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differential scanning calorimetry
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Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006672
EISBN: 978-1-62708-213-6
... Abstract Differential scanning calorimetry (DSC) is the most common thermal technique for polymer characterization. This article provides a detailed account of the various factors and processes involved in DSC. The discussion covers the equipment used, specimen preparation process, calibration...
Abstract
Differential scanning calorimetry (DSC) is the most common thermal technique for polymer characterization. This article provides a detailed account of the various factors and processes involved in DSC. The discussion covers the equipment used, specimen preparation process, calibration requirements, data analysis, and provides examples of the applications and interpretation of DSC.
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Published: 01 June 2016
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Published: 01 June 2016
Fig. 45 Differential scanning calorimetry examination of quench-rate effects in 7075 at different distances (mm) from the quenched end of a Jominy end quench specimen. Source: Ref 57
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Published: 01 June 2016
Fig. 21 Differential scanning calorimetry examination of quench-rate effects in 7075 at different distances (mm) from the quenched end of a Jominy end-quench specimen. GP, Guinier-Preston. Source: Ref 32
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Published: 01 June 2016
Fig. 3 Differential scanning calorimetry trace of alloy Al-0.6Mg-0.8Si started directly after quenching. The heating rate is 10 K/s. GP, Guinier-Preston. Adapted from Ref 7
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Published: 30 September 2015
Fig. 21 Differential scanning calorimetry plot with an exothermic crystallization event and an endothermic melting event. Courtesy of KTA-Tator, Inc.
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Published: 30 September 2015
Fig. 22 Differential scanning calorimetry spectrum of metallic zinc control revealing peak area of metallic zinc of 108 J/g. Courtesy of KTA-Tator, Inc.
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Published: 30 September 2015
Fig. 23 Differential scanning calorimetry spectrum revealing sample peak area of metallic zinc of 98.0 J/g. Courtesy of KTA-Tator, Inc.
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Published: 30 September 2015
Fig. 24 Differential scanning calorimetry spectrum revealing partially cured coating. Courtesy of KTA-Tator, Inc.
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Published: 30 September 2015
Fig. 25 Differential scanning calorimetry spectrum revealing the original sample reheated under the same conditions. Courtesy of KTA-Tator, Inc.
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Published: 01 November 1995
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Published: 01 November 1995
Fig. 6 Differential scanning calorimetry thermogram of polyethylene/polypropylene blend, 10 mcal/s range, 20 °C (36 °F)/min heating rate. PE, polyethylene; PP, polypropylene. Source: Ref 56
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Published: 01 November 1995
Fig. 7 Differential scanning calorimetry determination of the effect of a plasticizer on T m of nylon 11. Range, 0.0024 W (10 mcal/s); heating rate, 20 °C/min (36 °F/min); weight, 6.8 mg (0.105 gr), both samples. Source: Ref 51
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Published: 01 November 1995
Fig. 8 Differential scanning calorimetry determination of polyethylene in impact polycarbonate. Range, 0.00048 W (2 mcal/s; heating rate, 20 °C/min (36 °F/min); weight, 23 mg (0.355 gr). Source: Ref 51
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Published: 01 November 1995
Fig. 10 Differential scanning calorimetry thermogram of Fiberite 934 epoxy, 4.89 mg (0.075 gr), 10 °C/min (18 °F/min) heating rate
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Published: 01 January 2001
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Published: 01 January 2005
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Published: 01 January 2005
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Published: 01 January 2002
Fig. 5 Differential scanning calorimetry thermogram showing various transitions associated with polymeric materials. The (I) indicates that the numerical temperature was determined as the inflection point on the curve.
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Published: 01 January 2002
Fig. 6 Differential scanning calorimetry used to identify polymeric materials by determination of their melting point.
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