This article discusses the standard test methods that can be applied to many types of welds: tension, bending, impact, and toughness testing. It provides information on four qualification stages, namely, the weld material qualification, base material qualification, the weld procedure qualification, and the weld service assessment. The article describes two general types of measurements for residual stress in welds: locally destructive techniques and nondestructive techniques. Locally destructive techniques include hole drilling, chip machining, and block sectioning. Nondestructive techniques include X-ray diffraction, neutron diffraction, Barkhausen noise analysis, and ultrasonic propagation analysis. The article concludes with an overview of weldability testing.

This article provides a summary of the concepts discussed in the articles under the Section “Failure Analysis” in ASM Handbook, Volume 21: Composites. Most of the information in this Section is geared toward organic-matrix composites, although there is some information on failure analysis and fractography of ceramic- and metal-matrix composites.

Mechanical and environmental loadings cause a variety of failure modes in composites, including matrix cracking, fiber-matrix debonding, delamination between plies, and fiber breakage. This article summarizes visual analysis and nondestructive testing methods for the failure analysis of composites. These methods include radiography, ultrasonic techniques, acoustic emission, and thermograph. The article also provides information on destructive test techniques.

Before the quality of a soldered joint can be evaluated, the components that are required for the formation of a good soldered joint should be reviewed. These components are solder, applied heat, and solderable surface. This article discusses each of these as well as the end-use requirements and joint configurations required for the formation of a good soldered joint. It focuses on the visual, automatic, and destructive inspection techniques for determining overall joint quality.

Inspection involves two types of testing, namely, destructive and non-destructive. This article provides an overview of the various inspection plans, such as first-article inspection and periodic tests done by destructive metallurgical testing and the final inspection done by the application of non-destructive technology. It describes the processes involved in destructive methods, such as surface hardness measurement, induction hardening pattern and heat-affected zone inspection, and the examination of microstructure before and after induction hardening. It also discusses non-destructive evaluation techniques for defect detection and microstructure characterization as well as non-destructive evaluation for real-time monitoring of induction process.

Cold pressure welding can be accomplished by deforming in a lap or butt configuration, drawing, extrusion, and rolling. This article provides a discussion on cold pressure lap welding, cold pressure butt welding and cold pressure welding in drawing process with illustrations. It provides information on the combinations of metals that can be successfully cold welded.

This article discusses the need of and the strain basis for residual stress measurements and describes the nature of residual stress fields. A generic destructive stress relief procedure is described along with the issues generally involved in each procedural step. The article presents the stress reconstruction equations to be used for computational reconstruction of the stress fields from the measured strains for the destructive methods. It provides information on the sectioning, material removal, strain measurement, and chemical methods of residual stress measurement. The article reviews the semidestructive methods of residual stress measurement: blind hole drilling and ring coring, spot annealing, and X-ray diffraction techniques. Nondestructive methods such as neutron diffraction, ultrasonic velocity, and magnetic Barkhausen noise techniques, are also discussed.

The goal of using nondestructive evaluation (NDE) in conjunction with failure analysis is to obtain the most comprehensive set of data in order to characterize the details of the damage and determine the factors that allowed the damage to occur. The NDE results can be used to determine optimal areas upon which to focus for sectioning and metallography in order to further investigate the condition of the component. This article provides information on the inspection method available for failure analysis, including standard methods such as visual testing, penetrant testing, and magnetic particle testing. It covers the effects of various factors on the properties of the part that may impact failure analysis, describes the characterization of damage modes and crack sizes, and finally discusses the processes involved in application of NDE results to failure analysis.

This article describes the two commonly used standardized tests for determining the mechanical properties of thermal spray coatings: hardness testing and tensile adhesion testing. It discusses the destructive and non-destructive methods of residual-stress measurement. Electrochemical testing methodologies include two distinctly different methods: direct and alternating current impedance techniques for assessing the corrosion resistance of coating attributes. The article also reviews the testing methods for determining thermomechanical and environmental stability of thermal barrier coatings. It discusses the wear testing methodologies that are standardized by ASTM, including the pin-on-disk, block-on-ring, dry sand/rubber wheel, erosion, metallographic apparatus abrasion, fretting wear, cavitation, reciprocating ball-on-flat, impact, and rolling contact fatigue test. The article concludes with a discussion on the methods of testing abradability and erosion resistance in abradable coatings.

Induction hardening of steel components is the most common application of induction heat treatment of steel. This article provides a detailed account of electromagnetic and thermal aspects of metallurgy of induction hardening of steels. It describes induction hardening techniques, namely, scan hardening, progressive hardening, single-shot hardening, and static hardening. The article discusses the techniques used to control the heat pattern, and provides a brief review of quenching techniques used in the induction hardening. It provides guidelines for selecting the frequency and power for induction hardening, and describes common methods for measuring case depth, such as optical and microhardness, and surface hardness. It provides information on some complications and ambiguities associated with these measurements. The article also discusses the commonly used non-destructive testing methods, namely, magnetic particle testing, ultrasonic testing, and eddy current testing to evaluate induction-hardened components.

This article focuses on the general methods and approaches from the perspective of a reconstruction analyst and includes discussions relevant to materials failure analysts at the incident scene. The elements of accident reconstruction are described. These have conceptual similarity with the principles for failure analysis of material incidents that are less complex than a large-scale accident. The article provides a brief review of some general concepts on the use of modeling which can be a very powerful tool for information pertaining to the reconstruction of an accident where the model can be a physical, mathematical, or logical representation of a physical system or process.

This article is a brief guide to information sources on nondestructive testing (NDT). It provides examples of some of the standards bodies commonly used by NDT personnel. These include the American Society for Testing and Materials (ASTM) International, European Committee for Standardization (CEN), American Society of Mechanical Engineers (ASME), International Organization for Standardization (ISO), Aerospace Industries Association (AIA), American Welding Society (AWS), American Petroleum Institute (API), and American Society for Nondestructive Testing (ASNT). All of these organizations used industry subject-matter experts and a consensus process in the development of their codes and standards.

This article outlines the requirements and methods associated with the inspection of brazements. It emphasizes the incorporation of these requirements into the overall quality system. The article reviews the acceptance limits, design limitations, and nondestructive and destructive inspection techniques involved in the brazement inspection. Selected case studies are also provided for further reference.

Failure analysis is generally defined as the investigation and analysis of parts or structures that have failed or appeared to have failed to perform their intended duty. Methods of field inspection and initial examination are also critical factors for both reconstruction analysts and materials failure analysts. This article focuses on the general methods and approaches from the perspective of a reconstruction analyst. It describes the elements of accident reconstruction, which have conceptual similarity with the principles for failure analysis of material incidents that are less complex than a large-scale accident. The approach presented is that the analysis and reconstruction is based on the physical evidence. The article provides a brief review of some general concepts on the use and limitations of advanced data acquisition tools and computer modeling. Legal implications of destructive testing are discussed in detail.

Hyperthermia is a type of cancer treatment that requires directing a carefully controlled dose of heated nanoparticles to the cancerous tumor that leads to the destruction of cancer cells. Nanoparticles are used as the heat generating sources within the cancer cells and the tumors. The problem in controlling the temperature of nanoparticles is solved by the use of induction heating, which uses a high-frequency alternating magnetic field localized in the area of interest. This article provides an overview of this technique along with the description of its major components, namely, nanoparticles, induction heating setup, and magnetic field strength.

This article discusses the classification of the attachment and joining methods in plastics, including mechanical fastening, adhesive bonding, solvent bonding, and welding. It describes the mechanical fastening techniques used to join both similar and dissimilar materials with machine screws or bolts, nuts and washers, molded-in threads, self-threading screws, rivets, spring-steel fasteners, press fits, and snap fits. The article explains solvent bonding used for thermoplastic parts, and tabulates the solvent types used with various plastics. It also describes the surface preparation of plastics, chemical treatment for adhesion, and tabulates the adhesive types for bonding plastics to plastics and plastics to nonplastics. The article briefly describes the welding processes of thermoplastics, including fusion welding (hot-tool, hot gas, extrusion, and focused infrared), friction welding (vibration, spin, and ultrasonic), and electromagnetic welding (resistance, induction, dielectric, and microwave). It concludes with the evaluation of welds using destructive and nondestructive testing.

Probability of detection (POD) assesses the performance of a non-destructive evaluation (NDE)-based inspection, which is a method used to determine the capability of an inspection as a function of defect type and defect size. This article provides an overview of the concept of POD, why it is needed, the history behind the development of POD, how POD assessments are performed, and how modeling and simulation can be integrated into the execution of a POD assessment. It describes the methods by which POD is determined. This includes detail on the experimental process to acquire the needed data, the mathematical methods to obtain a POD curve, and techniques to assess uncertainty in the POD curve as it is obtained from a limited data set. The concept of model-assisted POD (MAPOD) is introduced, with additional details and representative examples of MAPOD.

Adhesive-bonded joints are extensively used in aircraft components and assemblies where structural integrity is critical. This article addresses the problem of how to inspect bonded assemblies so that all discrepancies are identified. It describes several inspection techniques and presents drawbacks and limitations of these techniques. Generic flaw types and flaw-producing mechanisms are listed in a table. The article discusses metal-to-metal defects, adherend defects, honeycomb sandwich defects, repair defects, and in-service defects. It reviews the methods applicable to the inspection of bonded structures, including visual inspection, ultrasonic inspection, X-ray radiography, and neutron radiography. The evaluation and correlation of inspection results are also discussed. The article concludes with information on the effects of ultrasonic wave interference in the ultrasonic inspection of adhesive-bonded joints.

Chemical analysis is a critical part of any failure investigation. With the right planning and proper analytical equipment, a myriad of information can be obtained from a sample. This article presents a high-level introduction to techniques often used for chemical analysis during failure analysis. It describes the general considerations for bulk and microscale chemical analysis in failure analysis, the most effective techniques to use for organic or inorganic materials, and examples of using these techniques. The article discusses the processes involved in the chemical analysis of nonmetallics. Advances in chemical analysis methods for failure analysis are also covered.