This article focuses on the fractography features of the conventional powdered metal (PM) process for ferrous powders. It discusses porosity, which is one of the inherent features present in components produced by conventional press-and-sinter processes, and green cracks, which are the most common fracture issue in conventional PM processes. It explains the effect of post-sintering operations. The article also presents the common ferrous powder metallurgy materials.

Certain metal products can be produced only by powder metallurgy; among these products are materials whose porosity is controlled. Successful production by powder metallurgy depends on the proper selection and control of process variables: powder characteristics; powder preparation; type of compacting press; design of compacting tools and dies; type of sintering furnace; composition of the sintering atmosphere; choice of production cycle, including sintering time and temperature; and secondary operations and heat treatment. When the application of a powder metallurgy part requires high levels of strength, toughness, or hardness, the mechanical properties can be improved or modified by infiltration, heat treatment, or a secondary mechanical forming operation such as cold re-pressing or powder forging. The article also discusses the effect of the secondary processes on P/M mechanical properties.

Metallographic analysis is primarily a collection of visual and imaging techniques that provide an insight into the background of a material or part and its behavior. Metallic specimens, both porous and pore-free, are opaque, and as a result, an optical examination must be performed on carefully prepared planar (two-dimensional) surfaces. This article discusses the preparation sequence of ferrous powders, which is normally separated into several well-defined steps: sample selection, sectioning, mounting, grinding, polishing, drying, and chemical etching and/or coating. It provides several suggestions to promote and encourage the safety of those performing metallographic preparation and analysis.

This article summarizes the general classification, mechanical properties, and applications of ferrous powder metallurgy (PM) materials for parts production. It discusses four principal ferrous PM alloy types: admixed elemental alloys, diffusion alloys, prealloys, and hybrid alloys. The article reviews the benefits and disadvantages as well as the effect of processing on the properties and material microstructure of these alloys. It contains tables that list the mechanical properties of various iron-copper and copper steels.

Iron powders are the most widely used powder metallurgy (P/M) material for structural parts. This article reviews low to medium density iron and low-alloy steel parts produced by the pressing and sintering technology. It explains different powder production methods, including Hoeganaes process, Pyron process, atomization of liquid metal, thermal decomposition and the electrodeposition process for carbonyl and electrolytic iron powders. It describes the types of compaction and sintering, explaining their effects of processing with designations. Further, the article deals with the mechanical and physical properties of ferrous P/M materials, which may depend on certain factors, namely microstructure, porosity, density, infiltration, re-pressing, chemical composition, and heat treatment.

This article discusses the production of low-alloy steel parts by powder forging, focusing on the material considerations, such as hardenability and inclusion assessment; and process considerations, including sintering and reheating, metal flow, and secondary operations. It presents the mechanical property data for copper and graphite powders mixed with an iron powder base to produce materials that generally contain 2″ Cu, including tensile, impact, and fatigue properties. Heat treatment procedures used in developing the properties of the prealloyed powder forged materials are also covered. Finally, the article describes the process steps and cost considerations in metal injection molding (MIM) and tabulates the composition, and mechanical properties of MIM low-alloy steels.

High-temperature sintering of ferrous components continues to be important in the powder metallurgy (PM) industry. Improvements in both production rates and properties are possible as sintering temperatures increase above 1120 deg C. This article provides an overview of the different various stages of the sintering process and the physical, chemical, and metallurgical phenomena occur within the mass of metal powder particles. It discusses the four advantages of high-temperature sintering of various ferrous PM materials: improved mechanical properties, improved physical properties, development of liquid phase, and ability to sinter active elements in alloy steels. The article also provides information on three sources of process control requirements, namely, the powder blend, green density, and sintering conditions.

This article briefly reviews the production methods and characteristics of plain carbon and low-alloy water-atomized iron and steel powders, high-porosity iron powder, carbonyl iron powder, and electrolytic iron powder. It emphasizes on atomized powders, because they are the most widely used materials for ferrous powder metallurgy. The article provides information on the properties and applications of these powders. It also includes an overview of diffusion alloying, basics of admixing, and bonded premixes.

Proper sectioning of the surface to be examined is a very important step in preparing steel specimens. The first step in preventing damage to the metallurgical structure is to minimize the amount of sectioning that is done. This article discusses the various metallographic techniques, namely mounting, grinding, polishing, and etching involved in the microstructural analysis of carbon and alloy steels, case hardening steels, cast iron, ferrous powder metallurgy alloys, wrought and cast stainless steels, tool materials, steel castings, iron-chromium-nickel heat-resistant casting alloys and different product forms of steels.

Various powder production processes allow precise control of the chemical composition and physical characteristics of powders and allow tailoring of specific attributes for targeted applications. Metal powders are produced by either mechanical methods or chemical methods. The commonly used mechanical methods include water and gas atomization, milling, mechanical alloying, and electrolysis. Some chemical methods include reduction of oxides. This article provides information on the reliable techniques for powder characterization and testing to evaluate the chemical and physical properties of metal powders, both as individual particles and in bulk forms.

The organizations that are most active in the development of standards for powder metallurgy (PM) are the American Society for Testing and Materials (ASTM), Metal Powder Industries Federation (MPIF), and International Standards Organization (ISO). This article presents the test method standards, materials standards, and material designation codes for PM materials. It provides information on the codes for structural parts, PM soft magnetic materials, PM self-lubricating bearings, metal injection molded materials, and powder forged materials.

This article reviews various segments of the powder metallurgy (PM) process from powder production and powder processing through the characterization of the materials and their properties. It covers the processing methods for consolidating metal powders including options for processing to full density. The article outlines the freeform fabrication process, also known as additive manufacturing and describes finishing operations of PM parts. It concludes with information on the applications of PM parts.

Powder forging is an extension of the conventional press and sinter powder metallurgy process, which is recognized as an effective technology for producing a variety of parts to net or near-net shape. This article focuses on the material considerations, such as powder characteristics, alloy development, and inclusion assessment; and process considerations, such as process stages, tool design, and secondary operations; of ferrous alloy powder forging. The mechanical properties of powder forged materials are also reviewed. The article discusses the quality assurance tests for powder forged materials: the part dimensions and surface finish measurement, magnetic particle inspection, metallographic analysis, and nondestructive testing. It concludes with a discussion on the applications of powder forged parts with examples.

This article provides an overview of the general methods of metal powder production. It details the primary methods for particle sizing used in additive manufacturing: sieving, laser diffraction and scattering, and digital image analysis. Methods of interpreting and understanding particle size distribution (PSD) data are presented, with an emphasis on the differences between count- and volume-based PSDs. The article then outlines practices for both qualitative and quantitative assessment of particle morphology.

Metal powders are used as fuels in solid propellants, fillers in various materials, such as polymers or other binder systems, and for material substitution. They are also used in food enrichment, environmental remediation market, and magnetic, electrical, and medical application areas. This article reviews some of the diverse and emerging applications of ferrous and nonferrous powders. It also discusses the functions of copier powders and the processes used frequently for copier powder coating.

This article provides information on the most frequently used atmospheres in commercial sintering of powder metallurgy iron and steel materials. These include endothermic, exothermic, dissociated ammonia, pure hydrogen, and nitrogen-base atmospheres. The article discusses sintering of iron and iron-graphite powder, iron-copper and iron-copper graphite, and alloy steels. The effects of various sinter conditions on the amount of combined carbon formed in the steel are also discussed. The article concludes with information on high-temperature sintering and sinter hardening.