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Search Results for capillary viscometer
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Published: 01 January 2000
Series: ASM Handbook
Volume: 8
Publisher: ASM International
Published: 01 January 2000
DOI: 10.31399/asm.hb.v08.a0003322
EISBN: 978-1-62708-176-4
... on the measurement of viscosity of semisolid alloy materials by using three types of viscometers: the coaxial cylinder viscometer, the cone-and-plate viscometer, and the capillary viscometer. forming bulk forming sheet-metal forming semisolid forming polymer extrusion process modeling compression test...
Abstract
Forming processes can be divided into three major categories: bulk forming, sheet-metal forming, and semisolid forming and polymer extrusion. This article introduces each process category with a description of the constitutive models. It outlines the required properties for process modeling and describes the test methods for determining these properties. The article discusses several compression tests used to determine stress-strain curves for bulk forming and tensile tests used to obtain stress-strain curves for sheet-metal forming. The article concludes with information on the measurement of viscosity of semisolid alloy materials by using three types of viscometers: the coaxial cylinder viscometer, the cone-and-plate viscometer, and the capillary viscometer.
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Published: 01 February 2024
Fig. 18 Polyvinyl pyrrolidone K30 polymer concentration control using an Ubbelohde-type capillary viscometer and Abbe-type refractometer at 30 °C (85 °F) solution
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Series: ASM Handbook
Volume: 22B
Publisher: ASM International
Published: 01 November 2010
DOI: 10.31399/asm.hb.v22b.a0005514
EISBN: 978-1-62708-197-9
... ), using a statistical approach to estimate experimental uncertainty, claim uncertainties in the range of 5 to10%. Comparison of the oscillating viscometer with the capillary viscometer reveals some differences. Iida ( Ref 6 ) suggests the end effect is inadequately weighted in the Roscoe treatment...
Abstract
The measurement of thermophysical properties of metal alloys, especially at high temperatures, is difficult because of the reactivity of some alloys. This article reviews the methods available for measurement of thermal and other physical properties for liquid, semi-solid, and solid commercial alloys, including adiabatic calorimetry, modulated calorimetry, Calvet calorimetry, single-pan calorimetry, and drop calorimetry. It describes differential scanning calorimetry and differential temperature analysis for measuring transition temperatures such as phase transformation or glass transition temperatures. The article schematically illustrates the laser flash apparatus for measuring the thermal diffusivity of solids and oscillation viscometer for measurements of the viscosity of metals. A summary of the measurement methods is presented in tables.
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Published: 31 December 2017
Fig. 3 Ostwald viscometer used to measure viscosity of Newtonian fluid. A given amount of fluid flows out of a container via a narrow capillary tube, and flow time is multiplied by a calibration factor to determine viscosity.
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Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006849
EISBN: 978-1-62708-395-9
... scales (design and diameter of the indenting probe) of imposed weight, and delayed hardness reading (Rockwell specifies a fixed time), as well as critical minimum thickness. Rheological Properties Melt flow analysis may be automated (capillary rheometer, ASTM D3835-16, Ref 7 ) or manual...
Abstract
This article addresses some established protocols for characterizing thermoplastics and whether they are homogeneous resins, alloyed, or blended compositions or highly modified thermoplastic composites. It begins with a discussion on characterizing mechanical, rheological, and thermal properties of polymer. This is followed by a section describing molecular weight determination using viscosity measurements. Next, the article discusses the use of cone and plate and parallel plate geometries in melt rheology. It then reviews the processes involved in the analysis of thermoplastic resins by chromatography. Finally, the article covers three operations of thermoanalysis, namely differential scanning calorimetry, thermogravimetric analysis, and thermomechanical testing.
Series: ASM Handbook
Volume: 18
Publisher: ASM International
Published: 31 December 2017
DOI: 10.31399/asm.hb.v18.a0006401
EISBN: 978-1-62708-192-4
... pressure ( p r ), film thickness ( h 0 ), bearing pocket diameter ( b ), and bearing load thickness ( l ). Adapted from Ref 25 Fig. 10 Selected properties of a hydrostatic bearing that incorporate an orifice or a capillary restrictor, as a function of average lubricant film thickness...
Abstract
This article provides a brief introduction to lubrication as a method to reduce friction between two surfaces. It discusses the surface characteristics of parts and explores how lubrication helps separate two contacting surfaces and thereby decreases the coefficient of friction. The article details the classifications of lubrication regimes, namely, boundary, mixed, hydrodynamic, and elastohydrodynamic lubrications. It discusses the various types of lubricant materials and additives, including liquid lubricants, solid lubricants, gaseous lubricants, greases, green lubricants, and nanomaterials. The article also reviews the properties of lubricants. It describes the tribological evaluation of lubricants, including stribeck test, four-ball test, block-on-ring test, pin-in-vee test, and reciprocating motion test.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006930
EISBN: 978-1-62708-395-9
... is that the force necessary to move the piston depends solely on the rate at which it is being pulled through the fluid; it is independent of the actual displacement. The manner in which this relates to commercial rheometers, including viscometers, is also shown in Fig. 1 . If an upper geometry is rotated...
Abstract
Rheology is defined as the study of the flow and deformation of matter. This article begins with an examination of flow behavior. It describes the geometries and methods employed for rheological testing of polymers in their molten state. It also discusses materials that are predominantly in the solid state and the methods employed for solids testing. Examples of unidirectional and dynamic oscillatory testing are provided for different mechanical behaviors.
Series: ASM Handbook
Volume: 18
Publisher: ASM International
Published: 31 December 2017
DOI: 10.31399/asm.hb.v18.a0006411
EISBN: 978-1-62708-192-4
... of lubricants are the Ostwald viscometer and the rheometer. The Ostwald viscometer ( Fig. 3 ) measures the viscosity of Newtonian fluid. A given amount of fluid flows out of a container via a narrow capillary tube, and flow time is multiplied by a calibration factor to determine its viscosity. The rheometer...
Abstract
The function of lubricants is to control friction and wear in a lubricating system containing machine elements such as gears and bearings. This article discusses the basic properties of lubricants to help scientists and engineers understand the principles behind lubricant selection. It reviews the functions of additives, such as friction modifiers, antiwear additives, viscosity modifiers, corrosion inhibitors, oxidation inhibitors, dispersants, and detergents. The article discusses the physical properties of liquid lubricants and the performance characteristics of lubricants. It describes the most common lubricant categories and provides information on the health and safety aspects of using liquid lubricants. The article concludes with a discussion on the lubricant-application method that plays a vital role in how the lubricant functions.
Series: ASM Handbook
Volume: 23A
Publisher: ASM International
Published: 12 September 2022
DOI: 10.31399/asm.hb.v23A.a0006861
EISBN: 978-1-62708-392-8
... microbubble. The quick evolvement of the microbubble exerts a pressure wave front on the liquid column, which, if capable to overcome the capillary force, ejects a microdroplet through the orifice with a particular velocity. The volume of the droplet is related to the electrical energy supplied to heat...
Abstract
Inkjet printing is extremely precise in terms of the ejected microdroplets (picoliter volume), contributing an unparalleled lateral resolution. Additionally, the benefits of high-speed deposition, contactless ink delivery, and the use of a range of ink materials endorse this technique as suitable for high-throughput 3D manufacturing. This article provides an overview of inkjet 3D printing (also referred to as 3D inkjetting). It then highlights the major components and accessories used in commercial and laboratory-based 3D inkjet printers. Next, the article describes the process physics of the transient phenomena involved in both binder-jetting- and direct-inkjetting-based 3D printing. It then discusses the scope and advantages of 3D inkjetting in the manufacturing of metallic, ceramic, and polymer-based biomaterials. The article also discusses several approaches and methodologies to examine the in vitro cytocompatibility and in vivo biocompatibility of both binder-jetted and direct-inkjetted scaffolds for biomedical applications. Finally, it discusses the challenges and troubleshooting methodologies in 3D inkjetting of biomaterials.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003053
EISBN: 978-1-62708-200-6
.... Viscometers are available with an array of probes that can measure the thin slips needed for slip casting or the plastic mix used in extrusion. Dry Pressing Dry pressing is the process by which ceramic powders are consolidated inside a cavity into a predetermined shape through the use of applied...
Abstract
Ceramic-forming processes usually start with a powder which is then compacted into a porous shape, achieving maximum particle packing density with a high degree of uniformity. This article compares and contrasts several forming processes, including mechanical consolidation, dry pressing, cold isostatic pressing, slip casting, tape casting, roll compaction, extrusion, and injection molding. It describes the advantages, equipment and tooling, and material requirements of green machining, the machining of ceramics in an unfired state with the intent of producing parts as close to as possible to their final shape. The article also provides useful information on drying methods, shrinkage, and defects as well as the removal of organic processing aids such as dispersants, binders, plasticizers, and lubricants.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006916
EISBN: 978-1-62708-395-9
... (such as the Brookfield viscometer) tests (ASTM D789) to determine the relative viscosity of polyamides. Alternately, a melt flow index (MFI) test (ASTM D1238) or capillary rheometer test (ASTM D3835) can be conducted to determine if there has been a significant reduction in viscosity due to degradation. Molded parts can...
Abstract
This article focuses on manufacturing-related failures of injection-molded plastic parts, although the concepts apply to all plastic manufacturing processes It provides detailed examples of failures due to improper material handling, drying, mixing of additives, and molecular packing and orientation. It also presents examples of failures stemming from material degradation improper use of metal inserts, weak weld lines, insufficient curing of thermosets, and inadequate mixing and impregnation in the case of thermoset composites.
Series: ASM Handbook
Volume: 4B
Publisher: ASM International
Published: 30 September 2014
DOI: 10.31399/asm.hb.v04b.a0005933
EISBN: 978-1-62708-166-5
..., semidilute nanofluids, semiconcentrated nanofluids, and concentrated nanofluids ( Ref 85 ). Xinfang et al., who measured the viscosity of copper-H 2 O nanofluid by using capillary viscometers, obtained results showing that the temperature and the sodium dodecylbenzenesulfonate (SDBS) concentration...
Abstract
Nanofluids offer a completely different behavior of wetting kinetics and heat-removal characteristics, which are exploited in industrial heat treatment for quenching. This article provides information on the important thermophysical properties of nanofluids, namely, thermal conductivity, viscosity, specific heat, density, and surface tension. It reviews wetting and boiling heat-transfer characteristics of nanofluids as quenchants and highlights the importance of using nanofluids as effective quench media for the hardening process during heat treatment. The article describes the effect of nanoparticle addition on the microstructure, mechanical properties of components, wetting kinetics, and kinematics.
Series: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.9781627083959
EISBN: 978-1-62708-395-9
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005255
EISBN: 978-1-62708-187-0
Abstract
This article reviews the pattern materials used in investment casting, which can be loosely grouped into waxes and plastics. The patternmaking process, pattern tooling, and pattern and cluster assembly are described. The article also describes the manufacture of ceramic shell molds and cores, detailing the binders and other materials used, as well as the formulation and control of slurries. Methods for pattern removal, mold firing, melting, casting, postcasting treatment, and inspection are explained. After presenting design recommendations for investment castings, the article concludes with information on applications and special versions of the investment casting process.
Series: ASM Handbook
Volume: 4F
Publisher: ASM International
Published: 01 February 2024
DOI: 10.31399/asm.hb.v4F.a0007002
EISBN: 978-1-62708-450-5
... of bitumen is typically determined using a vacuum capillary tube viscometer at 60 and 135 °C (140 and 275 °F) ( Ref 43 ). Fig. 14 Schematic illustration of selective solvent extraction to separate bitumen into structural groups. Source: Ref 43 Generally, bitumen is composed of asphaltic...
Abstract
In this article, an in-depth overview of petroleum quenching oils is provided, including oil composition, use, mechanism of the oil quenching processes, oil degradation, toxicology and safety, and quenching bath maintenance.
Book Chapter
Series: ASM Handbook
Volume: 4F
Publisher: ASM International
Published: 01 February 2024
DOI: 10.31399/asm.hb.v4F.a0007003
EISBN: 978-1-62708-450-5
..., calculated from the cooling curve data ( Ref 100 ), showed the HP value for the 15% PVP K30 solution was almost half of the value obtained for the petroleum oil quenchant ( Fig. 19 ). Fig. 18 Polyvinyl pyrrolidone K30 polymer concentration control using an Ubbelohde-type capillary viscometer...
Abstract
This article presents the fundamentals and nomenclature of polymer quenchants and provides a detailed discussion on the polymers used for quenching formulation. The article describes the effect of polymer structure on the quenching mechanism. It also presents the factors affecting polymer quenchant performance. The article details the use of polymer quenchants for intensive quenching and then focuses on the wire patenting processes and polymer quenchant analysis. The article presents the application of polymer quenchants for induction hardening. Finally, it provides details on cooling curve analysis of polymer quenchants.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.9781627082136
EISBN: 978-1-62708-213-6
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.9781627082006
EISBN: 978-1-62708-200-6
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003068
EISBN: 978-1-62708-200-6
.... ofAl203 made by thermal decomposition of gibbsite at absolute viscosity. See viscosity. 350 to 400 °C (660 to 750 °F), used as a catalyst, absorption. (1) The taking up of a liquid or gas by catalyst carder, and absorbent. It is chemically inert to capillary, osmotic, or solvent action. (2) The capacity...
Abstract
This article is a compilation of definitions for terms related to engineering materials, including plastics, elastomers, polymer-matrix composites, adhesives and sealants, ceramics, ceramic-matrix composites, glasses, and carbon-carbon composites.
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