The article provides an overview of the various types of testing machines: gear-driven or screw-driven machines and servohydraulic machines. It examines force application systems, force measurement, and strain measurement. The article discusses important instrument considerations and describes gripping techniques of test specimens. It analyzes test diagnostics and reviews the use of computers for gathering and reducing data. Emphasis is placed on universal testing machines with separate discussions of equipment factors for tensile testing and compressing testing. The influence of the machine stiffness on the test results is also described, along with a general assessment of test accuracy, precision, and repeatability of modern equipment.

This article focuses on coatings and overlays adopted for use as wear- and corrosion-resistant materials in oil sand processing. It describes the most common application processes for oil sand coatings and overlays, including welding, high-velocity oxyfuel thermal spray, laser cladding, and vacuum brazing. The article provides information on the selection of overlays and materials such as chromium-carbide-base overlays and tungsten carbide metal-matrix composites.

This article discusses the methods for assessing creep-rupture properties, particularly, nonclassical creep behavior. The determination of creep-rupture behavior under the conditions of intended service requires extrapolation and/or interpolation of raw data. The article describes the various techniques employed for data handling of most materials and applications of engineering interest. These techniques include graphical methods, methods using time-temperature parameters, and methods used for estimations when data are sparse or hard to obtain. The article reviews the estimation of required creep-rupture properties based on insufficient data. Methods for evaluation of remaining creep-rupture life, including parametric modeling, isostress testing, accelerated creep testing, evaluation by the Monkman-Grant coordinates, and the Materials Properties Council (MPC) Omega method, are also reviewed.

This article focuses on the ceramic coatings for ceramic and glass substrates. It describes the role of oxides in glazes and discusses the optical and appearance properties of various types of glazes, such as leadless glazes, lead-containing glazes, opaque glazes, and satin and matte glazes. The article provides information on the classification of pigments and the applications of ceramic coatings for decorations on ceramic and glass surfaces.

This article presents typical problems encountered in the analysis of experimental creep and creep-rupture data and the possible solutions to these drawbacks. It provides information on planning the test and creep strain/time relationships. The exponential creep equation and the rational polynomial creep equation are discussed. The article also describes the dependence of stress and temperature on equation parameters and explains the lot-centered regression analysis.

Compacted graphite iron (CGI) invariably includes some nodular (spheroidal) graphite particles, giving rise to the definition of the microstructure in terms of percent nodularity. This article discusses the graphite morphology and mechanical and physical properties of CGI. The mechanical and physical properties of CGI with ferritic and pearlitic matrix structures are summarized in a table. The article describes the standards for CGI, with the definition of the grades based on the minimum tensile strength. It also provides information on the applications of compacted graphite iron castings.

Corrosion fatigue refers to the phenomenon of cracking in materials under the combined actions of fatigue loading and a corrosive environment. This article focuses on the various mechanisms of corrosion fatigue, namely, hydrogen-assisted cracking, anodic dissolution, and surface energy reduction. It discusses the variables affecting corrosion fatigue. The effect of fatigue load frequency, environment, grain size, stress ratio, waveform, and temperature fatigue crack growth are also discussed.

This article describes the chemistry of phenolic resins and reviews their characteristics and properties for various composites fabrication processes. The fabrication processes include solution/hot-melt process, pultrusion, vacuum infusion, filament winding, sheet molding, and hand lay-up. The article illustrates the manufacturing process of phenolic honeycomb and provides information on the applications of phenolic composites.

This article reviews the basic mechanisms of elevated-temperature behavior and associated design considerations, with an emphasis on metals. It discusses the key concepts of elevated-temperature design. These include plastic instability at elevated temperatures; deformation mechanisms and strain components associated with creep processes; stress and temperature dependence; fracture at elevated temperatures; and environmental effects. The article describes the basic presentation and analysis methods for creep rupture. It provides information on the application of these methods to materials selection and the setting of basic design rules. The article examines the limitations of high-temperature components as well as the alternative design approaches and tests for most high-temperature components.

Scanning electron microscopy (SEM) has unique capabilities for analyzing fracture surfaces. This article discusses the basic principles and practice of SEM, with an emphasis on its applications in fractography. The topics include an introduction to SEM instrumentation, imaging and analytical capabilities, specimen preparation, and the interpretation of fracture features. SEM can be subdivided into four systems, namely, illuminating/imaging, information, display, and vacuum systems. The article also describes the major criteria and techniques of SEM specimen preparation, and the general features of ductile and brittle fracture modes.

Archaeometallurgists use metallography to reveal and interpret the microstructures of objects, in conjunction with the results of their chemical analyses and microanalyses. This article describes a number of special problems that occur while performing metallographic analyses on archaeological materials. It also presents case studies, with examples that illustrate situations where metallography has contributed to archaeometallurgical studies.

Neutron activation analysis (NAA) is a highly sensitive and accurate method of assaying bulk materials for trace levels of many elements. This article provides a detailed account on several types of NAA, namely, nondestructive and radiochemical thermal neutron activation, delayed neutron counting, epithermal and 14-MeV fast neutron activation, and prompt gamma activation analysis. It also includes application examples, explaining where and how each method is used and the types of elements on which they are effective.

Thermal analysis provides a powerful tool for researchers and engineers in determining both unknown and reproducible behavioral properties of polymer molecules. This article covers the thermal analysis and thermal properties of engineering plastics with respect to chemical composition, chain configuration, conformation of the base polymers, processing of the base polymers with or without additives; and the response to chemical, physical, and mechanical stresses of base polymers as unfilled, shaped articles or as components of composite structures. It also describes thermal analysis techniques, including differential scanning calorimetry, thermogravimetric analysis, thermomechanical analysis, and rheological analysis. This article also summarizes the basic thermal properties used in the application of engineering plastics, such as thermal conductivity, temperature resistance, thermal expansion, specific heat, and the determination of glass transition temperatures. It concludes with a discussion of the thermal and related properties of nine thermostat resin systems divided into three groups by low, medium, and high service temperature capabilities.

This article provides a detailed account of the concepts and applications of neutron activation analysis (NAA), covering the basic principles and neutron reactions of NAA as well as calibration methods used for NAA. The discussion also covers the factors pertinent to analytical sensitivity achievable with NAA, common neutron sources, sample-handling technique, and automated systems of NAA. The categories of NAA covered are instrumental neutron activation analysis, epithermal neutron activation analysis, radiochemical neutron activation analysis, 14 MeV fast neutron activation analysis, delayed neutron activation analysis, and prompt gamma activation analysis.

Corrosion, fatigue, and their synergistic interactions are among the principal causes of damage to aircraft structures. This article describes aircraft corrosion fatigue assessment in the context of different approaches used to manage aircraft structural integrity, schedule aircraft inspection intervals, and perform repair and maintenance of aircraft in service. It illustrates the types of corrosive attack observed in aircraft structures, including uniform, galvanic, pitting, filiform, fretting, intergranular, exfoliation corrosion, and stress-corrosion cracking. The article discusses geometric parameters such as pit dimensions, surface roughness, loss of metal thickness, and volume increase due to pillowing to quantitatively characterize the types of corrosion. It also explains the two most common fatigue life assessment methods used in the military aerospace industry: fatigue crack initiation and crack growth analysis.

This article discusses tools that are used for the systematic optimization of engineering designs. It focuses on the practical application of optimization technology in a computer-aided engineering environment. The article presents numerical optimization algorithms and provides some background on how these algorithms make decisions when searching for the optimal design. It also provides information on structural optimization, topology optimization, materials processing optimization, multidisciplinary optimization, and global optimization.

Machinability is more important in extending the applications of powder metallurgy (PM). This article provides an overview of the machining process and machinability measurement of PM steels. It discusses various approaches to improve machinability, including the closure of porosity, green machining, presintering, microcleanliness improvement, free-machining additives, microstructure modification, and improvements in tool materials. The effects of free-machining agents on machinability and the sintered properties of PM steels are also reviewed.