Heat treating furnaces require different control systems and integration for achieving optimum technical results and enabling safe operation. This article focuses on atmosphere furnaces, with some coverage on controls for vacuum furnaces. Heat treating operations require reliable monitoring and control of motion and position of various mechanical components with the help of mechanical limit switches, proximity sensors, and distance- and position-measuring devices. Using inputs from both flow meters and sensors, such as thermocouples and oxygen sensors, flow measurement control systems must be able to adjust the flow of gases for process optimization. The operator interface of a furnace-control system displays critical information such as the furnace temperature, atmosphere status, alarms, electronic chart recorders, recipe, and maintenance. A supervisory control and data-acquisition (SCADA) system is used to monitor, collect, and store data from multiple pieces of equipment.

Temperature control in heat treating is of paramount importance in maintaining the quality and achieving the desired metallurgical results. This article provides a detailed account of the factors affecting temperature control in heat treating furnaces, with information on temperature control systems, including contact sensors, noncontact sensors, controllers, energy-flow regulators, measurement instruments, and set-point programmers. Common contact sensors include temperature scales, thermocouples, and resistance temperature detectors, whereas optical pyrometers and on-line radiation thermometers fall under the noncontact type. The article describes two types of instrumentation used in heat treating: field test instruments for temperature-uniformity surveys and system-accuracy tests; and controlling, monitoring, and recording instruments for digital instrumentation.

This article discusses the installation of the most commonly used force-monitoring devices, namely, load cells and piezoelectric force sensors. It describes the purpose and operation of commonly used displacement sensors, such as linear variable differential transformers, proximity sensors, photoelectric sensors, and ultrasonic sensors. The article provides information on the sensors used for detecting tool breakages and flaws in parts, the measurement of material flow during sheet metal forming, and lubrication. It also describes the operating stages of machine vision systems used for automated quality-control purposes. The theory of eddy-current-based material properties evaluation is also discussed.

The atmosphere within a furnace chamber is a basic factor in achieving the desired chemical reactions with metals during heat treating. This article presents the fundamentals of heat treating atmospheres, and describes two groups of atmosphere control, namely, furnace atmosphere control and supply atmosphere control. The two basic types of atmospheric supply systems are generated atmospheres and nitrogen-base atmospheres. The article provides a brief overview of the gas reactions associated with oxidation and carbon control to ensure either carburization, or to prevent decarburization. It demonstrates how the carbon potential control is achieved by controlling water vapor concentration, carbon dioxide concentration, or oxygen partial pressure. The article also describes the various devices and analyzers used to monitor sampled gas from furnace atmospheres, namely, chromatographs, oxygen probes, Orsat analyzers, infrared analyzers, dewpoint analyzers, and hot-wire analyzers. Finally, it discusses the advantages, disadvantages, and limitations of these analyzers.

This article discusses various control processes carried out in powder feeding, thermal spraying, and gas flow of the thermal spray process to standardize the coating quality. Quality of the entire powder feeding process can be achieved by controlling the processing of feeding equipment as well as the characteristics of the powder being fed. Gas flow control can be achieved by using rotameters, critical orifices, and thermal mass flowmeters, whose ability to provide useful information is defined by their resolution, accuracy, linearity, and repeatability. The commercial thermal spray controls discussed here include the open-loop input-based, open-loop output-based, closed-loop input-based, and closed-loop output-based or adaptive controls. The article discusses the common causes and practical solutions for arc starting problems. It also outlines certain important developments in measuring individual and collective particle velocities, temperature, and trajectories as well as other plume characteristics for the plasma spray process.

This article discusses the effects of parameters on corrosivity and explains why it is critical to examine the parameter interactions prior to capturing the synergistic effects of the parameters on corrosion. It examines the methods of internal corrosion prediction for multiphase pipelines. The article reviews methodologies to perform internal corrosion direct assessment for pipelines. Real-time monitoring techniques for assessing actual corrosion at critical locations are discussed. The article also presents the case studies for multi-technique electrochemical corrosion monitoring.

The basic elements of control design are safety, process control, process verification, machine control, productivity, repeatability, and ease of setup. Effective systems of quality control/quality assurance are essential for heat treating practices. This article provides information on process control modes, as well as on process signatures of some items that require control, monitoring, verifying, and logging methods. It provides information on programmable logic controllers that have become efficient in machine control and monitoring. The article describes possible noise issues, National Electric Code clearance requirements, monitoring requirements, and machine accuracy that need to be considered when designing induction equipment.

This article provides an overview of the components of a resistance welding machine. It focuses on the single-phase control system and medium-frequency direct current system of resistance welding. The article also includes information on their feedback systems, rectification systems, and power sources.

This article focuses on epoxy because this resin category has widespread use and because it is tested using quality control measures typical of most resin systems. It explains that a typical resin system will consist of one or more epoxy resins, a curing agent, and a catalyst to control the rate of reaction. The article describes the component material tests, mixed resin system tests, and prepreg tests for the resin system. These tests include high-performance liquid chromatography, infrared spectroscopy, and gel permeation chromatography. The article contains a table that lists typical resin and prepreg property tests.

This article discusses the attempts made by the industry to create sensing approaches for modeling a process, part, and chemistry and kinetics. It reviews microwave curing of thick-section composites and the resin cure sensors that are used for resin cure monitoring. These include dielectric cure sensors, fiberoptics-based resin cure sensors, ultrasonics-based resin cure sensors, and dosimetry-based resin cure sensors. The article provides information on the resin cure control flow sensing, flow modeling, flow mapping, and resin flow. It addresses some practical issues in sensing resin cure and flow.

Quenching severity is agitation-dependent and therefore, magnitude and turbulence of fluid flow around a part in the quench zone are critically important relative to the uniformity of heat transfer throughout the quenching process. This article provides an overview of the measurement principles for different types of flow devices used in production quench tanks, namely, vane sensors, fluid-quench sensors, caterpillar quench-evaluation sensors, and thermal probes. Various methods of flow measurement in commercial quench tanks may be acceptable for adequate control to ensure a high-quality production process.

Gas analysis by mass spectrometry, or gas mass spectrometry, is a useful analytical tool for investigations performed in controlled atmospheres or in vacuum. This article provides sufficient information to determine if gas mass spectrometry can produce the data required and to determine the type of instrument necessary for a particular application. It discusses the working operations of gas mass spectrometer components, namely, the introduction system, ion sources, mass analyzers, and the ion detector. The article also provides information on resolution of a gas mass spectrometer determined by the width of the source slit and the collector slit. Finally, it describes the instrument set-up for gas mass spectrometry, and shows how to analyze the test results of gas mass spectrometry.

The heat treatment of steel involves a number of processes (such as stress relieving, normalizing, annealing etc) to condition the microstructure and obtain desired properties. This article discusses typical heat treating process control procedures for carbon and low-alloy steels, as well as the importance of time, and temperature control in heat treatment. Temperature Uniformity Survey, a testing procedure intended to map variations in temperature throughout the furnace work zone, helps in precise control of temperature. The article focuses on the measuring instruments used to determine gas pressure, vacuum level, gas flow, and gas composition. It focuses on their measuring quenchant characteristics, including bulk temperature, viscosity, composition, and cooling efficiency. The article describes the procedures for detecting variability in the incoming product. It presents, through an example, the general application of design of experiments techniques to locate and tune vital process parameters. The devices used in the control process of mechanical components are also reviewed.

Quenchant agitation can be obtained by circulating quenchant in a quench tank through pumps and impellers. The selection of the agitation method depends on the tank design, type and volume of the quenchant, part design, and the severity of quench required. This article describes flow measurement methods, temperature control, materials handling, and filtration processes during the agitation process. The maintenance of quenching installations is also discussed.

This article describes the thermodynamics and kinetics of gas carburizing reactions, and details the mass transfer mechanism during gas carburizing. It discusses the various considerations involved in carburizing process planning, and reviews successful operation of the gas carburizing process based on the control of three principal variables: temperature, atmosphere composition or carbon potential, and time. The article also describes the selection criteria for alloy, carbon sources, atmosphere types, and carbon monoxide level for endothermic carburizing atmospheres. It provides information on carburizing modeling, case depth prediction, case depth measurement, and case depth evaluation as well as on carburizing equipment, and also covers the factors affecting distortion after carburizing.

This article discusses various molten-metal treatments, namely fluxing, degassing, and molten-metal filtration. It focuses on various molten-metal handling systems for transporting, holding, or delivering molten metal to the mold/die system. These include launders, tundishes, holding furnaces or transport crucibles, molten-metal transfer pumps, teeming ladles, and dosing and pouring furnaces.

Inert gas fusion is a method of determining the quantitative content of gases in ferrous and nonferrous materials where gases, such as hydrogen, nitrogen, and oxygen, are physically and chemically adsorbed by the materials and later removed and swept by from the fusion area by an inert carrier gas. This article describes the operating principles and sample selection of inert gas fusion. It explains the mechanisms involved in the introduction of fusion gas, separation and detection of fusion gas by thermal-conductive and infrared detection methods. Additionally, the article explains the methods used for analyzing trace amounts of nitrogen, oxygen, and hydrogen in the carrier mediums, providing examples that aid in solving several problems.

This article focuses on various thermal analysis techniques used to verify the cure of a polymer composite. The techniques include differential scanning calorimetry (DSC), modulated DSC, thermomechanical analysis, dynamic mechanical analysis, and dielectric analysis. The article also provides an overview of the composite failure modes affected by matrix resin and testing approach.

Health and safety are critically important issues, and there are numerous aspects of the production and use of metal powders that may entail exposure to hazardous conditions. This article provides a discussion on the issues associated with the safe production and handling of metal powders and the safe operation of continuous mesh belt sintering furnaces with combustible atmospheres. It also provides a comprehensive high-level overview of the safety-related issues and concerns related to the use of compacting presses in the manufacturing sector.

Simulated service testing includes exposures of either structural components or test specimens in environments that are representative of many general service situations. This article discusses the selection criteria of test specimens and methods of assessing the corrosion effects. The ASTM International and NACE International standards that are directly or indirectly applicable to simulated service corrosion testing in water are tabulated. The article also describes the effects of variable concentrations of dissolved carbonates, such as calcium, magnesium, and/or sodium, in water on corrosion.