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differential scanning calorimetry

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Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006672
EISBN: 978-1-62708-213-6
... Abstract Differential scanning calorimetry (DSC) is the most common thermal technique for polymer characterization. This article provides a detailed account of the various factors and processes involved in DSC. The discussion covers the equipment used, specimen preparation process, calibration...
Series: ASM Handbook
Volume: 22B
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.hb.v22b.a0005514
EISBN: 978-1-62708-197-9
... commercial alloys, including adiabatic calorimetry, modulated calorimetry, Calvet calorimetry, single-pan calorimetry, and drop calorimetry. It describes differential scanning calorimetry and differential temperature analysis for measuring transition temperatures such as phase transformation or glass...
Series: ASM Handbook
Volume: 5B
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v05b.a0006063
EISBN: 978-1-62708-172-6
... environments for coating failure analysis. chromatography differential scanning calorimetry electrochemical impedance spectroscopy Fourier transform infrared spectroscopy laboratory corrosion testing microscopic visual examination scanning electron microscopy-energy dispersive X-ray spectroscopy...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003525
EISBN: 978-1-62708-180-1
... Abstract This article reviews the analytical techniques most commonly used in plastic component failure analysis. These include the Fourier transform infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, thermomechanical analysis, and dynamic mechanical analysis...
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003023
EISBN: 978-1-62708-200-6
... g , SAN 430 8.0 422 790 4 Nylon 6 16 183 360 155 310 T m 160 3.0 439 820 1.2 Nylon 6/6 15 218 425 165 330 T m 110 2.1 433 810 2.4 PET 18 151 305 130 265 T g 40 0.7 517 960 28.3 DSC, differential scanning calorimetry; TMA, thermomechanical...
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003465
EISBN: 978-1-62708-195-5
...; frequency: 10, 30, 100 kHz Abstract Abstract This article focuses on various thermal analysis techniques used to verify the cure of a polymer composite. The techniques include differential scanning calorimetry (DSC), modulated DSC, thermomechanical analysis, dynamic mechanical analysis...
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006673
EISBN: 978-1-62708-213-6
... to understand the changes in the sample. For this reason, TGA and other techniques are often combined. For instance, on its own, differential scanning calorimetry (DSC) calculates the difference in heat flow between a sample and an inert reference substance, from which the glass transition temperature...
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005240
EISBN: 978-1-62708-187-0
.... , and Waseda Y. , A High-Temperature System Based on the Laser Flash Method to Measure the Thermal Diffusivity of Melts , Int. J. Thermophys. , Vol 17 ( No. 1 ), 1996 , p 253 – 261 44. Höhne G. , Hemminger W. , and Flammershein H.-J. , Differential Scanning Calorimetry...
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003442
EISBN: 978-1-62708-195-5
... Fig. 1 Heat flow vs. temperature. Glass transition temperature, T g , is determined by differential scanning calorimetry. Glass transition is marked by a change in heat capacity. Glass transition temperature is characterized as being the midpoint of the transition range. Source: MIL- HDBK-17...
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003467
EISBN: 978-1-62708-195-5
... °F), which is slightly on the low side for a 120 °C (250 °F) carbon/epoxy system. Differential scanning calorimetry did not reveal any exothermic reactions, indicating a full cure of the composite spar. Further fractographic examination of several interlaminar fracture surfaces revealed evidence...
Series: ASM Handbook
Volume: 22B
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.hb.v22b.a0005523
EISBN: 978-1-62708-197-9
... Flash Method to Measure the Thermal Diffusivity of Melts , Int. J. Thermophys. , Vol 17 ( No. 1 ), 1996 , p 253 – 261 42. Höhne G. , Hemminger W. , and Flammershein H.-J. , Differential Scanning Calorimetry. An Introduction to Practitioners , Springer-Verlag , Berlin...
Series: ASM Handbook
Volume: 14A
Publisher: ASM International
Published: 01 January 2005
DOI: 10.31399/asm.hb.v14a.a0009013
EISBN: 978-1-62708-185-6
.... The specific heat influences the rate of cooling and heating of the workpiece and how much the temperature changes with local heating by deformation and friction. The two most common methods of measuring specific heat are differential thermal analysis (DTA) and differential scanning calorimetry (DSC...
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003460
EISBN: 978-1-62708-195-5
... analysis techniques, such as differential scanning calorimetry, thermomechanical analyses, dynamic mechanical analysis, and dielectric analysis, are generally used for determining the prior processing history, thermal exposure, and environmental service history. These analyses are used to help define...
Series: ASM Handbook
Volume: 24
Publisher: ASM International
Published: 15 June 2020
DOI: 10.31399/asm.hb.v24.a0006546
EISBN: 978-1-62708-290-7
... scanning calorimetry melt peaks for the part and for virgin powder. Source: Ref 14 Fig. 11 Effect of degree of particle melting (DMP) on ductility of polyamide 12 parts. ▘ = differential scanning calorimetry method; ● = optical microscopy method. Source: Ref 15 Fig. 14 Part shape...
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003462
EISBN: 978-1-62708-195-5
... analysis (TMA) trace of a carbon/bismaleimide composite Fig. 6 Differential scanning calorimetry (DSC) trace of an undercured boron/epoxy laminate Fig. 7 Micrograph of a cross section obtained from a carbon/epoxy, resin transfer molded component Abstract Abstract This article...
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.9781627081801
EISBN: 978-1-62708-180-1
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006272
EISBN: 978-1-62708-169-6
... (0.3 in.), (b) 24 mm (1.0 in.), (c) 56 mm (2.2 in.), and (d) 79 mm (3.1 in.). Source: Ref 32 Fig. 21 Differential scanning calorimetry examination of quench-rate effects in 7075 at different distances (mm) from the quenched end of a Jominy end-quench specimen. GP, Guinier-Preston. Source...
Series: ASM Handbook
Volume: 5A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v05a.a0005749
EISBN: 978-1-62708-171-9
... and VHN DR deposition rate DSC differential scanning calorimetry DTA differential thermal analysis DVS Deutschen Verband für Schweiss-technik e.V. (German Welding Society) EAW electric arc wire (spray) EB electron beam EB-PVD electron beam-physical vapor...
Series: ASM Handbook
Volume: 14A
Publisher: ASM International
Published: 01 January 2005
DOI: 10.31399/asm.hb.v14a.a0004025
EISBN: 978-1-62708-185-6
... and heating of the workpiece, and how much its temperature changes with local heating by deformation and friction. The two most common methods of measuring specific heat are differential thermal analysis (DTA) and differential scanning calorimetry (DSC). Figure 14 shows a DTA cell, in which a specimen (S...
Series: ASM Handbook
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003441
EISBN: 978-1-62708-195-5
... chromatography; GPC, gel permeation chromatography; RDS, rheometric dynamic scanning; DSC, differential scanning calorimetry; ARC, accelerated rate calorimeter; TGA, thermogravimetric analysis Comparison of instrumental techniques for surface analysis of fibers Table 1 Comparison of instrumental...