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in Thin Section Preparation and Transmitted Light Microscopy for Fiber-Reinforced Composites[1]
> Metallography and Microstructures
Published: 01 December 2004
Fig. 5 Photograph of a sacrificial hand vise used for rough and fine grinding the second face of the sample
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003791
EISBN: 978-1-62708-177-1
... Abstract This article reviews how process variations influence the characteristics of thermal spray coatings. It describes various specimen preparation techniques, which allow accurate microstructural analysis. These techniques include sectioning, cleaning, mounting, planar grinding, fine...
Abstract
This article reviews how process variations influence the characteristics of thermal spray coatings. It describes various specimen preparation techniques, which allow accurate microstructural analysis. These techniques include sectioning, cleaning, mounting, planar grinding, fine grinding, rough polishing, and etching. The article provides information on the problems associated with specimen preparation. It concludes with a discussion on the various methods of analysis for thermal spray coatings.
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Published: 01 December 2004
Fig. 26 Polarized light micrograph showing grinding artifacts in unalloyed uranium. Bands of fine twins are due to deformation from coarse grinding steps that was not removed by subsequent fine grinding and polishing. Electropolished using procedure 1 in Table 1 and anodized using procedure
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Published: 01 December 1998
Fig. 1 Three basic types of crushing-and-grinding circuits. (a) Conventional. (b) Autogenous. (c) Autogenous with separate fine grinding
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Published: 01 December 2004
Fig. 11 Effects of various grinding and polishing stages on the specimen surface. (a) The rolling action of diamond particles on a hard lap surface during planar grinding produces a flat specimen with a minimal amount of damage to the coating. (b) During fine grinding, rotating the specimen
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Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006089
EISBN: 978-1-62708-175-7
..., and fracture resistance increases. Particle fineness approaches a limit as milling continues, and maximum energy is expended. According to Ref 3 , the following major factors contribute to grind limit: Increasing resistance to fracture Increasing cohesion between particles, with decreasing particle...
Abstract
Milling of materials, whether hard and brittle or soft and ductile, is of prime interest and of economic importance to the powder metallurgy (PM) industry. This article discusses the principles of milling, milling parameters, and the powder characteristics required for the process. It discusses the changes in powder particle morphology that occur during milling of metal powders produced by various processes such as microforging, fracturing, agglomeration, and deagglomeration. The article also provides useful information on milling equipment such as tumbler ball mills, vibratory ball mills, attrition mills, and hammer and rod mills.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009076
EISBN: 978-1-62708-177-1
... 120-grit SiC paper, to a final thickness of 1 mm (0.04 in.). This is often time-consuming, depending on the original specimen thickness. Step 3: Mounting the Wafer in the Vise for Grinding the Second Surface Coarse and fine grinding is performed with the aid of a sacrificial hand vise ( Fig. 5...
Abstract
This article describes the various aspects relating to the selection and preparation of ultrathin-section specimens of fiber-reinforced polymeric composites for examination by transmitted light microscopy. It provides information on the contrast-enhancement methods used by transmitted-light microscopy and optimization of microscope conditions. Examples of composite ultrathin sections analyzed using transmitted-light microscopy contrast methods are also presented.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003737
EISBN: 978-1-62708-177-1
... Abstract This article discusses the specimen preparation of three types of cast and wrought heat-resistant alloys: iron-base, nickel-base, and cobalt-base. Specimen preparation involves sectioning, mounting, grinding, polishing, and etching. The article illustrates the microstructural...
Abstract
This article discusses the specimen preparation of three types of cast and wrought heat-resistant alloys: iron-base, nickel-base, and cobalt-base. Specimen preparation involves sectioning, mounting, grinding, polishing, and etching. The article illustrates the microstructural constituents of cast and wrought heat-resistant alloys. It describes the identification of ferrite by magnetic etching. The transmission electron microscopy examination of the fine strengthening phases in wrought alloys and bulk extraction in heat-resistant alloys are included. The article also reviews the gamma prime phase, gamma double prime phase, eta phase, laves phase, sigma phase, mu phase, and chi phase in wrought heat-resistant alloys.
Book Chapter
Book: Machining
Series: ASM Handbook
Volume: 16
Publisher: ASM International
Published: 01 January 1989
DOI: 10.31399/asm.hb.v16.a0002186
EISBN: 978-1-62708-188-7
... and shaping, broaching, drilling, reaming, counterboring, milling, sawing, and grinding operations performed on magnesium. Safety measures related to machining, handling of chips and fines, and fire extinguishing are also discussed. boring broaching clamping cold working counterboring drilling...
Abstract
Magnesium is machined in low-volume production on small, manually operated machine tools and on large, specially built, completely automated transfer machines operating at high production rates. This article focuses on the factors that affect the machining of magnesium. It discusses chip formation and distortion due to thermal expansion, cold work, and clamping and provides information on magnesium-matrix composites. The article describes materials, design, and sharpness as factors for selection of tool for machining magnesium. It illustrates turning and boring, planing and shaping, broaching, drilling, reaming, counterboring, milling, sawing, and grinding operations performed on magnesium. Safety measures related to machining, handling of chips and fines, and fire extinguishing are also discussed.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009073
EISBN: 978-1-62708-177-1
... previously, SiC papers are one of the most expensive options for rough and fine grinding. Figure 9 ( a , b ) show cross sections of 120-grit SiC paper before and after the grinding step of one mounted specimen. There is a significant reduction in the surface roughness after only one sample. In the first...
Abstract
Rough grinding and polishing of specimens are required to prepare fiber-reinforced composite samples for optical analysis. This article discusses the consumables, process variables, and the equipment that influence the sample preparation procedure. It describes the hand and automated grinding methods. The article summarizes the rough and final polishing steps for both hand and automated techniques. Common artifacts that may be created during grinding and polishing steps of composite samples are reviewed. These include scratches, fiber pull-out, matrix smears, streaks, erosion of different phases, and fiber and sample edge rounding and relief.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003795
EISBN: 978-1-62708-177-1
... Diamond disk 65 Water 300 ∼180 ∼40 Until flat Diamond disk 20 Water 300 ∼180 ∼40 5–10 Fine grinding Composite disk 6 Alcohol-based 300 ∼100 ∼23 5–15 Polishing Pellon cloth 6 Alcohol-based 150 ∼150 ∼34 15–120 Hard synthetic cloth 3 Alcohol-based 150 ∼120 ∼27 15...
Abstract
Microstructural analysis reveals many important details about the qualities and capabilities of high-performance ceramics. This article explains how to prepare ceramic samples for imaging and the imaging technologies normally used. It describes sectioning, mounting, grinding, and polishing as well as ceramographic etching. It discusses common imaging approaches, including scanning electron microscopy and thin-section polarized light techniques, a type of optical microscopy. The article also addresses microstructural classification, examining detailed micrographs from samples of aluminum oxide, zirconium dioxide, aluminum nitride, silicon carbide, and piezoelectric ceramics.
Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001232
EISBN: 978-1-62708-170-2
... or finish ( Table 1 ). In rough grinding processes, material removal occurs at a rapid rate, with less emphasis on surface roughness/tolerances. In contrast, high-precision methods emphasize the attainment of fine surface finish and close tolerances at the expense of material removal rates. In precision...
Abstract
Abrasive finishing is a method where a large number of multipoint or random cutting edges are coupled with abrasive grains as a bond or matrix material for effective removal of material at smaller chip sizes. This article provides a broad overview of the various categories of abrasive products and materials, abrasive finishing processes, and the mechanisms of delivering the abrasives to the grinding or machining zone. Abrasive finishing processes, such as grinding, honing, superfinishing, microgrinding, polishing, buffing, and lapping, are discussed. The article presents a brief discussion on abrasive jet machining and ultrasonic machining. It concludes with a discussion on the four categories of factors that affect the abrasive finishing or machining: machine tool, work material, wheel selection, and operational.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003055
EISBN: 978-1-62708-200-6
... in a variety of configurations. Honing, also called fine grinding, also uses fixed abrasives in a wheel or disk. Alternatively, abrasives can be applied to the work surface without being held in a grinding wheel. These methods, called free-abrasive machining, include lapping and polishing. Principles...
Abstract
Ceramics usually require some form of machining prior to use to meet dimensional and surface quality standards. This article focuses on abrasive machining, particularly grinding, and addresses common methods and critical process factors. It covers cylindrical, centerless, and disk grinding and provides information on tooling, wheel selection, work material, and operational factors. It also discusses precision slicing and slotting, lapping, honing, and polishing as well as abrasive waterjet, electrical discharge, laser, and ultrasonic machining.
Book: Composites
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003464
EISBN: 978-1-62708-195-5
... it was before grinding. Wet-grinding with silicon carbide (SiC) paper will not introduce damage that cannot be removed easily if 120, 320, and 600 grit papers are used sequentially. However, because of their short useful life, SiC papers are one of the most expensive options for rough and fine sanding (each...
Abstract
Microscopy is a valuable tool in materials investigations related to problem solving, failure analysis, advanced materials development, and quality control. This article describes the sample preparation techniques of composite materials. These techniques include mounting, rough grinding, and polishing. The preparation techniques of ultrathin sections are also summarized. The article explains the illumination methods used by reflected light microscopy to view a specimen. These consist of epi-bright-field illumination, epi-dark-field illumination, epi-polarized light, and epi-fluorescence. The article also provides information on transmitted light microscopy.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003190
EISBN: 978-1-62708-199-3
... value) surface would require grinding or additional subsequent operations, such as honing, superfinishing, buffing, or abrasive flow. Therefore, specifying very fine finishes will normally result in increased costs ( Table 3 ). Classification of machined surface finishes Table 3 Classification...
Abstract
Both surface finish and surface integrity must be defined, measured, and maintained within specified limits in the processing of any product. Surface texture is defined in terms of roughness, waviness, lay, and flaws. This article illustrates some of the designations of surface roughness and the symbols for defining lay and its direction. In addition, it describes the applications of surface integrity, typical surface integrity problems created in metal removal operations, and principal causes of surface alterations produced by machining processes. The article tabulates the effect of some machining methods on fatigue strength, and low-stress grinding procedures for steels, nickel-base high-temperature alloys, and titanium alloys.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003750
EISBN: 978-1-62708-177-1
... will be sufficient. When more detail is required, grind the specimen on a surface grinder, finishing with a fine, smaller-than-150-grit wheel using light feeds with a clean wheel. The greatest detail can be obtained using metallographic techniques ( Ref 1 ), but the size of the specimen will be limited...
Abstract
Macroetching is a procedure for revealing the large-scale structure of a metallic specimen, that is, the structure visible with the unaided eye, by etching an appropriately prepared surface. This article provides information on the basic procedures for macroetching as well as the apparatus used. It discusses selected etchants for efficient macroetching of various metals and their alloys, including iron, steel, high-alloy steels, stainless steels, high-temperature alloys, titanium, titanium alloys, aluminum, aluminum alloys, copper, and copper alloys. The article also describes various conditions that are revealed by the macroetching of aluminum.
Book: Thermal Spray Technology
Series: ASM Handbook
Volume: 5A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v05a.a0005729
EISBN: 978-1-62708-171-9
... Abstract Metallographic examination is a critical step in the assessment of thermal spray coating characteristics. This article discusses the major steps involved in metallographic examination: sectioning, mounting, grinding, polishing, optical microscopy, and image analysis. It provides...
Abstract
Metallographic examination is a critical step in the assessment of thermal spray coating characteristics. This article discusses the major steps involved in metallographic examination: sectioning, mounting, grinding, polishing, optical microscopy, and image analysis. It provides a discussion on etching to reveal grain structure. The article also provides recommendations for metallographic examination of some standard coatings.
Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001282
EISBN: 978-1-62708-170-2
... type of process to be used. Fig. 2 Typical microstructure of a plasma-sprayed tungsten metal coating showing the splat structure and the fine crystalline structure within the splats. (a) Scanning electron micrograph of a fracture surface. (b) Light micrograph of the same coating. Courtesy...
Abstract
This article introduces thermal spray coatings and describes the various types of coating processes and coating devices, including the flame spray, electric-arc spray, plasma spray, transferred plasma arc, high-velocity oxyfuel, and detonation gun. It provides information on the surface preparation methods and finishing treatments of coated parts. The article also explains the tests to evaluate the coating quality and the effects of coating structures and mechanical properties on coated parts. It concludes with a discussion on the uses of thermal spray coatings.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003245
EISBN: 978-1-62708-199-3
... more efficient abrasive. Rough polishing is most often done on a cloth-covered disk rotating at 150 rpm. The specimen is held by hand and moved in the direction opposite to the direction of wheel rotation. Alternatively, automatic devices can be used for grinding and polishing. Fine polishing...
Abstract
Proper sectioning of the surface to be examined is a very important step in preparing steel specimens. The first step in preventing damage to the metallurgical structure is to minimize the amount of sectioning that is done. This article discusses the various metallographic techniques, namely mounting, grinding, polishing, and etching involved in the microstructural analysis of carbon and alloy steels, case hardening steels, cast iron, ferrous powder metallurgy alloys, wrought and cast stainless steels, tool materials, steel castings, iron-chromium-nickel heat-resistant casting alloys and different product forms of steels.
Series: ASM Handbook
Volume: 2A
Publisher: ASM International
Published: 30 November 2018
DOI: 10.31399/asm.hb.v02a.a0006517
EISBN: 978-1-62708-207-5
...). Precision methods emphasize the attainment of fine surface finish and close tolerances at the expense of material removal rates, while rough grinding is for high material removal rates with less emphasis on surface roughness/tolerances. A comparison of these three general categories: Finishing process...
Abstract
Mechanical finishes usually can be applied to aluminum using the same equipment used for other metals. This article describes the two types of grinding used in mechanical finishing: abrasive belt grinding and abrasive wheel grinding. It reviews the binders and fluid carriers used in buffing, and discusses satin finishing and barrel finishing. It also describes lapping and honing techniques that are of special interest in treating aluminum parts that have received hard anodic coatings. Honing recommendations for aluminum alloys are presented in a table.
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