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Image
Coherent transition precipitates revealed by strain contrast (dark-field) i...
Available to PurchasePublished: 01 December 2004
Fig. 12 Coherent transition precipitates revealed by strain contrast (dark-field) in transmission electron microscopy. The specimen is a Cu-3.1Co alloy aged 24 h at 650 °C (1200 °F). The precipitate is a metastable face-centered cubic (fcc) phase of virtually pure cobalt in the fcc matrix
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Schematic of coherent structure of solute-rich precipitates region that cau...
Available to Purchase
in Physical Metallurgy Concepts in Interpretation of Microstructures
> Metallography and Microstructures
Published: 01 December 2004
Fig. 13 Schematic of coherent structure of solute-rich precipitates region that causes lattice strain (indicated schematically by dashed lines)
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Schematic of coherent structure of solute-rich precipitates region that cau...
Available to PurchasePublished: 01 June 2016
Fig. 28 Schematic of coherent structure of solute-rich precipitates region that causes lattice strain
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Image
Coherent transition precipitates revealed by strain contrast (dark-field) i...
Available to PurchasePublished: 01 June 2016
Fig. 40 Coherent transition precipitates revealed by strain contrast (dark-field) in transmission electron microscopy. The specimen is a Cu-3.1Co alloy aged 24 h at 650 °C (1200 °F). The precipitate is a metastable face-centered cubic (fcc) phase of virtually pure cobalt in the fcc matrix
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Image
Diffraction pattern from a specimen of shock-loaded Nitronic 40. The streak...
Available to PurchasePublished: 15 December 2019
Fig. 35 Diffraction pattern from a specimen of shock-loaded Nitronic 40. The streaking is due to precipitation of a coherent second phase and deformation-induced twinning. The shape of the coherent precipitates and the elastic strain they induce caused streaking of the precipitate diffraction
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Diffraction pattern from a specimen of shock-loaded Nitronic 40. The streak...
Available to PurchasePublished: 01 January 1986
Fig. 16 Diffraction pattern from a specimen of shock-loaded Nitronic 40. The streaking is due to precipitation of a coherent second phase and deformation-induced twinning. The shape of the coherent precipitates and the elastic strain they induce has caused streaking of the precipitate
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Image
Coherent (left) and noncoherent (right) precipitation. (a) and (b) A cohere...
Available to PurchasePublished: 27 April 2016
Fig. 17 Coherent (left) and noncoherent (right) precipitation. (a) and (b) A coherent or continuous structure forms when any precipitate is very small. (c) and (d) Coherency is lost after the particle reaches a certain size and forms its own crystal structure. Then a real grain develops
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Series: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003731
EISBN: 978-1-62708-177-1
... Abstract Precipitation reactions occur in many different alloy systems when one phase transforms into a mixed-phase system as a result of cooling from high temperatures. This article discusses the homogenous and heterogeneous nucleation and growth of coherent and semicoherent precipitates...
Abstract
Precipitation reactions occur in many different alloy systems when one phase transforms into a mixed-phase system as a result of cooling from high temperatures. This article discusses the homogenous and heterogeneous nucleation and growth of coherent and semicoherent precipitates. It describes two precipitation modes, namely, general or continuous precipitation and cellular or discontinuous precipitation. The article also provides information on the precipitation sequences in aluminum alloys.
Image
Loss of coherency of γ″ precipitates in alloy 718. q, aspect ratio; e, disk...
Available to PurchasePublished: 01 June 2016
Fig. 29 Loss of coherency of γ″ precipitates in alloy 718. q, aspect ratio; e, disk particle thickness; L, mean equivalent diameter of disk-shaped particle. Source: Ref 34
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Book Chapter
Principles of Heat Treating of Nonferrous Alloys
Available to PurchaseSeries: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006250
EISBN: 978-1-62708-169-6
... Abstract This article introduces the mechanism of diffusion and the common types of heat treatments such as annealing and precipitation hardening, which are applicable to most ferrous and nonferrous systems. Three distinct processes occur during annealing: recovery, recrystallization, and grain...
Abstract
This article introduces the mechanism of diffusion and the common types of heat treatments such as annealing and precipitation hardening, which are applicable to most ferrous and nonferrous systems. Three distinct processes occur during annealing: recovery, recrystallization, and grain growth. The article also describes the various types of solid-state transformations such as isothermal transformation and athermal transformation, resulting from the heat treatment of nonferrous alloys. It provides information on the homogenization of chemical composition within a cast structure.
Book Chapter
Metallurgy of Heat Treatable Aluminum Alloys
Available to PurchaseSeries: ASM Handbook
Volume: 2A
Publisher: ASM International
Published: 30 November 2018
DOI: 10.31399/asm.hb.v02a.a0006509
EISBN: 978-1-62708-207-5
... of precipitation hardening include: Aluminum-copper systems with hardening from coherent precipitation of Guinier-Preston (GP) zones and subsequent transition precipitates (θ″ and θ′), which ultimately soften with the equilibrium phase CuAl 2 (θ) Aluminum-copper-magnesium systems, where magnesium...
Abstract
Heat treatment of aluminum alloys frequently refers to the heat treatable aluminum alloys that can be strengthened by solution treatment, quenching, and subsequent hardening. This article introduces the general metallurgy of strengthening aluminum alloys by heat treatment. It discusses various heat treatable alloying elements, such as copper, chromium, iron, magnesium, silicon, zinc, and lithium. The article describes the age-hardening treatments and generalized precipitation sequence for aluminum alloys. It reviews the solution heat treatment in terms of solution heating time and temperature, as well as high-temperature oxidation. The article also discusses quench sensitivity, vacancy loss, grain-boundary precipitates, and quench delay for the heat treatment of aluminum. It concludes with a discussion on the deformation of aluminum alloys prior to aging.
Book Chapter
Heat Treatable Nonferrous Alloys
Available to PurchaseSeries: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006274
EISBN: 978-1-62708-169-6
.... If this step is done properly, the precipitates can result in significant hardening of the alloy. In some cases, the precipitates are even coherent with the crystal matrix of the parent metal (see also the article “Principles of Heat Treating of Nonferrous Alloys” in this Volume). Although the aging process...
Abstract
This article describes the different types of precipitation and transformation processes and their effects that can occur during heat treatment of various nonferrous alloys. The nonferrous alloys are aluminum alloys, copper alloys, magnesium alloys, nickel alloys, titanium alloys, cobalt alloys, zinc alloys, and heat treatable silver alloys, gold alloys, lead alloys, and tin alloys. It also provides a detailed discussion on the effects due to precipitation and transformation processes in these non-ferrous alloys.
Book Chapter
Metallurgy of Heat Treatable Aluminum Alloys
Available to PurchaseSeries: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006287
EISBN: 978-1-62708-169-6
... aluminum alloys include: Aluminum-copper systems, with strengthening from coherent and transition precipitates prior to the formation of the equilibrium intermetallic CuAl 2 (2 xxx and 2 xx.x alloy series) Al-Cu-Mg systems, in which magnesium intensifies precipitation hardening with CuAl 2...
Abstract
This article describes the general categories and metallurgy of heat treatable aluminum alloys. It briefly reviews the key impurities and each of the principal alloying elements in aluminum alloys, namely, copper, magnesium, manganese, silicon, zinc, iron, lithium, titanium, boron, zirconium, chromium, vanadium, scandium, nickel, tin, and bismuth. The article discusses the secondary phases in aluminum alloys, namely, nonmetallic inclusions, porosity, primary particles, constituent particles, dispersoids, precipitates, grain and dislocation structure, and crystallographic texture. It also discusses the mechanisms used for strengthening aluminum alloys, including solid-solution hardening, grain-size strengthening, work or strain hardening, and precipitation hardening. The process of precipitation hardening involves solution heat treatment, quenching, and subsequent aging of the as-quenched supersaturated solid solution. The article briefly discusses these processes of precipitation hardening. It also reviews precipitation in various alloy systems, including 2xxx, 6xxx, 7xxx, aluminum-lithium, and Al-Mg-Li systems.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006268
EISBN: 978-1-62708-169-6
... of reversion, duplex annealing, and retrogression and re-aging are included. age hardening aging alloying aluminum alloys coherent precipitates precipitate-free zones semi-coherent precipitates ternary phase diagrams AGE HARDENING (or just aging) is the final step of the entire hardening...
Abstract
This article describes the effects of alloying and heat treatment on the metastable transition precipitates that occur in age hardenable aluminum alloys. Early precipitation stages are less well understood than later ones. This article details the aging sequence and characteristics of precipitates that occur in the natural aging and artificial aging of Al-Mg-Si-(Cu) alloys, Al-Mg-Cu alloys, microalloyed Al-Mg-Cu-(Ag, Si) alloys, aluminum-lithium-base alloys, and Al-Zn-Mg-(Cu) alloys. Crystal structure, composition, dimensions, and aging conditions of precipitates are detailed. Effects of reversion, duplex annealing, and retrogression and re-aging are included.
Image
Aging sequence in 7050. (a) Initial Guinier-Preston (GP) zone formation. (b...
Available to PurchasePublished: 30 November 2018
Fig. 14 Aging sequence in 7050. (a) Initial Guinier-Preston (GP) zone formation. (b) GP zone present and formation of semiincoherent η′. (c) Semiincoherent η′ and formation of coherent equilibrium precipitate η. (d) Precipitation of equilibrium precipitate η. Source: Ref 5
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Image
Aging sequence in 7050. (a) Initial Guinier-Preston (GP) zone formation. (b...
Available to PurchasePublished: 01 June 2016
Fig. 32 Aging sequence in 7050. (a) Initial Guinier-Preston (GP) zone formation. (b) GP zone present and formation of semi-incoherent η′. (c) Semi-incoherent η′ and formation of coherent equilibrium precipitate η. (d) Precipitation of equilibrium precipitate η. Source: Ref 57
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Image
(a) Ashby and (b) Orowan models for interaction of dislocations with cohere...
Available to PurchasePublished: 31 December 2017
Fig. 12 (a) Ashby and (b) Orowan models for interaction of dislocations with coherent and incoherent precipitates
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Book Chapter
Physical Metallurgy Concepts in Interpretation of Microstructures
Available to PurchaseSeries: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003723
EISBN: 978-1-62708-177-1
... in defining relationships between the microstructure of a material and its macroscopic properties. Second-phase boundaries also exist in many alloys (either intentionally from alloying or from impurities). Second phases are precipitates that form when a solute (i.e., alloying element or impurities...
Abstract
This article introduces basic physical metallurgy concepts that may be useful for understanding and interpreting variations in metallographic features and how processing affects microstructure. It presents some basic concepts in structure-property relationships. The article describes the use of equilibrium binary phase diagrams as a tool in the interpretation of microstructures. It reviews an account of the two types of solid-state phase transformations: isothermal and athermal. The article discusses isothermal transformation and continuous cooling transformation diagrams which are useful in determining the conditions for proper heat treatment (solid-state transformation) of metals and alloys. The influence of the mechanisms of phase nucleation and growth on the morphology, size, and distribution of grains and second phases is also described.
Image
Wrought, solution-annealed, and aged beryllium-copper (Cu-1.8%Be-0.3%Co) in...
Available to PurchasePublished: 01 December 2004
.). Polarized light and sensitive tint bring out the diffuse crisscross markings due to the submicroscopic γ′ precipitates and coherency strain fields. The magnification bar is 50 μm long. (b) Tint etching with Klemm's I did not reveal the structure as well, although the grain size is revealed. Tint etchants
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Image
Stress amplitude, Δσ/2, in Fe-0.3C-4Ni-1Al-1Cu steel versus reversals, 2 N ...
Available to PurchasePublished: 01 January 1996
°F) plus 8 h at 550 °C (1020 °F), coherent NiAl and copper precipitates are present. There is very little cyclic softening for this treatment. The cycles to fatigue crack initiation in a notched specimen were more than ten times greater for the latter treatment at a nominal stress amplitude of 196 MN
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