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Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0003314
EISBN: 978-1-62708-176-4
... fatigue testing machines and bending fatigue machines. Load cells, grips and alignment devices, extensometry and strain measuring devices, environmental chambers, graphic recorders, furnaces, and heating systems of ancillary equipment are discussed. The article presents technologies available...
Abstract
This article describes the phenomena of crack initiation and early growth. It examines specimen design and preparation as well as the apparatus used in crack initiation testing. The article provides descriptions of the various commercially available fatigue testing machines: axial fatigue testing machines and bending fatigue machines. Load cells, grips and alignment devices, extensometry and strain measuring devices, environmental chambers, graphic recorders, furnaces, and heating systems of ancillary equipment are discussed. The article presents technologies available to accomplish closed loop control of materials testing systems in performing standard materials tests and for the development of custom testing applications. It explores the advanced software tools for materials testing. The article includes a description of baseline isothermal fatigue testing, creep-fatigue interaction, and thermomechanical fatigue. The effects of various variables on fatigue resistance and guidelines for fatigue testing are also presented.
Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005931
EISBN: 978-1-62708-166-5
... systems must be able to adjust the flow of gases for process optimization. The operator interface of a furnace-control system displays critical information such as the furnace temperature, atmosphere status, alarms, electronic chart recorders, recipe, and maintenance. A supervisory control and data...
Abstract
Heat treating furnaces require different control systems and integration for achieving optimum technical results and enabling safe operation. This article focuses on atmosphere furnaces, with some coverage on controls for vacuum furnaces. Heat treating operations require reliable monitoring and control of motion and position of various mechanical components with the help of mechanical limit switches, proximity sensors, and distance- and position-measuring devices. Using inputs from both flow meters and sensors, such as thermocouples and oxygen sensors, flow measurement control systems must be able to adjust the flow of gases for process optimization. The operator interface of a furnace-control system displays critical information such as the furnace temperature, atmosphere status, alarms, electronic chart recorders, recipe, and maintenance. A supervisory control and data-acquisition (SCADA) system is used to monitor, collect, and store data from multiple pieces of equipment.
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005217
EISBN: 978-1-62708-187-0
... of the analysis sample differs from that of the standard sample. The temperature difference between the analysis sample and the standard sample is recorded at the same time the furnace temperature is recorded. Fig. 5 Schematic of principal setup for differential thermal analysis equipment. T n...
Abstract
Thermal analysis is a classical method of determining phase diagrams and can be used to analyze the deviation from solidification under equilibrium conditions. This article discusses the use of thermal analysis in industrial processes and in research. It describes the theoretical basis of simplified and differential thermal analysis. Techniques for determining liquidus and solidus temperatures using cooling curves are also discussed.
Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005925
EISBN: 978-1-62708-166-5
... K element up to 200 °C (400 °F), suitable for a heat treating area, and is strong enough for pulling through a conduit. Type K or N should be used for all the furnace measurements to maintain uniformity, that is, recording and control of furnace temperatures, plus the high limit safety control...
Abstract
Temperature control in heat treating is of paramount importance in maintaining the quality and achieving the desired metallurgical results. This article provides a detailed account of the factors affecting temperature control in heat treating furnaces, with information on temperature control systems, including contact sensors, noncontact sensors, controllers, energy-flow regulators, measurement instruments, and set-point programmers. Common contact sensors include temperature scales, thermocouples, and resistance temperature detectors, whereas optical pyrometers and on-line radiation thermometers fall under the noncontact type. The article describes two types of instrumentation used in heat treating: field test instruments for temperature-uniformity surveys and system-accuracy tests; and controlling, monitoring, and recording instruments for digital instrumentation.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005788
EISBN: 978-1-62708-165-8
... Abstract Inverse hardening a steel of adequate hardenability requires a workpiece of sufficiently large cross section, an appropriate cooling medium, and the right quenching conditions. This article explains the Temperature Gradient Quenching Analysis System (TGQAS), which can measure, record...
Abstract
Inverse hardening a steel of adequate hardenability requires a workpiece of sufficiently large cross section, an appropriate cooling medium, and the right quenching conditions. This article explains the Temperature Gradient Quenching Analysis System (TGQAS), which can measure, record, and evaluate all quenching processes in common use, describing their heat extraction dynamics by corresponding thermodynamic functions. It discusses the metallurgical aspects of steels with an emphasis on two different processes, namely, heat extraction (a thermodynamic process) and microstructural transformation (a metallurgical process) that are initiated at the moment when the austenitized workpiece is immersed in the quenchant. The article describes the uses of polyalkylene glycol copolymer and the effect of hardness and fatigue resistance on AISI 4140 type steel.
Series: ASM Handbook
Volume: 1A
Publisher: ASM International
Published: 31 August 2017
DOI: 10.31399/asm.hb.v01a.a0006330
EISBN: 978-1-62708-179-5
... with a furnace. It provides a discussion on the dilatometer analysis that is generally used to measure linear displacement as a function of temperature for all types of materials, and the problems associated with volume-change measurements. The article presents a graphical representation of a consequence...
Abstract
Solidification of cast iron alloys brings about volumetric changes. This article describes direct measurements of volume changes with an illustration of the analysis of volumetric changes during solidification of cast iron with the use of a specially designed riser combined with a furnace. It provides a discussion on the dilatometer analysis that is generally used to measure linear displacement as a function of temperature for all types of materials, and the problems associated with volume-change measurements. The article presents a graphical representation of a consequence of the anisotropy, where the calculated volume change is illustrated as a function of temperature. It concludes with a review of kinetic of graphite expansion.
Series: ASM Handbook
Volume: 14A
Publisher: ASM International
Published: 01 January 2005
DOI: 10.31399/asm.hb.v14a.a0003989
EISBN: 978-1-62708-185-6
... An economical technique to convert a cast structure to a wrought structure is through the use of open-die forging and furnace treatments, collectively known as cogging. Traditionally, the forging elements of cogging have been carried out by using a two-die forge, but cogging can also include work done...
Abstract
This article describes the presses, transportation equipment, and manufacturing processes associated with cogging. It discusses the practical and metallurgical issues encountered during the conversion of ingot to billet. The article explains the use of numerical modeling as part of the continuing efforts to reduce the cost and time associated with developing new cogging sequences, increase the yield, make the processes more robust, and increase the quality of the produced product.
Series: ASM Handbook
Volume: 4C
Publisher: ASM International
Published: 09 June 2014
DOI: 10.31399/asm.hb.v04c.a0005904
EISBN: 978-1-62708-167-2
... Abstract The crucible induction furnace is growing as an alternative melting unit to the cupola furnace due to its low specific power and reduced power consumption during solid melting material. This article details the process engineering features of the crucible induction furnace...
Abstract
The crucible induction furnace is growing as an alternative melting unit to the cupola furnace due to its low specific power and reduced power consumption during solid melting material. This article details the process engineering features of the crucible induction furnace. It discusses the various processes involved in melting, holding, and pouring of liquid melt in crucible induction furnaces wherein the holding operation is carried out in channel furnace and pouring operation in pressure-actuated pouring furnaces. The article examines the behavior of furnace refractory lining to defects such as erosion, infiltration, crack formation, and clogging, and the corresponding preventive measures to avoid the occurrence of these defects. It elucidates the overall furnace operations, including commissioning, operational procedures, automatic process monitoring, inductor change, and dealing with disturbances.
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003520
EISBN: 978-1-62708-180-1
..., or sketches of the failure and adjacent areas Any service deviations that might have contributed to the failure Opinions of operating personnel regarding the failure The investigator should carefully study available blueprints and other graphic records to obtain a comprehensive picture...
Abstract
This article outlines the basic steps to be followed and the range of techniques available for failure analysis, namely, background data assembling, visual examination, microfractography, chemical analysis, metallographic examination, electron microscopy, electron microprobe analysis, X-ray techniques, and simulations. It also describes the steps for analyzing the data, preparing the report, preservation of evidence, and follow-up on recommendations.
Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005955
EISBN: 978-1-62708-166-5
... designs. Insulated Designs Insulated designs resemble the wall of a conventional low-temperature furnace and are well known for their efficiency. One or more layers of graphite felt or high-temperature refractory fiberfill or ceramic fiber are placed between the inner molybdenum or graphic foil...
Abstract
Vacuum heat treating consists of thermally treating metals and alloys in cylindrical steel chambers that have been pumped down to less than normal atmospheric pressure. This article provides a detailed account of the operations and designs of vacuum furnaces, discussing their pressure levels, resistance heating elements, quenching systems, work load support, pumping systems, and temperature control systems. It describes the classification of instruments used for measuring and recording pressure inside a vacuum processing chamber. Common devices include hydrostatic measuring devices and devices for measuring thermal and electrical conductivity. The article also describes the applications of the vacuum heat treating process, namely, vacuum nitriding and vacuum carburizing. Finally, it reviews the heat treating process of tool steels, stainless steels, Inconel 718, and titanium and its alloys.
Series: ASM Handbook
Volume: 22B
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.hb.v22b.a0005529
EISBN: 978-1-62708-197-9
... heated Allcase (Surface Combustion, Inc.) furnace. The material was loaded in a round stainless steel drum measuring 267 mm in diameter by 298 mm high. Thermocouples were buried at various points in the load, and the temperatures were recorded against time. The locations of the thermocouples are shown...
Abstract
This article provides information on the heat-source model, conduction heat-transfer model of parts and fixtures, and the radiation heat-transfer and convection heat-transfer models in a furnace. It describes the two types of furnaces used for heat treating: batch furnaces and continuous furnaces. The heating methods, such as direct-fired heating, radiant-tube heating, and electrical heating, are also discussed. Furnace temperature control is essential to ensure quality heat treatment. The article explains the operating procedure of the automatic temperature controllers used in most furnace operations. Heating simulations can be validated by comparison with measured results in full-scale furnaces. The article also presents several case studies to illustrate the use of the simulations.
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001778
EISBN: 978-1-62708-178-8
... at different rates, and the anions will be separated into distinct bands moving through and out of the column. With the proper selection of eluent solution and resin, the emerging bands of ions are very narrow and well resolved from each other. By providing a means for detecting the bands, they can be recorded...
Abstract
Ion chromatography (IC) is an analytical technique that uses columns packed with ion exchange resins to separate ions in aqueous solutions and dynamically elute them to a detector. This article provides information on the different modes of detection, namely, eluent-suppressed conductivity detection, single-column ion chromatography with conductivity detection, ion chromatography with spectrophotometric detection, and amperometric electrochemical detection. It describes the modes of separation techniques in IC and reversed-phase IC. The article discusses the detection capabilities of IC, the procedures for preparing solid and liquid samples, as well as the applications of IC.
Series: ASM Handbook
Volume: 22B
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.hb.v22b.a0005544
EISBN: 978-1-62708-197-9
.../inclusion detection, crack segmentation, material distribution in composite materials, and component assembly analysis. Volume Graphics GmbH http://www.volumegraphics.com/products/vgstudiomax VTK VTK (Visualization Toolkit) is an open-source software system for three-dimensional computer graphics...
Abstract
This article demonstrates the depth and breadth of commercial and third-party software packages available to simulate metals processes. It provides a representation of the spectrum of applications from simulation of atomic-level effects to manufacturing optimization. The article tabulates the software name, function or process applications, vendor or developer, and website information.
Book Chapter
Series: ASM Handbook
Volume: 1A
Publisher: ASM International
Published: 31 August 2017
DOI: 10.31399/asm.hb.v01a.a0006337
EISBN: 978-1-62708-179-5
... Abstract Various types of furnaces have been used for cast iron melting. In terms of tonnage, the primary melting methods used by iron casting facilities are cupola and induction furnaces. This article describes the operation and control principles of cupola furnace. It discusses the advantages...
Abstract
Various types of furnaces have been used for cast iron melting. In terms of tonnage, the primary melting methods used by iron casting facilities are cupola and induction furnaces. This article describes the operation and control principles of cupola furnace. It discusses the advantages of specialized cupolas such as cokeless cupola and plasma-fired cupola. Melting in iron foundries is a major application of induction furnaces. The article describes the operations of two induction furnaces: the channel induction furnace and the induction crucible furnace. It explains the teapot principle of pressure-actuated pouring furnaces and provides information on the effect of pouring magnesium-treated melts.
Series: ASM Handbook
Volume: 4C
Publisher: ASM International
Published: 09 June 2014
DOI: 10.31399/asm.hb.v04c.a0005853
EISBN: 978-1-62708-167-2
... of the induction process, are also addressed. calibration induction brazing induction heating induction melting infrared sensors quality control thermal imagers two-color infrared thermometers vacuum furnaces INDUCTION HEATING is used to heat parts for forging, annealing, heat treating, welding...
Abstract
This article provides an overview of the basic theory of infrared (IR), including emissivity and E slope. It explains how the IR thermometer works, and provides guidance on choosing a thermometer, in particular, deciding between a two-color and a single-wavelength thermometer and installing and maintaining them. The article discusses typical applications of induction heating, and describes how the IR thermometer controls the temperature. While the majority of the article discusses spot thermometers, thermal imagers, which are fast and are used for both research and control of the induction process, are also addressed.
Book Chapter
Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0003288
EISBN: 978-1-62708-176-4
... is also included on most test stands. During creep tests, the time must be recorded with the creep values. Furnaces Furnaces used in creep and stress-rupture testing generally are tubular, with an electrical-resistance winding that heats the test specimen through radiation in an air atmosphere...
Abstract
This article reviews the basic equipment and methods for creep and creep rupture testing. It begins with a discussion on the creep properties, including stress and temperature dependence, as well as of the extrapolation techniques that permit estimation of the long-term creep and rupture strengths of materials. The article describes the different types of equipment for determination of creep characteristics, including test stands, furnaces, and extensometers. It also discusses the different testing methods for creep rupture: constant-load testing and constant-stress testing. The article presents other testing considerations and concludes with information on stress relaxation testing.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006644
EISBN: 978-1-62708-213-6
... crystal was recorded as early as 1931 by Berg ( Ref 1 ) and later by Barrett ( Ref 2 ), developing the technique commonly known as Berg-Barrett reflection topography, which is used to study large-sized crystals. Subsequently, the x-ray topography technique was developed to image and characterize defects...
Abstract
X-ray topography is the general term for a family of x-ray diffraction imaging techniques capable of providing information on the nature and distribution of imperfections. This article provides a detailed account of x-ray topography techniques, providing information on the historical background and development trends in x-ray diffraction topography. The discussion covers the general principles, components of systems, and applications of x-ray topography techniques, namely conventional X-ray topographic techniques and synchrotron x-ray topographic techniques.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005806
EISBN: 978-1-62708-165-8
... nitrocarburizing and austenitic nitrocarburizing. The article includes a discussion on the difficulties in specimen cleaning, importance of furnace purge, uses of pre and post oxidation, depassivation, or activation, and requirements for perfect nucleation in nitriding process. In nitriding, the successful...
Abstract
This article summarizes the terminology for gas reactions, and discusses low-temperature nitriding and nitrocarburizing of stainless steels. It describes the various nitriding processes, namely, high- and low-pressure nitriding, oxynitriding, sulfonitriding, oxysulfonitriding, ferritic nitrocarburizing and austenitic nitrocarburizing. The article includes a discussion on the difficulties in specimen cleaning, importance of furnace purge, uses of pre and post oxidation, depassivation, or activation, and requirements for perfect nucleation in nitriding process. In nitriding, the successful atmosphere control depends on various potentials. The article summarizes the methods of measuring potentials in nitriding and nitrocarburizing, provides useful information on the furnaces used, and the safety precautions to be followed in the nitriding process. It also describes the sample preparation procedures and testing methods to ensure the quality of the sample.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006667
EISBN: 978-1-62708-213-6
..., but is outside the scope of this article. Fig. 2 Graphical display of the neutron bound coherent scattering length for the naturally occurring elemental abundances. Not captured in this plot is the fact that 3 He, 10 B, and some rare earth isotopes from the elements cadmium, samarium, gadolinium...
Abstract
This article provides a brief introduction to neutron diffraction as well as its state-of-the-art capabilities. The discussion covers the general principles of the neutron, neutron-scattering theory, generation of neutrons, types of incident radiation, and purposes of single-crystal neutron diffraction, powder diffraction, and pair distribution function analysis. The relationship between detector space and reciprocal space are presented. Various factors involved in sample preparation, calibration, and techniques used for analyzing diffraction data are described. The article also presents application examples and possible future developments in neutron diffraction.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003760
EISBN: 978-1-62708-177-1
... to reduce the time required for sectioning. Material can also be removed semiautomatically or automatically using focused ion beam ( Ref 6 ) techniques. Going to the extreme, the 3D atom probe has been used to strip individual atoms from a specimen, while recording the atomic position and species ( Ref 7...
Abstract
Three-dimensional microscopy can be used to reveal the shape, distribution, and connectivity of three-dimensional (3D) features that lie buried within an opaque material. This article discusses several experimental techniques that can be used to generate 3D images. These include serial sectioning, focused ion beam tomography, atom probe tomography, and X-ray microtomography. Nine case studies are presented that represent the work of the various research groups currently working on 3D microscopy using serial sectioning and illustrate the variants of the basic experimental techniques. The article also discusses the techniques for reconstruction and visualization of 3D microstructures with advanced computer software and hardware.
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