in the field. This article begins with information on the basis of the x-ray signal. This is followed by information on the operating principles and applications of detectors for x-ray spectroscopy, namely energy-dispersive spectrometers, wavelength-dispersive spectrometers, and handheld x-ray fluorescence systems. The processes involved in x-ray analysis in the SEM and handheld x-ray fluorescence analysis are then covered. The article ends with a discussion on the applications of x-ray spectroscopy in failure analysis.
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006459
EISBN: 978-1-62708-190-0
... of image conversion techniques allow the viewing of radiographic images while the testpiece is being irradiated and moved with respect to the radiation source and the radiation detector. Real-time radiography is a technique in which the x-rays cause fluorescence of a sensor, and that image is visually...
Abstract
Digital radiography is a technique that uses digital detector arrays (linear or area) to capture an X-ray photonic signal and convert it to an electronic signal for display on a computer. This article begins with an overview of real-time radiography and provides a schematic illustration of a typical radioscopic system using an X-ray image intensifier. It discusses the advantages and limitations of real-time radiography. Computed radiography (CR) is one of the radiography techniques that utilizes a reusable detector comprised of photostimuable luminescence (PSL) storage phosphor. The article provides a schematic illustration of a typical storage phosphor imaging plate. It concludes with a discussion on the benefits of digital radiography.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006645
EISBN: 978-1-62708-213-6
... Abstract This article provides a detailed account of X-ray spectroscopy used for elemental identification and determination. It begins with an overview of the operating principles of X-ray fluorescence (XRF) spectrometer, as well as a comparison of the operating principles of wavelength...
Abstract
This article provides a detailed account of X-ray spectroscopy used for elemental identification and determination. It begins with an overview of the operating principles of X-ray fluorescence (XRF) spectrometer, as well as a comparison of the operating principles of wavelength-dispersive spectrometer (WDS) and energy-dispersive spectrometer (EDS). This is followed by a discussion on the mechanism and effects of X-ray radiation, X-ray emission, and X-ray absorption. The article then discusses components used, operation, and applications of WDS and EDS. Some of the factors and processes involved in sample preparation for XRF analysis are also included. The article further provides information on the practical procedure for and the applications of WDS and EDS qualitative and quantitative analyses.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006759
EISBN: 978-1-62708-295-2
... maintenance, including assurance that adequate calibrations have been upheld. Methods such as x-ray fluorescence (XRF), arc or spark optical emission spectroscopy (OES), and inductively coupled plasma OES (ICP-OES) can be considered quantitative methods. To obtain optimal quantitative results, the sample...
Abstract
Chemical analysis is a critical part of any failure investigation. With the right planning and proper analytical equipment, a myriad of information can be obtained from a sample. This article presents a high-level introduction to techniques often used for chemical analysis during failure analysis. It describes the general considerations for bulk and microscale chemical analysis in failure analysis, the most effective techniques to use for organic or inorganic materials, and examples of using these techniques. The article discusses the processes involved in the chemical analysis of nonmetallics. Advances in chemical analysis methods for failure analysis are also covered.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006763
EISBN: 978-1-62708-295-2
... is digital photography. The digital camera is incorporated in the scanning electron microscope. X-ray spectroscopy image photography may also be used for the recording of x-ray images and maps. Fig. 30 Setup for scanning electron microscopic examination of exemplar fractured crankshaft Fig. 31...
Abstract
Failure analysis is an investigative process that uses visual observations of features present on a failed component fracture surface combined with component and environmental conditions to determine the root cause of a failure. The primary means of recording the conditions and features observed during a failure analysis investigation is photography. Failure analysis photographic imaging is a combination of both science and art; experience and proper imaging techniques are required to produce an accurate and meaningful fracture surface photograph. This article reviews photographic principles and techniques as applied to failure analysis, both in the field and in the laboratory. The discussion covers the processes involved in field and laboratory photographic documentations, provides a description of professional digital cameras, and gives information on photographic lighting and microscopic photography. Special techniques can be employed to deal with highly reflective conditions and are also described in this article.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003527
EISBN: 978-1-62708-180-1
... not benefit by color photography. The primary techniques of photography associated with scanning electron microscopy are digital photography and instant film photography. X-ray imaging spectroscopy associated with scanning electron microscopy typically uses digital photography for the recording of x-ray...
Abstract
This article reviews photographic principles, namely, visual examination, field photographic documentation, and laboratory photographic documentation, as applied to failure analysis and the specific techniques employed in both the field and laboratory. It provides information on the photographic equipment used in failure analysis and on film and digital photography. The article describes the basics of photography and the uses of different types of lighting in photography of a fractured surface. The article also addresses the techniques involved in macrophotography and microscopic photography as well as other special techniques.
Book Chapter
Series: ASM Handbook
Volume: 23A
Publisher: ASM International
Published: 12 September 2022
DOI: 10.31399/asm.hb.v23A.a0006890
EISBN: 978-1-62708-392-8
.... They are usually inexpensive and provide low accuracy. On the other hand, active devices emit radiation, which can be visible by light, x-ray, or ultrasound, and they detect the reflection or radiation passing through an object ( Ref 49 – 57 ). Optical Noncontact Devices A commonly used optical passive...
Abstract
Bioprinting has been advancing in the field of tissue engineering as the process for fabricating scaffolds, making use of additive manufacturing technologies. In situ bioprinting (also termed intraoperative bioprinting) is a promising solution to address the limitations of conventional bioprinting approaches. This article discusses the main approaches and technologies for in situ bioprinting. It provides a brief overview of the bioprinting pipeline, highlighting possible solutions to improve currently used approaches. Additionally, case studies of in situ bioprinting are provided and in situ bioprinting future perspectives are discussed.
Book: Fractography
Series: ASM Handbook
Volume: 12
Publisher: ASM International
Published: 01 June 2024
DOI: 10.31399/asm.hb.v12.a0006845
EISBN: 978-1-62708-387-4
..., including scanning electron microscope fractography, energy-dispersive x-ray spectroscopy of the deposit, and metallographic examination, were clearly indicated by the initial fractographic results. These additional analyses indicated an intergranular fracture covered by a tenacious oxide scale, which...
Abstract
Fracture surfaces can provide an important and indispensable record of many factors in simple or complex failures. Visual examination of fracture surfaces can reveal the type and direction of loading, with fracture-surface features often providing definitive evidence of torsion, tension, bending, and compressive loads. This article discusses tools and techniques of visual examination and characteristic features of fracture features. A brief review of ductile and brittle fracture-surface features is provided. The article also describes macroscopic features that can be used to identify fracture-initiation sites, locations of final overload, and the directions of crack propagation. In addition, the use of these features to characterize loading at the time of failure is also described.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.9781627082136
EISBN: 978-1-62708-213-6
Book: Fractography
Series: ASM Handbook
Volume: 12
Publisher: ASM International
Published: 01 June 2024
DOI: 10.31399/asm.hb.v12.a0006945
EISBN: 978-1-62708-387-4
... contrast DNG digital negative DOF depth of field DPI dots per inch DSLR digital single-lens reflex camera dual-beam SEM SEM with ion guns for milling, plating, and imaging EBSD electron backscattered diffraction EDX energy-dispersive x-ray analysis EPS Encapsulated...
Abstract
This article presents a basic overview of technology-driven advances in the imaging of primarily metallic fracture surfaces. It describes various types of microscopes, including scanning electron, dual-beam, ion source, and transmission electron microscopes, and their capabilities. It also covers other useful hardware, such as computer-aided tomography (CAT) and micro-computer-aided tomography (micro-CAT) instruments. The article introduces some of the fracture image postprocessing methods and software, including image registration or alignment, focus stacking, Z-stacking, focal plane merging, and image stitching.
Book Chapter
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003524
EISBN: 978-1-62708-180-1
... of electromagnetic inspection include: Depth of penetration is shallow. Materials to be inspected must be electrically conductive. Indications are influenced by more than one variable. Reference standards are required. Residual Stress Analysis X-ray diffraction is the most common method...
Abstract
This article describes the preliminary stages and general procedures, techniques, and precautions employed in the investigation and analysis of metallurgical failures that occur in service. The most common causes of failure characteristics are described for fracture, corrosion, and wear failures. The article provides information on the synthesis and interpretation of results from the investigation. Finally, it presents key guidelines for conducting a failure analysis.
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006449
EISBN: 978-1-62708-190-0
... or no interest that affect instrument indications to a greater degree than variables of interest present an obstacle to the process. One of the most common nondestructive methods used to verify chemical composition is portable x-ray fluorescence spectrometry. However, this method is not discussed in this article...
Abstract
This article provides information on the application of nondestructive examination (NDE) technologies to tube and pipe products. These include modeling and simulation methods, eddy-current methods, magnetic methods, acoustic methods, and physical methods. A summary of nondestructive examination methods based on flaw type and product stage is presented in a table. The article also discusses in-service inspection of tubular products and presents an example that illustrates the importance of nondestructive testing (NDT) for welds in austenitic stainless steel tubing.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006822
EISBN: 978-1-62708-329-4
... the chemical composition of surface residue. Various techniques may be used, including energy-dispersive spectroscopy, x-ray diffraction, or gas chromatography/mass spectrometry. Where microbiologically influenced corrosion is suspected as a possible cause or contributor to a failure, deposit samples should...
Abstract
This article discusses the failure analysis of several steel transmission pipeline failures, describes the causes and characteristics of specific pipeline failure modes, and introduces pipeline failure prevention and integrity management practices and methodologies. In addition, it covers the use of transmission pipeline in North America, discusses the procedures in pipeline failure analysis investigation, and provides a brief background on the most commonly observed pipeline flaws and degradation mechanisms. A case study related to hydrogen cracking and a hard spot is also presented.
Series: ASM Handbook
Volume: 18
Publisher: ASM International
Published: 31 December 2017
DOI: 10.31399/asm.hb.v18.a0006360
EISBN: 978-1-62708-192-4
... . This technique is destructive like the Daimler-Benz adhesion test but is highly accurate. Results can be verified by scanning electron microscopy (SEM) or transmission electron microscopy (TEM) of cross-section samples of the coated surface. Coating thickness can also be measured using x-ray fluorescence (XRF...
Abstract
This article describes two variations of carbon-base coatings: diamondlike carbon (DLC) coatings and polycrystalline diamond (PCD) coatings. It discusses the basics of a few deposition methods as they apply to industrially relevant coatings. The methods include deposition of tungsten-containing hydrogenated amorphous carbon films, deposition of tetrahedral amorphous carbon films, and deposition of silicon-incorporated hydrogenated amorphous carbon films. The most common deposition technologies for diamond films are also discussed. The article provides information on surface preparation for DLC and diamond deposition. It also provides a discussion on the coating composition and structure, mechanical and tribological properties, and applications of DLC and diamond coatings. The quality control techniques for DLC and diamond coatings are specified to meet customer requirements and ensure repeatable quality.
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006788
EISBN: 978-1-62708-295-2
... surface deposits using techniques such as x-ray diffraction (XRD), energy-dispersive x-ray analysis (EDX), and x-ray fluorescence (XRF) to discover corrosion products or even oxidants such as MnO 2 or elemental sulfur that can be matched to a known corrosion scenario. The turnaround time for this work...
Abstract
This article focuses on the mechanisms of microbiologically influenced corrosion as a basis for discussion on the diagnosis, management, and prevention of biological corrosion failures in piping, tanks, heat exchangers, and cooling towers. It begins with an overview of the scope of microbial activity and the corrosion process. Then, various mechanisms that influence corrosion in microorganisms are discussed. The focus is on the incremental activities needed to assess the role played by microorganisms, if any, in the overall scenario. The article presents a case study that illustrates opportunities to improve operating processes and procedures related to the management of system integrity. Industry experience with corrosion-resistant alloys of steel, copper, and aluminum is reviewed. The article ends with a discussion on monitoring and preventing microbiologically influenced corrosion failures.
Series: ASM Handbook
Volume: 4C
Publisher: ASM International
Published: 09 June 2014
DOI: 10.31399/asm.hb.v04c.a0005858
EISBN: 978-1-62708-167-2
... an atom or molecule and break the intra- and intermolecular links, unlike cosmic rays and x-rays or γ rays emitted by radioactive substances. Near Field and Far Field When the distance between the source and the exposed person is less than 1.6 times the wavelength, this person is in a zone called...
Abstract
This article provides an overview of electromagnetic fields (EMFs) and discusses their direct and indirect effects on human health. It provides a detailed description of the exposure levels of EMFs in residential and work environments. The article examines the international and European standards and regulations regarding occupational exposure to EMFs encountered in industrial activities. It discusses the categories of work equipment or activities that may expose the worker above and under the orientation value. The article also describes the main principles underlying the protection system adopted for the frequency range of 50 Hz to 10 MHz.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.9781627083294
EISBN: 978-1-62708-329-4
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.9781627081993
EISBN: 978-1-62708-199-3