Simulated service testing is the most reliable predictor of corrosion behavior that is important for specific objectives. These include materials selection, predicting the probable service life of a product or structure, evaluating new commercial alloys and processes, and calibrating laboratory corrosion tests in short of in-plant tests and actual service experience. This article provides a detailed discussion on the types of atmospheres used in simulated service testing. It describes the specifics of atmospheric-corrosion test that include equipment, test arrangement, and test specimen; factors affecting atmospheric corrosion; and evaluation of exposed atmospheric-corrosion panels. The article concludes with a discussion on the empirical model used for analyzing the atmospheric-corrosion measurements for estimating the service life of the part being evaluated.

This article focuses on the application of solid-state nuclear magnetic resonance (NMR) spectroscopy in materials science, especially for inorganic and organic polymer solids. It begins with a discussion on the general principles of NMR, providing information on nuclear spin descriptions and line narrowing and spectral resolution and describing the impact of magnetic field on nuclear spins and the factors determining resonance frequency. This is followed by a description of various systems and equipment necessary for NMR spectroscopy. A discussion on general sampling for solid-state NMR, sample-spinning requirements, and extraneous signals is then included. Various factors pertinent to accurate calibration of the NMR spectrum are also described. The article provides information on some of the parameters both beneficial and problematic for processing NMR data. It ends with a description of the applications of NMR in glass science and ceramics.

This article is a brief account of low-energy ion-scattering spectroscopy (LEIS) for determining the atomic structure of solid surfaces. It begins with a description of the general principles of LEIS. This is followed by a section providing information on the equipment used for LEIS. Various steps involved in the sample preparation, calibration, and data analysis are then discussed. The article concludes with a section on the applications and interpretation of LEIS in material analysis, including discussion on surface structural analysis, layer-by-layer (Frank-van der Merwe) growth, and low-energy atom-scattering spectroscopy.

Differential scanning calorimetry (DSC) is the most common thermal technique for polymer characterization. This article provides a detailed account of the various factors and processes involved in DSC. The discussion covers the equipment used, specimen preparation process, calibration requirements, data analysis, and provides examples of the applications and interpretation of DSC.

Dynamic mechanical analysis (DMA) is a powerful tool for studying the viscoelastic properties and behavior of a range of materials as a function of time, temperature, and frequency. This article describes various systems and equipment used in DMA setup and discusses the processes involved in preparation of test specimen for DMA measurements. Some factors to be considered when calibrating the DMA instrument are provided, along with a description on processes for interpreting the temperature and frequency dependence of DMA curves as well as the applications of DMA.

Thermomechanical analysis (TMA) is a thermal analysis technique in which the length of a specimen is precisely measured versus temperature and time as the specimen is subjected to controlled heating and cooling. This article discusses the various factors and processes involved in TMA. The discussion covers the general principles, equipment used, specimen preparation process, calibration conditions, data analysis steps, and examples of the applications and interpretation of TMA.

This article discusses various concepts of micro x-ray diffraction (XRD) used for the examination of materials in situ. The discussion covers the principles, equipment used, sample preparation procedure, considerations for calibrating a detector, steps for performing data analysis, and applications and interpretation of micro-XRD.

A close-interval survey (CIS) is a series of structure-to-electrolyte direct current potential measurements performed at regular intervals for assessing the level of cathodic protection (CP) on pipelines and other buried or submerged metallic structures. This article describes the equipment required to perform the CIS. It provides a discussion on the activities that should be performed during the preparation and execution of the CIS. The dynamic stray current identification and compensation by CIS is discussed briefly. The article also explains various factors involved in the validation of CIS data. It concludes with information on CIS data interpretation.

The article provides an overview of the various types of testing machines: gear-driven or screw-driven machines and servohydraulic machines. It examines force application systems, force measurement, and strain measurement. The article discusses important instrument considerations and describes gripping techniques of test specimens. It analyzes test diagnostics and reviews the use of computers for gathering and reducing data. Emphasis is placed on universal testing machines with separate discussions of equipment factors for tensile testing and compressing testing. The influence of the machine stiffness on the test results is also described, along with a general assessment of test accuracy, precision, and repeatability of modern equipment.

The goal of using nondestructive evaluation (NDE) in conjunction with failure analysis is to obtain the most comprehensive set of data in order to characterize the details of the damage and determine the factors that allowed the damage to occur. The NDE results can be used to determine optimal areas upon which to focus for sectioning and metallography in order to further investigate the condition of the component. This article provides information on the inspection method available for failure analysis, including standard methods such as visual testing, penetrant testing, and magnetic particle testing. It covers the effects of various factors on the properties of the part that may impact failure analysis, describes the characterization of damage modes and crack sizes, and finally discusses the processes involved in application of NDE results to failure analysis.

This article provides information on soldering iron and the most common soldering iron tip. It describes the classifications of hand soldering equipment based on its temperature control method. These are constant-voltage, variable temperature, and tip-temperature-controlled soldering irons. The article also reviews the selection criteria of the soldering iron.

This article defines quality, quality assurance, quality control, and quality management of processes, products, and services. It describes the evolution of quality control and quality assurance in the coatings industry. The article also discusses the standards, quality programs, and certifications in the coatings industry.

This article discusses the inspection/reference standards that are absolutely critical for proper application of ultrasonic inspection systems. Many of the standards and specifications for ultrasonic inspection require the use of standard reference blocks. The article lists the variables that should be considered when selecting standard reference blocks and describes the three types of standard blocks ordinarily used for calibration or reference: area-amplitude blocks, distance-amplitude blocks, and blocks of the type sanctioned by the International Institute of Welding. It reviews the determination of area-amplitude and distance-amplitude curves of a straight-beam pulse-echo ultrasonic inspection system. The article discusses the three principal conventional manual ultrasonic sizing techniques: 6 dB drop technique, maximum-amplitude technique, and 20 dB drop technique. It provides information on the dimension-measurement applications of ultrasonic inspection methods.

Heat treating furnaces require different control systems and integration for achieving optimum technical results and enabling safe operation. This article focuses on atmosphere furnaces, with some coverage on controls for vacuum furnaces. Heat treating operations require reliable monitoring and control of motion and position of various mechanical components with the help of mechanical limit switches, proximity sensors, and distance- and position-measuring devices. Using inputs from both flow meters and sensors, such as thermocouples and oxygen sensors, flow measurement control systems must be able to adjust the flow of gases for process optimization. The operator interface of a furnace-control system displays critical information such as the furnace temperature, atmosphere status, alarms, electronic chart recorders, recipe, and maintenance. A supervisory control and data-acquisition (SCADA) system is used to monitor, collect, and store data from multiple pieces of equipment.

Ultrasonic inspection is a nondestructive technique that is useful in both quality control and research applications for flaw detection in fiber-reinforced composite materials. This article describes ultrasonic nondestructive analysis by outlining its three basic types of scans. It reviews the important quality control techniques used during the manufacture of composite components by analyzing tooling control, material control, pattern orientation control, and in-process control.

The purpose of accreditation is to evaluate and assure high-quality results from suppliers of products or services without incurring the costs associated with auditing each supplier. This article describes laboratory accreditation based on the general requirements of International Organization for Standardization/International Electrotechnical Commission (ISO/IEC) Guide 25, "General Requirements for the Competence of Calibration and Testing Laboratories." The Guide 25 is a balanced standard that addresses quality system requirements of ISO 9000 and the technical requirements needed to perform testing or calibration. The article describes an accreditation process that would enhance the international acceptance of test data for mechanical testing laboratories.

Risk assessments (RAs) must be customized to the specific workplaces and to the actual work being performed. It is performed to make the workers and their management aware of the hazards in the work environment, identify each risk in a methodical manner, and put in place a plan to mitigate the hazards. Information on risk assessment presented in this article provides a logical approach that can be taken to minimize risk and maximize thermal spray practitioners' safety. There are basically four steps to improving operational safety by using RAs: identifying the risks for each activity, rating the risk, putting in place the actions required to minimize risk, and reviewing and updating the RAs on a regular basis. The article presents two case studies to illustrate the concepts involved in RAs.

This article provides a clear but nonexhaustive description of the general principle of atomic emission, with a particular focus on instrumentation, and summarizes the main characteristics of the inductively coupled plasma optical emission spectrometer technique. Basic atomic theory as well as the instrument characteristics and their influence on the instrument performances are presented. The advantages, drawbacks, and developments of this technique are discussed, and, finally, alternative techniques and examples of applications are provided.

Miscellaneous hardness tests encompass a number of test methods that have been developed for specific applications. These include dynamic, or "rebound," hardness tests using a Leeb tester or a Scleroscope; static indentation tests on rubber or plastic products using the durometer or IRHD testers; scratch hardness tests; and ultrasonic microindentation testing. This article reviews the procedures, equipment, and applications associated with these alternate hardness test methods.

The gage repeatability and reproducibility (GRR) study is a procedure for determining the repeatability of a test instrument and the reproducibility of a specific gage in operation. This article reviews the general method of GRR studies and its application for indentation hardness testing. It describes a long method and a short method for evaluation of GRR. The article analyzes factors of hardness testing instruments and provides guidelines for hardness tests. It concludes with a list of suggestions that can improve hardness tests.