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differential scanning calorimetry
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Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006672
EISBN: 978-1-62708-213-6
... Abstract Differential scanning calorimetry (DSC) is the most common thermal technique for polymer characterization. This article provides a detailed account of the various factors and processes involved in DSC. The discussion covers the equipment used, specimen preparation process, calibration...
Abstract
Differential scanning calorimetry (DSC) is the most common thermal technique for polymer characterization. This article provides a detailed account of the various factors and processes involved in DSC. The discussion covers the equipment used, specimen preparation process, calibration requirements, data analysis, and provides examples of the applications and interpretation of DSC.
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Published: 01 June 2016
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Published: 01 June 2016
Fig. 21 Differential scanning calorimetry examination of quench-rate effects in 7075 at different distances (mm) from the quenched end of a Jominy end-quench specimen. GP, Guinier-Preston. Source: Ref 32
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Published: 01 June 2016
Fig. 3 Differential scanning calorimetry trace of alloy Al-0.6Mg-0.8Si started directly after quenching. The heating rate is 10 K/s. GP, Guinier-Preston. Adapted from Ref 7
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Published: 01 June 2016
Fig. 45 Differential scanning calorimetry examination of quench-rate effects in 7075 at different distances (mm) from the quenched end of a Jominy end quench specimen. Source: Ref 57
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Published: 30 September 2015
Fig. 21 Differential scanning calorimetry plot with an exothermic crystallization event and an endothermic melting event. Courtesy of KTA-Tator, Inc.
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Published: 30 September 2015
Fig. 22 Differential scanning calorimetry spectrum of metallic zinc control revealing peak area of metallic zinc of 108 J/g. Courtesy of KTA-Tator, Inc.
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Published: 30 September 2015
Fig. 23 Differential scanning calorimetry spectrum revealing sample peak area of metallic zinc of 98.0 J/g. Courtesy of KTA-Tator, Inc.
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Published: 30 September 2015
Fig. 24 Differential scanning calorimetry spectrum revealing partially cured coating. Courtesy of KTA-Tator, Inc.
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Published: 30 September 2015
Fig. 25 Differential scanning calorimetry spectrum revealing the original sample reheated under the same conditions. Courtesy of KTA-Tator, Inc.
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Published: 01 January 2001
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Published: 15 June 2020
Fig. 10 Differential scanning calorimetry traces of Cu-11.85Al-3.2Ni-3Mn and Cu-11.35Al-3.2Ni-3Mn-0.5Zr for both laser powder-bed fusion (LPBF) and suction-cast (SC) specimens. Source: Ref 104
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Published: 15 December 2019
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Published: 15 December 2019
Fig. 2 Differential scanning calorimetry thermogram showing various transitions associated with polymeric materials. The (I) indicates that the numerical temperature was determined as the inflection point on the curve. Source: Ref 6
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Published: 15 December 2019
Fig. 4 Modulated differential scanning calorimetry separation of glass transition temperature ( T g ) from enthalpic relaxation. Upper curve: T g ; lower curve: enthalpic relaxation. The (I) indicates that the numerical temperature was determined as the inflection point on the curve. Source
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Published: 15 December 2019
Fig. 5 Differential scanning calorimetry used to identify polymeric materials by determination of their melting point. Source: Ref 6
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Published: 15 December 2019
Fig. 6 Differential scanning calorimetry used to detect glass transitions within amorphous thermoplastic resins. The (I) indicates that the numerical temperature was determined as the inflection point on the curve. Source: Ref 6
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Published: 15 December 2019
Fig. 7 Differential scanning calorimetry thermogram representing the reference clip material, exhibiting an endothermic transition characteristic of the melting of a nylon 6/6 resin. The results also showed a second melting transition attributed to a hydrocarbon-based impact modifier. Source
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Published: 15 December 2019
Fig. 8 Differential scanning calorimetry thermogram representing a molding resin pellet that had produced brittle parts. The thermogram shows a major melting transition associated with nylon 6/12 and a weaker transition attributed to polypropylene. Source: Ref 6
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Published: 15 December 2019
Fig. 9 Differential scanning calorimetry thermogram representing a molding resin pellet that had produced brittle parts. The thermogram shows a major melting transition associated with nylon 6/12 and a weaker transition attributed to polypropylene. Source: Ref 6
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