Guided wave testing (GWT) is a method of nondestructive evaluation for the inspection of pipelines. This article focuses mainly on explaining GWT as it is applied in routine established use, covered by standards, in the oil and gas industry and also introduces some of the other contexts in which its use is growing in other evolving applications. It discusses the various guided wave modes and their selection criteria. The article provides information on considerations for mode control and the sensitivity of the GWT to the defect. It also shows some examples of advanced GWT.

Flammability is the ability of a material to undergo easy ignition and rapid flaming combustion. This article provides information on flammability tests of polymers and codes and regulations that cite these tests. Many organizations are involved in the characterization and specification of flammability properties, resulting in several categorization strategies for flammability tests, including tests for specific fire response characteristics, research tests versus acceptance tests, tests for different levels of severity, and tests for basis of origin. The article presents an overview on the basic approaches in improving the fire resistance of polymers and the burning process (heating, decomposition, ignition, combustion, and propagation). It provides a brief description on the test methods which are classified into two types, one based on fire response characteristics and the other on particular applications of polymeric materials.

This article reviews the various types of mechanical testing methods, including hardness testing; tension testing; compression testing; dynamic fracture testing; fracture toughness testing; fatigue life testing; fatigue crack growth testing; and creep, stress-rupture, and stress-relaxation testing. Shear testing, torsion testing, and formability testing are also discussed. The discussion of tension testing includes information about stress-strain curves and the properties described by them.

Mechanical testing is an evaluative tool used by the failure analyst to collect data regarding the macro- and micromechanical properties of the materials being examined. This article provides information on a few important considerations regarding mechanical testing that the failure analyst must keep in mind. These considerations include the test location and orientation, the use of raw material certifications, the certifications potentially not representing the hardware, and the determination of valid test results. The article introduces the concepts of various mechanical testing techniques and discusses the advantages and limitations of each technique when used in failure analysis. The focus is on various types of static load testing, hardness testing, and impact testing. The testing types covered include uniaxial tension testing, uniaxial compression testing, bend testing, hardness testing, macroindentation hardness, microindentation hardness, and the impact toughness test.

Wear is mechanically-induced surface damage that results in the progressive removal of material. Because different types of wear occur in machinery, many different types of wear tests have been developed to evaluate its effects on materials and surface treatments. This article provides an explanation on mechanisms, forms (sliding, impact, and rolling) and the causes of wear. It describes the wear measuring methods, including the mass loss method, wear width method, and scar depth method. The units used to report wear vary with type of wear and with the purpose for which the data are to be used. Listing the considerations of tribosystem analysis, the article provides information on selection of ASTM wear test methods grouped by wear type. The article concludes by tabulating the testing geometries and parameters that are commonly controlled and reported when conducting wear tests.

This article introduces the principal methodologies and some advanced technologies that are being applied for nondestructive evaluation (NDE) of fiber-reinforced polymer-matrix composites. These include acoustic emission, ultrasonic, eddy-current, computed tomography, electromagnetic acoustic transducer, radiography, thermography, and low-frequency vibration methods. The article also provides information on NDE methods commonly used for metal-matrix composites.

Independent verification of coating system performance can be based on laboratory testing and/or field exposure. Qualification testing is a critical component to coating system selection. This article focuses on performance evaluations that are used to prequalify coating systems, namely, facility-specific, industry-specific, coating-type-specific, or a combination of these. It describes the standard laboratory tests used to generate performance data, namely, physical, compositional, chemical exposure, and application characteristics tests. The pros and cons of using manufacturer-generated data versus independently generated data are discussed. The article provides information on accelerated corrosion/weathering testing and nuclear level 1/level 2 service coatings qualification. It also describes the procedures for establishing minimum performance requirements and for determining when requalification testing may be required.

Nondestructive testing (NDT), also known as nondestructive evaluation (NDE), includes various techniques to characterize materials without damage. This article focuses on the typical NDE techniques that may be considered when conducting a failure investigation. The article begins with discussion about the concept of the probability of detection (POD), on which the statistical reliability of crack detection is based. The coverage includes the various methods of surface inspection, including visual-examination tools, scanning technology in dimensional metrology, and the common methods of detecting surface discontinuities by magnetic-particle inspection, liquid penetrant inspection, and eddy-current testing. The major NDE methods for internal (volumetric) inspection in failure analysis also are described.

This article discusses a number of workability tests that are especially applicable to the forging process. The primary tests for workability are those for which the stress state is well known and controlled. The article provides information on the tension test, torsion test, compression test, and bend test. It examines specialized tests including plane-strain compression test, partial-width indentation test, secondary-tension test, and ring compression test. The article explains that workability is determined by two main factors: the ability to deform without fracture and the stress state and friction conditions present in the bulk deformation process. These two factors are described and brought together in an experimental workability analysis.

This article discusses the equipment design, procedures, experimental considerations, and interpretation of the torsion tests used to establish workability. It describes the application of torsion testing to obtain flow-stress data and to gage fracture-controlled workability and flow-localization-controlled failure. The article discusses the torsion test used to establish the processing parameters that are required to produce the desired microstructures.

This article describes testing and characterization methods of ceramics for chemical analysis, phase analysis, microstructural analysis, macroscopic property characterization, strength and proof testing, thermophysical property testing, and nondestructive evaluation techniques. Chemical analysis is carried out by X-ray fluorescence spectrometry, atomic absorption spectrophotometry, and plasma-emission spectrophotometry. Phase analysis is done by X-ray diffraction, spectroscopic methods, thermal analysis, and quantitative analysis. Techniques used for microstructural analysis include reflected light microscopy using polarized light, scanning electron microscopy, transmission electron microscopy, energy dispersive analysis of X-rays, and wavelength dispersive analysis of X-rays. Macroscopic property characterization involves measurement of porosity, density, and surface area. The article describes testing methods such as room and high-temperature strength test methods, proof testing, fracture toughness measurement, and hardness and wear testing. It also explains methods for determining thermal expansion, thermal conductivity, heat capacity, and emissivity of ceramics and glass and measurement of these properties as a function of temperature.

This article briefly introduces the concepts of failure analysis, including root-cause analysis (RCA), and the role of failure analysis as a general engineering tool for enhancing product quality and failure prevention. It initially provides definitions of failure on several different levels, followed by a discussion on the role of failure analysis and the appreciation of quality assurance and user expectations. Systematic analysis of equipment failures reveals physical root causes that fall into one of four fundamental categories: design, manufacturing/installation, service, and material, which are discussed in the following sections along with examples. The tools available for failure analysis are then covered. Further, the article describes the categories of mode of failure: distortion or undesired deformation, fracture, corrosion, and wear. It provides information on the processes involved in RCA and the charting methods that may be useful in RCA and ends with a description of various factors associated with failure prevention.

This article aims to identify and illustrate the types of overload failures, which are categorized as failures due to insufficient material strength and underdesign, failures due to stress concentration and material defects, and failures due to material alteration. It describes the general aspects of fracture modes and mechanisms. The article briefly reviews some mechanistic aspects of ductile and brittle crack propagation, including discussion on mixed-mode cracking. Factors associated with overload failures are discussed, and, where appropriate, preventive steps for reducing the likelihood of overload fractures are included. The article focuses primarily on the contribution of embrittlement to overload failure. The embrittling phenomena are described and differentiated by their causes, effects, and remedial methods, so that failure characteristics can be directly compared during practical failure investigation. The article describes the effects of mechanical loading on a part in service and provides information on laboratory fracture examination.

This article focuses on the factors that determine the extent of deformation a metal can withstand before cracking or fracture occurs. It informs that workability depends on the local conditions of stress, strain, strain rate, and temperature in combination with material factors. The article discusses the common testing techniques and process variables for workability prediction. It illustrates the simple and most widely used fracture criterion proposed by Cockcroft and Latham and provides a workability analysis using the fracture limit line. The article describes various workability tests, such as the tension test, ring compression test, plane-strain compression test, bend test, indentation test, and forgeability test. It concludes with information on the role of the finite-element modeling software used in workability analysis.

This article describes the allotropic modification and atmospheric corrosion of pure tin. Corrosion of pure tin due to oxidation reaction, and reaction with the other gases, water, acids, bases, and other liquid media, is discussed. The article provides information on corrosion behavior on soft solders, pewter, bearing alloys, tin-copper alloys, and tin-silver alloys. It reviews the influence of corrosion on immersion tin coating, tin-cadmium alloy coatings, tin-cobalt coatings, tin-copper coatings, tin-lead coatings, tin-nickel coatings, and tin-zinc coatings. The general properties and corrosion resistance of tinplate are summarized. The article also describes the methods of corrosion testing of coatings; these include an analysis of coating thickness measurements, porosity and rust resistance testing, solderability test, and specific special tests.

This article discusses the identifying characteristics of the forms or mechanisms of corrosion that commonly attack copper metals, as well as the most effective means of combating each. It tabulates corrosion ratings of wrought copper alloys in various corrosive media. The article describes the corrosion behavior of copper alloys in specific environments. It reviews the corrosion characteristics of copper and copper alloys in various acids, alkalis, salts, organic compounds, and gases. The article provides information on the behavior of copper alloys that is susceptible to stress-corrosion cracking in various industrial and chemical environments. It concludes with a discussion on various corrosion testing methods, including aqueous corrosion testing, dynamic corrosion tests, and stress-corrosion testing.

Acoustic emission is the generation of stress waves by sudden movement in stressed materials. This article begins with a comparison of acoustic emission from most other nondestructive testing (NDT) methods, and discusses the range of applicability of acoustic emission. It describes the instrumentation principles of acoustic emission and reviews the role of acoustic emission in materials studies. The article illustrates the testing of metal-matrix composites (MMCs) using acoustic emission and the use of acoustic emission inspection in production quality control. It concludes with information on the structural test applications of acoustic emission inspection to find defects and to assess or ensure structural integrity.

Friction and wear are important when considering the operation and efficiency of components and mechanical systems. Among the different types and mechanisms of wear, adhesive wear is very serious. Adhesion results in a high coefficient of friction as well as in serious damage to the contacting surfaces. In extreme cases, it may lead to complete prevention of sliding; as such, adhesive wear represents one of the fundamental causes of failure for most metal sliding contacts, accounting for approximately 70% of typical component failures. This article discusses the mechanism and failure modes of adhesive wear including scoring, scuffing, seizure, and galling, and describes the processes involved in classic laboratory-type and standardized tests for the evaluation of adhesive wear. It includes information on standardized galling tests, twist compression, slider-on-flat-surface, load-scanning, and scratch tests. After a discussion on gear scuffing, information on the material-dependent adhesive wear and factors preventing adhesive wear is provided.

Temperature control in heat treating is of paramount importance in maintaining the quality and achieving the desired metallurgical results. This article provides a detailed account of the factors affecting temperature control in heat treating furnaces, with information on temperature control systems, including contact sensors, noncontact sensors, controllers, energy-flow regulators, measurement instruments, and set-point programmers. Common contact sensors include temperature scales, thermocouples, and resistance temperature detectors, whereas optical pyrometers and on-line radiation thermometers fall under the noncontact type. The article describes two types of instrumentation used in heat treating: field test instruments for temperature-uniformity surveys and system-accuracy tests; and controlling, monitoring, and recording instruments for digital instrumentation.

This article provides a detailed discussion on the most commonly employed tests and specific examples of the use of these tests in evaluating the corrosion resistance of powder metallurgy (P/M) stainless steels. It describes the influence of various processing parameters on the corrosion resistance of P/M stainless steels. The approaches used to improve the corrosion resistance of sintered stainless steels are discussed briefly. The article also presents a discussion on the manufacturing and corrosion characteristics of P/M superalloys.