The quantitative characterization of fracture surface geometry, that is, quantitative fractography, can provide useful information regarding the microstructural features and failure mechanisms that govern material fracture. This article is devoted to the fractographic techniques that are based on fracture profilometry. This is followed by a section describing the methods based on scanning electron microscope fractography. The article also addresses procedures for three-dimensional fracture surface reconstruction. In each case, sufficient methodological details, governing equations, and practical examples are provided.

This article reviews the origins and development of scratch tests, the experimental configurations used in these tests, and the application of the tests to characterize the mechanical response of materials. It provides information on the measurement of indentation hardness. The article describes the important parameters of the scratch test. Finally, it discusses the sliding indentation fracture process of brittle materials.

The influence of friction and wear on the function and structure of tribological systems is determined by various types of tribological tests. This article introduces the general categories of tribological testing and describes the basic objectives of testing. It reviews the results of tribological tests, where the system-dependent characteristics of friction and wear data can be expressed in different forms, such as tribographs, transition diagrams, and tribomaps. A summary of various methods of surface analysis is presented in a table. The article discusses the relationship between wear and reliability in terms of exponential distribution, Weibull distribution, and gamma distribution. It concludes with information on the effects of interaction on failure probability.

This article reviews friction and wear of various dental materials that have been studied by fundamental wear measurements, simulated service wear measurements, and clinical measurements. The materials include dental amalgam, composite restorative materials, pit and fissure sealants, dental cements, porcelain and plastic denture teeth, dental feldspathic porcelain and ceramics, endodontic instruments, periodontal instruments, and orthodontic wires. The article describes the correlations of properties such as the hardness, fracture toughness, and wear. It provides information on wear mechanism such as the sliding adhesive wear, two-body abrasion, three-body abrasion, erosion, and fatigue.

Corrosion, fatigue, and their synergistic interactions are among the principal causes of damage to aircraft structures. This article describes aircraft corrosion fatigue assessment in the context of different approaches used to manage aircraft structural integrity, schedule aircraft inspection intervals, and perform repair and maintenance of aircraft in service. It illustrates the types of corrosive attack observed in aircraft structures, including uniform, galvanic, pitting, filiform, fretting, intergranular, exfoliation corrosion, and stress-corrosion cracking. The article discusses geometric parameters such as pit dimensions, surface roughness, loss of metal thickness, and volume increase due to pillowing to quantitatively characterize the types of corrosion. It also explains the two most common fatigue life assessment methods used in the military aerospace industry: fatigue crack initiation and crack growth analysis.

The characterization, testing, and nondestructive evaluation of ceramics and glasses are vital to manufacturing control, property improvement, failure prevention, and quality assurance. This article provides a broad overview of characterization methods and their relationship to property control, both in the production and use of ceramics and glasses. Important aspects covered include the means for characterizing ceramics and glasses, the corresponding rationale behind them, and relationship of chemistry, phases, and microconstituents to engineering properties. The article also describes the effects that the structure of raw ceramic materials and green products and processing parameters have on the ultimate structure and properties of the processed piece. The effects that trace chemistry and processing parameters have on glass properties are discussed. The article describes mechanical tests and failure analysis techniques used for ceramics.

Ceramics are used widely in a number of different clinical applications in the human body. This article provides a brief history of the bioceramics field and discusses the classification of bioceramics. These include bioinert ceramics, bioactive ceramics, and bioresorbable ceramics. The article describes third-generation bioceramics, classified by Hench and Polak, such as silicate-substituted hydroxyapatite and bone morphogenic protein-carrying calcium phosphate coatings. It reviews several examination methods used to test the biocompatibility of ceramics, namely, biosafety testing, biofunctionality testing, bioactivity testing, and bioresorbability testing.

This article discusses corrosion fatigue, its effects on the damage tolerance of aircraft, and its predictive modeling. A conceptual framework is presented that incorporates two distinctive cyclic-based life-prediction philosophies and expands them both to include the time domain in order to consider the effects of corrosion. These philosophies include crack initiation used for safe-life design and crack growth used for damage tolerance. The article presents the methodology for computing the effects of real-time age degradation on an aircraft structure for two different corrosion types: crevice and pitting corrosion. It describes the rationale and techniques needed to apply the age-based structural integrity processes to in-service structures in order to realize the benefits throughout the full structural life cycle.

Liquid impingement erosion has been defined as progressive loss of original material from a solid surface due to continued exposure to impacts by liquid drops or jets. This article focuses on the core nature of erosion by liquid impingement, due to the greater appreciation of the distinctions between the different forms of erosion. It discusses steam turbine blade erosion, aircraft rain erosion, and rain erosion of wind turbine blades. The article describes the mechanisms of liquid impact erosion and time dependence of erosion rate. It reviews critical empirical observations regarding both impingement variables (velocity, impact angle, droplet size, and physical properties of liquids) and erosion resistance of materials, including the correlation between erosion resistance and mechanical properties and the effects of alloying elements and microstructure. The article also provides information on the ways to combat erosion.

Fatigue damage in metals is caused by the simultaneous action of cyclic stress, tensile stress, and plastic strain. This article details the fundamental aspects of the stages of the fatigue failure process. These include cyclic plastic deformation prior to fatigue crack initiation, initiation of one or more microcracks, propagation or coalescence of microcracks to form one or more microcracks, and propagation of one or more macrocracks.

This article reviews the general characteristics of fretting wear in mechanical components with an emphasis on steel. It focuses on the effects of physical variables and the environment on fretting wear. The variables include the amplitude of slip, normal load, frequency of vibration, type of contact and vibration, impact fretting, surface finish, and residual stresses. The form, composition, and role of the debris are briefly discussed. The article also describes the measurement, mechanism, and prevention of fretting wear. It concludes with several examples of failures related to fretting wear.

Metallographic examination is a critical step in the assessment of thermal spray coating characteristics. This article discusses the major steps involved in metallographic examination: sectioning, mounting, grinding, polishing, optical microscopy, and image analysis. It provides a discussion on etching to reveal grain structure. The article also provides recommendations for metallographic examination of some standard coatings.

The article provides a discussion on the parameters influencing abrasive wear and the elements and standards of abrasion wear tests. It emphasizes the general test procedures, advantages, and limitations of various types of abrasive wear testing. Wear testing for scratch wear, dry abrasion against fixed particles, dry abrasion against loose particles, wet abrasion against fixed or loose particles, gouging-abrasion, small particle erosion, impact abrasion, slurry abrasion, and microabrasion, are also discussed.

This article introduces various techniques commonly used in the characterization of semiconductors, namely single-crystal, polycrystalline, amorphous, oxide, organic, and low-dimensional semiconductors and semiconductor devices. The discussion covers material classification, fabrication methods, sample preparation, bulk/elemental characterization methods, microstructural characterization methods, surface characterization methods, and electronic characterization methods.

This article provides an overview of cavitation erosion with a specific focus on the estimation of mass loss. It describes the mechanisms of cavitation erosion and the types of laboratory devices to evaluate the resistance to cavitation erosion of materials. The laboratory devices include rotating disks, vibratory devices, cavitating liquid jets, and high-speed cavitation tunnels. The article discusses materials selection and surface protection to prevent cavitation erosion. It reviews the fluid-structure interaction that plays a role in cavitation erosion particularly for compliant materials. The article provides information on the numerical prediction of cavitation erosion damage by the finite element method (FEM).

This article provides information on the application of nondestructive examination (NDE) technologies to tube and pipe products. These include modeling and simulation methods, eddy-current methods, magnetic methods, acoustic methods, and physical methods. A summary of nondestructive examination methods based on flaw type and product stage is presented in a table. The article also discusses in-service inspection of tubular products and presents an example that illustrates the importance of nondestructive testing (NDT) for welds in austenitic stainless steel tubing.

This article describes two variations of carbon-base coatings: diamondlike carbon (DLC) coatings and polycrystalline diamond (PCD) coatings. It discusses the basics of a few deposition methods as they apply to industrially relevant coatings. The methods include deposition of tungsten-containing hydrogenated amorphous carbon films, deposition of tetrahedral amorphous carbon films, and deposition of silicon-incorporated hydrogenated amorphous carbon films. The most common deposition technologies for diamond films are also discussed. The article provides information on surface preparation for DLC and diamond deposition. It also provides a discussion on the coating composition and structure, mechanical and tribological properties, and applications of DLC and diamond coatings. The quality control techniques for DLC and diamond coatings are specified to meet customer requirements and ensure repeatable quality.

This article presents a general understanding of causes and possible solutions for defects in the most common metal additive manufacturing (AM) processes: laser powder-bed fusion (L-PBF), laser directed-energy deposition (DED-L), and binder jetting (BJ).

Fretting is the small-amplitude oscillatory movement that can occur between contacting surfaces, which are nominally at rest. This article discusses fretting wear in mechanical components and the mechanisms of fretting wear. It describes the role of fretting conditions, such as fretting duration, slip amplitude, normal load, fretting frequency, contact geometry, type of vibration, and surface finish, as well as the role of environmental conditions. The article reviews the influence of an aqueous environment on the mechanism of fretting. The steps that can be taken to reduce or eliminate damage due to fretting are extremely diverse. The article presents some general indications of how to address the fretting wear problem.

Bioprinting has been advancing in the field of tissue engineering as the process for fabricating scaffolds, making use of additive manufacturing technologies. In situ bioprinting (also termed intraoperative bioprinting) is a promising solution to address the limitations of conventional bioprinting approaches. This article discusses the main approaches and technologies for in situ bioprinting. It provides a brief overview of the bioprinting pipeline, highlighting possible solutions to improve currently used approaches. Additionally, case studies of in situ bioprinting are provided and in situ bioprinting future perspectives are discussed.