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calibration
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Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006634
EISBN: 978-1-62708-213-6
... Abstract Most modern instrumental techniques produce an output or signal that is not absolute. To obtain quantitative information, the raw output from an instrument must be converted into a physical quantity. This is done by standardizing or calibrating the raw response from an instrument...
Abstract
Most modern instrumental techniques produce an output or signal that is not absolute. To obtain quantitative information, the raw output from an instrument must be converted into a physical quantity. This is done by standardizing or calibrating the raw response from an instrument and subsequently analyzing the uncertainty from both the calibration process and the measurement process. This article briefly summarizes the most common calibration and uncertainty analysis methods, namely external standard methods, abbreviated external standard methods, internal normalization, internal standard, standard addition, and serial dilution methods. In addition, it includes information on the traceability of true value of a measured quantity.
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Published: 01 January 1986
Fig. 4 Calibration curve for ICP analysis showing detection limits and concentration of analyte in sample.
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Published: 01 January 1986
Fig. 13 Calibration curve for the determination of aluminum in thermite by flame AAS.
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Published: 01 January 1986
Fig. 5 Calibration curve showing absorbance as a function of sample concentration.
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Published: 01 January 1986
Fig. 17 Calibration of B 2 O 3 concentration from ICE versus height of the B-O overtone band. The line drawn through the data is from the linear least squares fit of the data.
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Published: 01 January 1986
Fig. 11 Calibration curve for quantitative analysis of paraben concentrations in baby lotion.
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Published: 01 August 2013
Fig. 52 Chart for calibration of Pitot tube, assuming a Pitot tube factor, K , of 1.0. Velocity equals K 64.4 h , where h is the pressure head, in feet of water. (a) Low velocity. (b) Full range
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Published: 01 December 2004
Fig. 9 Image calibration. Spacing between line segments of the micrometer reticle is 0.01 mm. Consequently, the segment length of 420 pixels corresponds with the distance of 0.1 mm.
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Published: 01 January 2003
Fig. 27 Configuration and K I calibration of a double-beam plate specimen. Normalized stress intensity K I plotted against a / H ratio. ( W − a ) indifferent, crackline-loaded, single-edge cracked specimen. Source: Ref 33
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Published: 15 December 2019
Fig. 12 Examples of calibration curves in spark optical emission spectroscopy using the ratio method. Source: Ref 8 . Reprinted with permission of Elsevier
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Published: 15 December 2019
Fig. 5 Typical calibration curve representing the concentration of the analyzed element (μg/L) as a function of the relative intensity. The detection limit is defined as the standard deviation of the lowest measurable concentration. As illustrated, the standard concentration should be within
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Published: 15 December 2019
Fig. 17 Calibration of B 2 O 3 concentration from ion chromatography exclusion versus height of the B–O overtone band. The line drawn through the data is from the linear least-squares fit of the data.
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Published: 15 December 2019
Fig. 1 An example calibration curve prepared by use of the external standard method. The instrument response is represented by A , and the concentration resulting in that response is [ A ]. While curves for two analytes are shown, in principle as many analytes as desired can be plotted. While
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Published: 15 December 2019
Fig. 2 An example of a single-point calibration curve. The instrument response is represented by A , and the concentration resulting in that response is [ A ]. The origin (0,0) is assigned as part of the curve, and is assumed to have no uncertainty.
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Published: 15 December 2019
Fig. 3 An example of two standards plus a blank calibration curve. The blank is subtracted from each of the standards. The instrument response is represented by A , and the concentration resulting in that response is [ A ].
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Published: 15 December 2019
Fig. 4 An example of calibration by multiple standard addition. Three additions (spikes) of the analyte X are shown, as is the extrapolation to the unknown concentration, X 0 .
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in Review of Ultrasonic Testing for Metallic Additively Manufactured Parts
> Additive Manufacturing Design and Applications
Published: 30 June 2023
Fig. 33 (a) Calibration block. Size: 140 × 60 × 20 mm (5.5 × 2.4 × 0.8 in.). (b) Inspection of the calibration sample in immersion. SDH, side-drilled hole
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in Review of Ultrasonic Testing for Metallic Additively Manufactured Parts
> Additive Manufacturing Design and Applications
Published: 30 June 2023
Fig. 34 Calibration abacus based on machined flaws. Each dot corresponds to the measurement of a hole-reflected amplitude from one position of the probe. The different curves show the expected intensity in decibels per distance to the probe. The shaded regions show confidence intervals.
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