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Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006097
EISBN: 978-1-62708-175-7
... the influence of compaction characteristics of stainless steel powders in tool materials selection, lubrication, annealing, double pressing/double sintering, and warm compaction. annealing apparent density compressibility double sintering flow rate green density green strength lubrication metal...
Abstract
This article provides an overview of the compaction of metal powder in a rigid die and reviews the compaction characteristics of stainless steel powders, including green density, compressibility, green strength, apparent density, flow rate, and sintered density. It describes the influence of compaction characteristics of stainless steel powders in tool materials selection, lubrication, annealing, double pressing/double sintering, and warm compaction.
Image
Published: 30 September 2015
Fig. 1 Nominal density levels achieved for AISI 4640 high-strength, low-alloy (HSLA) powder metallurgy (PM) steel using various PM consolidation processes. Hot isostatic pressing (HIP) achieves true pore-free material from powder. HT, high-temperature; DP-DS, double-press, double-sinter
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Book: Fatigue and Fracture
Series: ASM Handbook
Volume: 19
Publisher: ASM International
Published: 01 January 1996
DOI: 10.31399/asm.hb.v19.a0002374
EISBN: 978-1-62708-193-1
... °C, 3 h, 200 MPa 4.46 Axial R = −1 475 P+S, pressed and sintered; PIM, powder injection molded and sintered; HIP, hot isostatically pressed; HT, heat treated; SP, shot peened; DP + DS, double pressed and double sintered; PF, powder forged Fracture studies of P/M alloys are usually...
Abstract
This article discusses the fracture and fatigue properties of powder metallurgy (P/M) materials depending on the microstructure. It describes the effects of porosity on the P/M processes relevant to fatigue and fracture resistance. The article details the factors determining fatigue and fracture resistance of P/M materials. It reviews the methods employed to improve fatigue and fracture resistance, including carbonitriding, surface strengthening and sealing treatments, shot-peening, case hardening, repressing and resintering, coining, sizing, and postsintering heat treatments. Safety factors for P/M materials are also detailed.
Series: ASM Handbook
Volume: 20
Publisher: ASM International
Published: 01 January 1997
DOI: 10.31399/asm.hb.v20.a0002486
EISBN: 978-1-62708-194-8
... Copper infiltrated 7.3–7.5 3.50–3.55 Warm formed 7.2–7.4 3.10–3.30 Double pressed and sintered 7.2–7.4 4.00–4.10 Metal injection molded 7.5–7.6 45.0–70.0 Hot forged 7.8 5.00–5.50 Double press and sinter + HIP 7.87 6.00–7.00 (a) These numbers are only averages; smaller...
Abstract
This article begins with a discussion on general powder metallurgy design considerations that assist in the selection of the appropriate processing method. It reviews powder processing techniques, conventional press-and-sinter methods, and full-density processes to understand the design restrictions of each powder processing method. The article provides comparison of powder processing methods based on their similarities, differences, advantages, and disadvantages. It concludes with a discussion on design issues for the components of powder processing technologies.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003112
EISBN: 978-1-62708-199-3
... compaction can increase density levels to 7.2 g/cm 3 to slightly more than 7.4 g/cm 3 (about 95% of theoretical density). High-temperature sintering also produces higher densities. Secondary processes, such as infiltration or double-pressing/double-sintering, can be used to increase densities to levels...
Abstract
Iron powders are the most widely used powder metallurgy (P/M) material for structural parts. This article reviews low to medium density iron and low-alloy steel parts produced by the pressing and sintering technology. It explains different powder production methods, including Hoeganaes process, Pyron process, atomization of liquid metal, thermal decomposition and the electrodeposition process for carbonyl and electrolytic iron powders. It describes the types of compaction and sintering, explaining their effects of processing with designations. Further, the article deals with the mechanical and physical properties of ferrous P/M materials, which may depend on certain factors, namely microstructure, porosity, density, infiltration, re-pressing, chemical composition, and heat treatment.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006076
EISBN: 978-1-62708-175-7
... modified, economical press and sinter technique ( Ref 3 ). Higher-density PM parts are also produced using the double-press, double-sinter technique, but production costs are increased. A substantially pore-free material is produced using molten metal infiltration. In the process, a porous metallic...
Abstract
The two most important classes of materials that are manufactured via infiltration methods are copper- and silver-infiltrated refractory metals and refractory carbides, and copper-infiltrated steels. This article focuses on copper-infiltrated steels and discusses the basic requirements for infiltration, which is a technique that is only applicable to material systems that meet certain requirements. It addresses these requirements and describes the conventional (partial) infiltration process of powder metallurgy (PM) steel. The materials used in the process, such as matrix and infiltrant, are discussed. The article also details several criteria used to evaluate the performance of an infiltration process. It concludes with information on alloy steels and fully infiltrated steels.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006083
EISBN: 978-1-62708-175-7
... Abstract Warm compaction uses both powder heating and die heating to effect higher component densities, whereas warm die compaction uses only die heating to achieve higher density. This article explains the influences of green and sintered properties and pore-free density during compaction...
Abstract
Warm compaction uses both powder heating and die heating to effect higher component densities, whereas warm die compaction uses only die heating to achieve higher density. This article explains the influences of green and sintered properties and pore-free density during compaction of materials. It provides information on the concept of pore-free density and process considerations: die heating and powder heating. The article concludes with a review of the tooling design for warm compaction.
Image
Published: 15 June 2020
Fig. 15 ZrO 2 gear with double-sided grooves fabricated using polycaprolactone (PCL) support material: (a) cross section of CAD model, (b) sintered part. Source: Ref 63
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Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006081
EISBN: 978-1-62708-175-7
... for the production of high-density, high-strength PM components through double pressing/double sintering and heat treatment. Grade JIP 4100V powder achieves a green density of 7.05 g/cm 3 (0.255 lb/in. 3 ) at a compaction pressure of 690 MPa (100 ksi). This is attributed to the low oxygen, carbon, and nitrogen...
Abstract
This article briefly reviews the production methods and characteristics of plain carbon and low-alloy water-atomized iron and steel powders, high-porosity iron powder, carbonyl iron powder, and electrolytic iron powder. It emphasizes on atomized powders, because they are the most widely used materials for ferrous powder metallurgy. The article provides information on the properties and applications of these powders. It also includes an overview of diffusion alloying, basics of admixing, and bonded premixes.
Book: Corrosion: Materials
Series: ASM Handbook
Volume: 13B
Publisher: ASM International
Published: 01 January 2005
DOI: 10.31399/asm.hb.v13b.a0003835
EISBN: 978-1-62708-183-2
... on the corrosion resistance of P/M stainless steels. The approaches used to improve the corrosion resistance of sintered stainless steels are discussed briefly. The article also presents a discussion on the manufacturing and corrosion characteristics of P/M superalloys. corrosion resistance powder...
Abstract
This article provides a detailed discussion on the most commonly employed tests and specific examples of the use of these tests in evaluating the corrosion resistance of powder metallurgy (P/M) stainless steels. It describes the influence of various processing parameters on the corrosion resistance of P/M stainless steels. The approaches used to improve the corrosion resistance of sintered stainless steels are discussed briefly. The article also presents a discussion on the manufacturing and corrosion characteristics of P/M superalloys.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003185
EISBN: 978-1-62708-199-3
... using the same processing equipment dimensional change The shrinkage or growth of a part as a result of sintering double-action pressing Method by which a powder is pressed in a die between two punches moving from opposite directions into the die cavity flow rate The time...
Abstract
This article focuses on the significant fundamental powder characteristics, which include particle size, particle size distribution, particle shape, and powder purity, followed by an overview of general and individual powder production processes such as mechanical, chemical, electrochemical, atomizing, oxide reduction, and thermal decomposition processes. It also covers the consolidation of powders by pressing and sintering, as well as by high density methods. Further emphasis is provided on the distinguishing features of powders, their manufacturing processes, compacting processes, and consolidated part properties. In addition, a glossary of powder metallurgy terms is included.
Series: ASM Handbook
Volume: 4C
Publisher: ASM International
Published: 09 June 2014
DOI: 10.31399/asm.hb.v04c.a0005902
EISBN: 978-1-62708-167-2
... cracks in the refractory lining and of achieving even sintering over the whole channel length. Fig. 12 Single-loop inductor for cast iron. Courtesy of ABP Induction Systems In contrast, double-loop channel inductors ( Fig. 13 ) are used primarily for melting and holding nonferrous metals...
Abstract
An induction channel furnace consists of a tiltable furnace vessel with refractory lining onto which an inductor or several inductors are flange mounted. This article includes a discussion on the design for holding and dosed-pouring of the iron melts, design for melting the materials, and refractory lining of furnace vessel. It provides information on the structural changes and refractory lining of channel inductors. The article also includes a discussion on power supplies deployed in channel inductor furnaces: line-frequency power supply for melting iron, and converter power supply for melting nonferrous metals. It concludes with an overview of the inductor cooling circuit.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006022
EISBN: 978-1-62708-175-7
... hardened during the sinter-brazing phase and has a density of 7.0 g/cm 3 . The assembly also has a doubled-pressed and double-sintered cam plate made to 7.3 g/cm 3 density with an ultimate tensile strength of 1170 MPa (170 ksi) and a mean tempered hardness exceeding 40 HRC. To form the parts and maintain...
Abstract
This article reviews various segments of the powder metallurgy (PM) process from powder production and powder processing through the characterization of the materials and their properties. It covers the processing methods for consolidating metal powders including options for processing to full density. The article outlines the freeform fabrication process, also known as additive manufacturing and describes finishing operations of PM parts. It concludes with information on the applications of PM parts.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006101
EISBN: 978-1-62708-175-7
... of the infiltrant slug is calculated to fill the surface-connected, interconnected pore volume of the compact. The infiltration process can be either a single step or double step. In the single-step process, parts are infiltrated at the same time as they are sintered. It is extremely important for the green compact...
Abstract
This article summarizes the general classification, mechanical properties, and applications of ferrous powder metallurgy (PM) materials for parts production. It discusses four principal ferrous PM alloy types: admixed elemental alloys, diffusion alloys, prealloys, and hybrid alloys. The article reviews the benefits and disadvantages as well as the effect of processing on the properties and material microstructure of these alloys. It contains tables that list the mechanical properties of various iron-copper and copper steels.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006080
EISBN: 978-1-62708-175-7
... ( Ref 2 ). Powder characteristics, such as size and shape, are unimportant in the forging deformation process itself, but they may have important effects on the compaction and sintering processes prior to forging. For example, whether the powders are spherical or irregularly shaped, fine or coarse...
Abstract
Successful application of forging and hot pressing involves careful consideration of powder preparation and forming process parameters. This article describes the important process features for powder forging and hot pressing, along with specific applications and materials used.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006074
EISBN: 978-1-62708-175-7
... Molded parts are designated as being in the “green” or unsintered state following common terminology used for die-compacted metal powder parts. The usual next step is sintering to increase density to a maximum value close to theoretical or to a designed lower value for intentionally porous structures...
Abstract
This article describes the unique aspects of cold isostatic pressing (CIP) in comparison with die compaction, for powder metallurgy parts. It details the components of CIP equipment, including pressure vessels, pressure generators, and tooling material. The article reviews the part shapes and their influence in determining tap density of the filled mold. It provides a discussion on process parameters, such as dwell time, depressurization rate, evaluation of green strength and density, and thermal processing, and illustrates a process flowchart for the production of CIP parts.
Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003789
EISBN: 978-1-62708-177-1
... equipment and techniques and provides data on etchants and etching procedures. specimen grinding liquid-phase sintering macroexamination metallographic examination microstructure particle size analysis powder metallurgy alloys particle shape analysis specimen polishing specimen preparation...
Abstract
This article provides information on the microstructure of powder metal alloys and the special handling requirements of porous materials. It covers selection, sectioning, mounting, grinding, and polishing, and describes procedures, such as washing, liquid removal, and impregnation, meant to preserve pore structures and keep them open for analysis. The article compares and contrasts the microstructures of nearly 50 powder metal alloys, using them to illustrate the effect of consolidation and compaction methods as well as particle size, composition, and shape. It discusses imaging equipment and techniques and provides data on etchants and etching procedures.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006034
EISBN: 978-1-62708-175-7
... characteristics History of development in PM presses Table 1 History of development in PM presses Years Compacting press 1955–1959 Cam press, HP 1960–1964 Toggle press, MP 1965–1969 Large size HP (500 +), large size MP (500 +) 1970–1974 Multistepped MP, double die compacting press...
Abstract
Powder metallurgy compacting presses usually are mechanically or hydraulically driven, but they can incorporate a combination of mechanically, hydraulically, and pneumatically driven systems. This article provides a comparison of mechanical and hydraulic presses based on the cost, production rate, and machine overload protection. The article lists the classification of powder metallurgy parts based on complexity of shapes as suggested by the Metal Powder Industries Federation, such as Class I parts, Class II parts, Class III parts, and Class IV parts. It describes rigid tooling compaction and details the powder-fill ratio considerations for these classes. The article elaborates on the types of tooling systems and presses used for these classes. Some important factors and components used in designing a tool are also described. Finally, the article considers tool materials, including punches, core rods, and punch clamp rings.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006095
EISBN: 978-1-62708-175-7
... for Ti-6Al-4V alloy show that as densification approaches theoretical maximum values, the powder-based titanium alloys with optimized chemical composition (in terms of oxygen, hydrogen, and chlorine) can match both the static as well as fatigue properties of wrought ingot-based double-arc-remelt Ti-6Al...
Abstract
This article focuses on mechanical testing characterization of blended elemental powder metallurgy (PM) titanium alloys and prealloyed PM titanium alloys. It examines the tensile properties, fracture toughness, stress-corrosion threshold resistance, fatigue strength, crack propagation properties, and processing-microstructure-property relationships of these alloys. The article also reviews five considerations for powder process selection.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006110
EISBN: 978-1-62708-175-7
... was performed in a nitrogen-backfilled vacuum furnace. Tensile and yield strengths showed marked increases in the high-temperature sintered materials, with the elongation and impact energy at least doubling for both materials. The sintered density of the belt-sintered samples, though not reported, can...
Abstract
High-temperature sintering of ferrous components continues to be important in the powder metallurgy (PM) industry. Improvements in both production rates and properties are possible as sintering temperatures increase above 1120 deg C. This article provides an overview of the different various stages of the sintering process and the physical, chemical, and metallurgical phenomena occur within the mass of metal powder particles. It discusses the four advantages of high-temperature sintering of various ferrous PM materials: improved mechanical properties, improved physical properties, development of liquid phase, and ability to sinter active elements in alloy steels. The article also provides information on three sources of process control requirements, namely, the powder blend, green density, and sintering conditions.
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