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electrochemical parameters
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Series: ASM Handbook
Volume: 13C
Publisher: ASM International
Published: 01 January 2006
DOI: 10.31399/asm.hb.v13c.a0004209
EISBN: 978-1-62708-184-9
... and evaluation of dental materials are summarized. The article examines the effects of restoration contact on electrochemical parameters and reviews the concentration cells developed by dental alloy-environment electrochemical reactions. The composition and characterization of biofilms, corrosion products...
Abstract
This article describes dental alloy compositions and its properties. It discusses the safety and efficacy considerations of dental alloy devices. The article defines and compares interstitial fluid and oral fluid environments. Artificial solutions developed for the testing and evaluation of dental materials are summarized. The article examines the effects of restoration contact on electrochemical parameters and reviews the concentration cells developed by dental alloy-environment electrochemical reactions. The composition and characterization of biofilms, corrosion products, and other debris that deposit on dental material surfaces are discussed. The article evaluates the types of alloys available for dental applications, including direct filling alloys, crown and bridge alloys, partial denture alloys, porcelain fused to metal alloys, wrought wire alloys, soldering alloys, and implant alloys. The effects of composition and microstructure on the corrosion of each alloy group are also discussed. The article concludes with information on the tarnishing and corrosion behavior of these alloys.
Series: ASM Handbook
Volume: 2A
Publisher: ASM International
Published: 30 November 2018
DOI: 10.31399/asm.hb.v02a.a0006523
EISBN: 978-1-62708-207-5
... Abstract Anodizing produces a uniform, continuous, highly ordered network of individual cells comprising a layer whose thickness and cell dimensions, and ultimately engineering properties, depend on the electrochemical parameters of the anodizing process. This article discusses the nucleation...
Abstract
Anodizing produces a uniform, continuous, highly ordered network of individual cells comprising a layer whose thickness and cell dimensions, and ultimately engineering properties, depend on the electrochemical parameters of the anodizing process. This article discusses the nucleation and growth of anodic aluminum oxide and the important characteristics of the finished porous anodic aluminum oxide. In industry, anodic oxides and the anodizing processes have been categorized into types that exhibit specific properties to suit specific applications. The article reviews the two most basic types of oxides, namely, barrier-layer anodic oxides and porous anodic oxides. It concludes with a description of postanodizing processes, such as dyeing and sealing.
Series: ASM Handbook
Volume: 13C
Publisher: ASM International
Published: 01 January 2006
DOI: 10.31399/asm.hb.v13c.a0004214
EISBN: 978-1-62708-184-9
... , 15 ) have evaluated the effects of critical parameters such as pH and velocity on CO 2 corrosion. Predictive models, including a combination of the parameters discussed in this article along with electrochemical considerations, have also been used to arrive at the corrosion rate ( Ref 16 , 17...
Abstract
This article discusses the effects of parameters on corrosivity and explains why it is critical to examine the parameter interactions prior to capturing the synergistic effects of the parameters on corrosion. It examines the methods of internal corrosion prediction for multiphase pipelines. The article reviews methodologies to perform internal corrosion direct assessment for pipelines. Real-time monitoring techniques for assessing actual corrosion at critical locations are discussed. The article also presents the case studies for multi-technique electrochemical corrosion monitoring.
Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003633
EISBN: 978-1-62708-182-5
... Abstract Stress-corrosion cracking (SCC) is a phenomenon in which time-dependent crack growth occurs when the necessary electrochemical, mechanical, and metallurgical conditions exist. This article provides an overview of the environmental phenomenon, mechanisms, and controlling parameters...
Abstract
Stress-corrosion cracking (SCC) is a phenomenon in which time-dependent crack growth occurs when the necessary electrochemical, mechanical, and metallurgical conditions exist. This article provides an overview of the environmental phenomenon, mechanisms, and controlling parameters of SCC. It describes the phenomenological and mechanistic aspects of the initiation and propagation of SCC. The article includes a phenomenological description of crack initiation and propagation that describes well-established experimental evidence and observations of stress corrosion. Discussions on mechanisms describe the physical process involved in crack initiation and propagation. The article also includes information on dissolution models and mechanical fracture models.
Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003696
EISBN: 978-1-62708-182-5
... of the electrochemical parameters of the metal-solution system, the geometry of the equipment, any special operational conditions, and the special requirements of the environment around the system. The electrochemical parameters of concern are the potential at which the vessel must be maintained for corrosion protection...
Abstract
This article presents a brief history and the uses of the anodic protection technique. It compares anodic and cathodic protection and describes the design considerations of the anodic protection system. The article discusses the specific requirements of equipment required for anodic protection. It also explains the applications and economic aspects of anodic protection, with examples.
Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003598
EISBN: 978-1-62708-182-5
... Abstract This article provides a discussion on a working principle, the operations, characteristics, capabilities, and applications of electrochemical grinding (ECG). The basic elements of the ECG machine tool are also presented. electrochemical grinding machine tools HYBRID...
Book Chapter
Book: Machining
Series: ASM Handbook
Volume: 16
Publisher: ASM International
Published: 01 January 1989
DOI: 10.31399/asm.hb.v16.a0002153
EISBN: 978-1-62708-188-7
..., electrochemical honing, and hone forming. It also examines various process parameters in microhoning and concludes with information on the applications of microhoning. electrochemical honing external honing flat honing gear tooth honing hone forming honing microhoning plateau honing HONING...
Abstract
Honing serves an important purpose of generating specified functional characteristics for surfaces besides removing stock and involves the correction of errors resulting from previous machining operations. This article discusses the process capabilities of honing in terms of bore size, bore shape, and stock removal. It illustrates the uses of air, ring, expanding, plug, and bar gages for automatic size control in power stroking of honing tools. The article provides a short description of various honing processes, such as external honing, gear tooth honing, plateau honing, flat honing, electrochemical honing, and hone forming. It also examines various process parameters in microhoning and concludes with information on the applications of microhoning.
Book: Machining
Series: ASM Handbook
Volume: 16
Publisher: ASM International
Published: 01 January 1989
DOI: 10.31399/asm.hb.v16.a0002164
EISBN: 978-1-62708-188-7
... for cathodes, cathodes, and cathode holder/manifold. The article concludes with information on the process parameters of the STEM system. electrochemical machining fuel nozzles oil passages shaped tube electrolytic machining turbine blades turbine disk cooling passages SHAPED TUBE ELECTROLYTIC...
Abstract
Shaped tube electrolytic machining (STEM) is a modified electrochemical machining (ECM) process that uses an acid electrolyte so that the removed metal goes into the solution instead of forming a precipitate. This article lists some specific machining applications of the STEM process, including turbine blade cooling holes, turbine vane cooling holes, turbine disk cooling passages, oil passages, and fuel nozzles. It describes the limitations and advantages of the STEM process. The article discusses the various tool parts of the STEM system, including the holding fixture, guide for cathodes, cathodes, and cathode holder/manifold. The article concludes with information on the process parameters of the STEM system.
Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003579
EISBN: 978-1-62708-182-5
... Abstract The electrode potential is one of the most important parameters in the thermodynamics and kinetics of corrosion. This article discusses the fundamentals of electrode potentials and illustrates the thermodynamics of chemical equilibria by using the hydrogen potential scale...
Abstract
The electrode potential is one of the most important parameters in the thermodynamics and kinetics of corrosion. This article discusses the fundamentals of electrode potentials and illustrates the thermodynamics of chemical equilibria by using the hydrogen potential scale and the Nernst equation. It describes galvanic cell reactions and corrosion reactions in an aqueous solution in an electrochemical cell. The article explores the most common cathodic reactions encountered in metallic corrosion in aqueous systems. The reactions included are proton reduction, water reduction, reduction of dissolved oxygen, metal ion reduction, and metal deposition. The article also presents the standard equilibrium potentials measured at 25 deg C relative to a standard hydrogen electrode for various metal-ion electrodes in a tabular form.
Series: ASM Handbook
Volume: 2A
Publisher: ASM International
Published: 30 November 2018
DOI: 10.31399/asm.hb.v02a.a0006494
EISBN: 978-1-62708-207-5
.... This article reviews these general machining factors as well as specific cutting tool and cutting parameters for the six basic chip-forming processes of turning, shaping, milling, drilling, sawing, and broaching. Best practices for each of the six chip-forming processes are suggested for optimized machining...
Abstract
The horsepower requirements to cut various metal alloys provide an indication of the relative ease and cost of machining, but several other important factors include cutting tool material, chip formation, cutting fluids, cutting tool wear, surface roughness, and surface integrity. This article reviews these general machining factors as well as specific cutting tool and cutting parameters for the six basic chip-forming processes of turning, shaping, milling, drilling, sawing, and broaching. Best practices for each of the six chip-forming processes are suggested for optimized machining of aluminum alloys. The article lists the inherent disadvantages of machining processes that involve compression/shear chip formation. It discusses the machining of aluminum metal-matrix composites and nontraditional machining of aluminum, such as abrasive jet, waterjet, electrodischarge, plasma arc, electrochemical, and chemical machining.
Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003586
EISBN: 978-1-62708-182-5
... can be used to extract information on the corrosion rate of the electrochemical interface or conversely the reduction-oxidation rate of an interface dominated by redox reactions as well as the Tafel parameters. This is an advantage over linear polarization resistance and EIS methods, which can provide...
Abstract
This article addresses electrochemical methods for instantaneous rate determination and threshold determination as well as nonelectrochemical methods that can determine incremental or cumulative rates of corrosion. Electrochemical methods for the study of galvanic corrosion rates and localized corrosion and evaluation of corrosion rates under paints are also discussed. The article describes nonelectrochemical methods that can determine incremental or cumulative rates of corrosion. Methods presented include polarization methods, polarization resistance methods, electrochemical impedance methods, frequency modulation methods, electrochemical noise resistance, potential probe methods, cyclic potentiodynamic polarization methods, potentiostatic and galvanostatic methods, electrochemical noise (EN) methods, scratch-repassivation method, and electrochemical impedance spectroscopy (EIS) techniques. Gravimetric determination of mass loss, electrical-resistance methods, magnetic methods, quartz crystal microbalance method, solution analysis methods, and metrological methods are nonelectrochemical methods. The article presents an electrochemical test that examines the susceptibility of stainless steel alloys to intergranular corrosion.
Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003599
EISBN: 978-1-62708-182-5
... the electrolyte resistance. Raising the temperature and increasing the concentration of dissolved metal salt can decrease the absolute values of the overpotentials. Typical refining conditions are summarized in Table 3 . Operating parameters in metal electrochemical refining Table 3 Operating parameters...
Abstract
Electrochemical refining is the purification process for producing commercially pure metals from crude metals. This article describes the principles of electrochemical reactions. It discusses the physical properties of the basic components of electrochemical refining cell. The article also explains the engineering considerations required in the refining process. Theoretical and technological principles of electrochemical refining are illustrated, with examples.
Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001296
EISBN: 978-1-62708-170-2
... Polarization resistance measurements Impedance measurements In the first type, different electrical parameters can be present. In the latter type, only system-adjusted values are measured ( Ref 1 , 2 , 7 , 8 , 9 ). All measurements are performed in different electrochemical cells ( Fig. 3...
Abstract
This article focuses on the testing and typical corrosion behavior of coating-substrate systems in aqueous solutions and humid aggressive atmospheres. It includes a short review of the fundamentals of corrosion, followed by a discussion of specific system behavior, electrochemical and laboratory accelerated tests, and simulated service tests. The article also contains examples of different types of corrosion damage and presents guidelines for improving corrosion resistance.
Series: ASM Handbook
Volume: 23
Publisher: ASM International
Published: 01 June 2012
DOI: 10.31399/asm.hb.v23.a0005683
EISBN: 978-1-62708-198-6
... reactions. For every electrochemical reaction, an equilibrium potential, E o (also called the single electrode potential, half-cell potential, reduction potential, or redox potential), can be defined on the basis of the thermodynamic parameters. At this potential, the electrical current densities...
Abstract
The interaction of an implant with the human body environment may result in degradation of the implant, called corrosion. This article discusses the corrosion testing of metallic implants and implant materials. The corrosion environments for medical implants are the extracellular human body fluids, very complex solutions containing electrolytes and nonelectrolytes, inorganic and organic constituents, and gases. The article describes the fundamentals of electrochemical corrosion testing and provides a brief discussion on various types of corrosion tests. It illustrates corrosion current density determination by Tafel extrapolation, potentiodynamic measurement of the polarization resistance, electrochemical impedance measurement, and potentiostatic deaeration. Tests combining corrosion and mechanical forces, such as fretting corrosion tests, environment-assisted cracking tests, and ion-leaching tests are also discussed.
Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003644
EISBN: 978-1-62708-182-5
... commercial software programs contain a number of typical electrochemical tests, such as potentiostatic, potentiodynamic, galvanostatic polarization, and other tests, such as the measurement of the galvanic current, the electrochemical impedance, or ECN. The user can input the particular parameters...
Abstract
This article reviews the fundamentals of electrochemical corrosion test methods. The features and requirements of the instrumentation needed for an electrochemical test are briefly discussed. The article provides a discussion on the various electrochemical techniques and tests available for laboratory studies of corrosion phenomena. The techniques and tests include no-applied-signal tests, small-signal polarization tests, large-signal polarization tests, scanning electrode techniques, and miscellaneous techniques.
Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001233
EISBN: 978-1-62708-170-2
.... Machining parameters: U (in Fig. 2 ) = 17 V; electrolyte pressure, 0.3 MPa; electrolyte, 15% NaCl; time of machining, 75 s; maximum current per piece, 180 A Fig. 7 Tooling for electrochemical machining deburring. (a) Valve casing. (b) A fragmentary schematic of the production jig. Machining...
Abstract
Nontraditional finishing processes include electrochemical machining (ECM), electrodischarge machining (EDM), and laser beam machining. These processes belong to nonabrasive finishing methods where surface generation occurs with an insignificant amount of mechanical interaction between the processing tool and the workpiece surfaces. This article provides information on the equipment used, applications, process capabilities, and limitations of ECM and EDM.
Image
Published: 01 January 1994
Fig. 6 Schematic of electrochemical machining: smoothing, deburring, and radiusing of piston pin. Machining parameters: U (in Fig. 2 ) = 17 V; electrolyte pressure, 0.3 MPa; electrolyte, 15% NaCl; time of machining, 75 s; maximum current per piece, 180 A
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Book: Machining
Series: ASM Handbook
Volume: 16
Publisher: ASM International
Published: 01 January 1989
DOI: 10.31399/asm.hb.v16.a0002160
EISBN: 978-1-62708-188-7
... be tolerated in parts subjected to alternating high stress. Intergranular attack can usually be avoided with proper selection of electrolyte and ECM parameters. Surfaces that have been electrochemically machined have little or no residual stress. When electrochemical machining replaces mechanical machining...
Abstract
Electrochemical machining (ECM) is the controlled removal of metal by anodic dissolution in an electrolytic cell in which the workpiece is the anode and the tool is the cathode. This article begins with a description of the ECM system and then discusses the primary variables that affect current density and the material removal rate in the ECM process. It reviews the various characteristics of electrolytes and considers tool material and design. It also provides an overview of the properties of the workpiece and defines the surface finish and accuracy of an electrochemically machined sample. The variety of work done by electrochemical machining is also exemplified in the article.
Series: ASM Handbook
Volume: 13A
Publisher: ASM International
Published: 01 January 2003
DOI: 10.31399/asm.hb.v13a.a0003656
EISBN: 978-1-62708-182-5
... of the current signals measured from the different electrodes is an indication of the degree of variations in the electrochemical properties among the electrodes, it may be used as an effective single-parameter indicator for localized corrosion. Figure 6 shows typical responses of the dispersion of the current...
Abstract
This article provides a discussion on the operation of various methods and sensors that have been used or have the potential to be used for on-line, real-time monitoring of localized corrosion. These include the electrochemical noise (ECN) method, nonelectrochemical methods, the galvanically coupled differential flow cell, galvanically coupled crevice cell, coupled multielectrode sensor, and electrochemical biofilm activity sensor.
Image
Published: 01 January 1994
Fig. 7 Tooling for electrochemical machining deburring. (a) Valve casing. (b) A fragmentary schematic of the production jig. Machining parameters: 15% water solution of NaNO 3 ; U (in Fig. 2 ) = 15 V; machining time, 8 s; electrolyte pressure, 1 MPa; maximum current per piece, 20 A
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