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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003788
EISBN: 978-1-62708-177-1
.... The article also illustrates the microstructure of different types of soft magnetic material and permanent magnets. bitter technique domain imaging Faraday method Lorentz transmission electron microscopy magnetic force microscopy magnetic materials magnetism magneto-optical Kerr method materials...
Abstract
Microstructural analysis of specialized types of magnetic materials is centered on the examination of optical, electron, and scanning probe metallographic techniques unique to magnetic materials. This article provides a comprehensive overview of magnetic materials, their characteristics and sample preparation procedures. It reviews the methods pertaining to the microstructural examination of bulk magnetic materials, including microscopy techniques specified to magnetic materials characterization, with specific examples. The techniques used in the study of magnetic domain structures (microstructure) include the magneto-optical Kerr method, the Faraday method, the Bitter technique, scanning electron microscopy (magnetic contrast Types I and II), scanning electron microscopy with polarization analysis, Lorentz transmission electron microscopy, and magnetic force microscopy. The article also illustrates the microstructure of different types of soft magnetic material and permanent magnets.
Image
Published: 01 December 2004
Fig. 21 Domain imaging using the Faraday effect for a Gd 0.94 Tb 0.75 Er 1.31 Al 0.5 Fe 4.5 O 12 garnet crystal, grown in a PbO and B 2 O 3 flux at 1300 °C (2370 °F). (a) Magnetic domain structure of 50 μm thick platelet cut parallel to the (111) plane. Black and white areas represent
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Image
Published: 01 December 2004
Fig. 16 Basic imaging of domain walls by the Bitter technique for samples with strain free surfaces is shown in this line drawing. (a) Ferrofluid particles collect at domain walls due to the fringe field associated with the magnetization rotation through the wall width and the particle
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Image
Published: 01 December 2004
Fig. 15 Bitter domain images of a nickel-cobalt single crystal thick film using dark-field imaging and a microscope with attached field coils. (a) Demagnetized sample with no applied field showing the closure domains. (b) An applied field of 3.6 Oe to the right makes the domain walls
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Image
Published: 01 December 2004
Fig. 22 Domain images of a barium ferrite single crystal (85 μm thick) with hexagonal plane normal to the plane of the sample. (a) Faraday effect image showing the characteristic domain structure throughout the thickness of the sample. (b) Bitter pattern of the same area as (a), indicating
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Image
Published: 01 December 2004
Fig. 36 Comparison of Kerr microscopy domain image (a) with magnetic force microscopy images (c) and (d) for a “fir-tree” domain structure, typical of slight misorientation from the (100) surface of an αFe whisker. (b) Indicates the direction of the magnetization for each of the chevrons
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Image
Published: 01 December 2004
of polarization rotation upon reflection. (b) Adjusting the analyzer for maximum contrast provides a domain image with light/dark contrast for magnetization in the up/down orientations, respectively.
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Image
Published: 01 December 2004
Fig. 32 A ray diagram for the Fresnel imaging of magnetic domains using a transmission electron microscope. (a) When the current to the objective lens is increased above the in-focus condition, the image becomes overfocused and the electrons are deflected toward and away from the domain walls
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Image
Published: 01 December 2004
Fig. 33 A ray diagram illustrating the Foucault imaging of magnetic domains using a transmission electron microscope. The Lorentz force on the electrons passing through the magnetic material causes a deflection of their trajectory. A displacement of the objective aperture allows the electrons
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Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001767
EISBN: 978-1-62708-178-8
... of the instrumentation and principles of SEM, broadly explaining its capabilities in resolution and depth of field imaging. It describes three additional functions of SEM, including the use of channeling patterns to evaluate the crystallographic orientation of micron-sized regions; use of backscattered detectors...
Abstract
Scanning electron microscopy (SEM) has shown various significant improvements since it first became available in 1965. These improvements include enhanced resolution, dependability, ease of operation, and reduction in size and cost. This article provides a detailed account of the instrumentation and principles of SEM, broadly explaining its capabilities in resolution and depth of field imaging. It describes three additional functions of SEM, including the use of channeling patterns to evaluate the crystallographic orientation of micron-sized regions; use of backscattered detectors to reveal grain boundaries on unetched samples and domain boundaries in ferromagnetic alloys; and the use of voltage contrast, electron beam-induced currents, and cathodoluminescence for the characterization and failure analysis of semiconductor devices. The article compares the features of SEM with that of scanning Auger microscopes, and lists the applications and limitations of SEM.
Book Chapter
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006474
EISBN: 978-1-62708-190-0
.... acoustical holography liquid-surface acoustical holography optical holography scanning acoustical holography sleeve-bearing stock through-transmission breast imaging system ACOUSTICAL HOLOGRAPHY is the extension of holography into the ultrasonic domain. The principles of acoustical holography...
Abstract
Acoustical holography is the extension of holography into the ultrasonic domain. The basic systems for acoustical holography are the liquid-surface type and the scanning type. This article discusses the applications for acoustical holography, including inspection of large composite parts, through-transmission breast imaging system, inspection of welds in thick materials, and inspection of sleeve-bearing stock. It describes the basic system for liquid-surface acoustical holography and scanning acoustical holography. A comparison between these techniques is also provided.
Image
Published: 01 December 2004
to the right and black to the left. (c) Image of the y-component of the magnetization (white contrast upward and black contrast downward). (d) Total in-plane magnetization intensity, with image contrast at the domain walls due to larger probe diameter than the domain wall width. Reproduced with permission from
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Image
Published: 15 December 2019
Fig. 19 (a) 1 × 1 μm phase image of styrene-ethylene/butylene- styrene polymer. (b) Corresponding topography image. Although the existence of the two domains is observed in (b), the different blocks are more clearly differentiated in (a), enabling a clearer understanding of the morphology
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Image
Published: 01 December 2004
Fig. 34 Transmission electron micrographs of Fe-55Pd arc-melted alloy annealed at 500 °C (930 °F) for 36 h. (a) Bright-field image of the sample (with [130] zone axis) exhibiting a polytwinned microstructure. (b) Lorentz under-focus (Fresnel) image of the sample showing the immobile domain
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Image
Published: 01 December 2004
of the sample. The resulting SE image has contrast variation across the width of the domain with peak brightness and darkness at the domain walls.
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Image
Published: 01 December 2004
Fig. 28 Secondary electron image of a Nd 2 Fe 14 B single crystal grown using flux growth synthesis. Type I magnetic contrast clearly shows the maze pattern domains, typical of these uniaxial materials. The large depth of field, characteristic of scanning electron imaging techniques
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Image
Published: 01 December 2004
Fig. 18 As-cast Fe 80 B 18.3 P 1.7 metallic glass alloy. Complex magnetic domain structure resulting from the residual stress pattern due to rapid-solidification processing. Dark-field imaging and the Bitter powder pattern technique were used to produce this image. Reproduced with permission
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Published: 01 January 1997
Fig. 6 Topology optimization examples of a frame structure. (a) Initial frame structure showing design domain. (b) First three natural mode shapes. (c) Optimal material distribution from topology optimization as computed and after filtering the topology image to simplify the structural layout
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in Computational Models for Prediction of Solidification Microstructure
> Cast Iron Science and Technology
Published: 31 August 2017
Fig. 15 Three-dimensional (3-D) simulated microstructure evolution during divorced eutectic solidification of a spheroidal graphite iron. (a) Solid fraction ( f s ) = 0.24. (b) f s = 0.55. (c) f s = 0.99. (Images taken at the center of a 3-D calculation domain). Source: Ref 63
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Image
in Formation of Microstructures, Grain Textures, and Defects during Solidification
> Metals Process Simulation
Published: 01 November 2010
Fig. 13 (a) Image of a cellular automaton simulation of solidification in a Zn-0.2wt%Al galvanized coating. The 5 by 3 mm domain is cooled at –12 K/s with a positive temperature gradient from left to right. (b) Experimental and calculated number densities of grains as a function of the cooling
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