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Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003249
EISBN: 978-1-62708-199-3
... describes the classification of materials characterization methods including, bulk elemental characterization, bulk structural characterization, microstructural characterization, and surface characterization. Further, the article reviews the selection of materials characterization methods most commonly used...
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006670
EISBN: 978-1-62708-213-6
..., fabrication methods, sample preparation, bulk/elemental characterization methods, microstructural characterization methods, surface characterization methods, and electronic characterization methods. semiconductor characterization Introduction This article introduces various techniques commonly...
Book Chapter

By Wei-Kan Chu
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001775
EISBN: 978-1-62708-178-8
... Abstract Rutherford backscattering spectrometry (RBS) is a major materials characterization technique that can provide information in a short analysis time. It is used for quantitative compositional analysis of thin films, layered structures, or bulk materials and to measure surface impurities...
Book Chapter

Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006669
EISBN: 978-1-62708-213-6
... Abstract This article discusses several purposes and types of materials characterization techniques. Some of the factors to be considered when selecting appropriate characterization methods are described. The article also presents the scope and organization of this volume. materials...
Book Chapter

By K.H. Eckelmeyer
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003252
EISBN: 978-1-62708-199-3
... Abstract Microstructural analysis is the combined characterization of the morphology, elemental composition, and crystallography of microstructural features through the use of a microscope. This article reviews three types of the most commonly used electron microscopies in metallurgical studies...
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006766
EISBN: 978-1-62708-295-2
... in the articles “ Optical Emission Spectroscopy ,” “ Inductively Coupled Plasma Optical Emission Spectroscopy ,” and “ Ion Chromatography ” in Materials Characterization , Volume 10 of the ASM Handbook , 2019, and in the article “ Bulk Elemental Analysis ” in the Metals Handbook Desk Edition , 2nd ed., 1998...
Book Chapter

Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006678
EISBN: 978-1-62708-213-6
... for characterization of metals and alloys Table 1 Analytical methods used for characterization of metals and alloys Technique Elemental analysis Speciation Compound Isotopic or mass analysis Qualitative analysis (identification of constituents) Semiquantitative analysis (order of magnitude...
Book Chapter

By Bo Hu
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006649
EISBN: 978-1-62708-213-6
... on the important properties to characterize powders, namely the particle size, surface area, density, porosity, particle hardness, compressibility, green strength, and flowability. For characterization of powders, both individual particles and bulk powders are used to evaluate their physical and chemical...
Book Chapter

By R.E. Whan, K.H. Eckelmeyer, S.H. Weissman
Series: ASM Handbook Archive
Volume: 10
Publisher: ASM International
Published: 01 January 1986
DOI: 10.31399/asm.hb.v10.a0001726
EISBN: 978-1-62708-178-8
... electron microscopy, many techniques that require special modifi- by which twinning in polycrystalline sam- cations or conditions to perform the desired ductors" is divided into bulk/elemental anal- ples can be characterized. Similarly, under analysis are omitted. The previous section of ysis...
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006126
EISBN: 978-1-62708-175-7
... Abstract This article discusses the capabilities and limitations of various material characterization methods that assist in the selection of a proper analytical tool for analyzing particulate materials. Commonly used methods are microanalysis, surface analysis, and bulk analysis...
Book Chapter

By M. Clara Wright
Series: ASM Handbook
Volume: 11
Publisher: ASM International
Published: 15 January 2021
DOI: 10.31399/asm.hb.v11.a0006759
EISBN: 978-1-62708-295-2
... with both bulk hardness and conductivity provides an indication of the alloy and temper ( Ref 2 ). There are times when a conclusive PMI is not possible due to alloys having overlapping weight percentages for similar elements as well as overlapping mechanical properties. In this case, other methods may...
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006086
EISBN: 978-1-62708-175-7
... properties of metal powders, both as individual particles and in bulk forms. chemical properties electrolysis gas atomization mechanical alloying metal powders milling oxides reduction physical properties powder characterization powder production water atomization METAL POWDER PRODUCTION...
Book Chapter

By Dehua Yang
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006675
EISBN: 978-1-62708-213-6
.... A quick reference summary of surface-analysis methods is presented in this article. atomic force microscopy scanning probe microscopy surface layers surface analysis THIS DIVISION, “Surface Analysis,” is a new addition in Materials Characterization , Volume 10 of ASM Handbook (2019...
Book Chapter

By K.H. Eckelmeyer
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003250
EISBN: 978-1-62708-199-3
... and precision methods, and sample requirements. The amount of material that needs to be sampled, operating principles, and limitations of the stated methods are also discussed. alloys bulk elemental analysis combustion and inert gas fusion analysis metals optical emission spectroscopy X-ray...
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006652
EISBN: 978-1-62708-213-6
... solids Table 1 Analytical methods used for characterization of organic solids Technique(a) Elemental analysis Speciation Compound Isotopic or mass analysis Qualitative analysis (identification of constituents) Semiquantitative analysis (order of magnitude) Quantitative analysis...
Book Chapter

Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006671
EISBN: 978-1-62708-213-6
... spectroscopy; XRD, x-ray diffraction; XRS, x-ray spectrometry. (a) Limited number of elements or groups. (b) Under special conditions Characterization techniques for ceramics and glasses Table 1 Characterization techniques for ceramics and glasses Wet analytical chemistry, ultraviolet/visible...
Book Chapter

By Gary Runyon, Binky Sargent
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006056
EISBN: 978-1-62708-175-7
... matrix interference, moderate spectral interference, high investment costs, elemental sets fixed by configuration, depth profiles Surface and bulk Inductively coupled plasma optical emission spectrometry (ICP-OES) Spectral emission Low matrix interference, high spectral interference, high operation...
Series: ASM Handbook
Volume: 24A
Publisher: ASM International
Published: 30 June 2023
DOI: 10.31399/asm.hb.v24A.a0006970
EISBN: 978-1-62708-439-0
... reconstructed using the Integrated Visualization and Analysis Software (version 3.8.6). The mass spectrum was used to analyze the bulk composition of this sample ( Table 2 ). When comparing this composition to the bulk alloy composition, it was observed that the LEAP sample was lean in alloying elements...
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006648
EISBN: 978-1-62708-213-6
.... Calibration and Accuracy Calibrations are needed to find the proportionality between the measured intensity and the element concentration in bulk analysis. This proportionality can be directly obtained by using matrix-matched certified reference materials (CRMs) whenever both sample and calibration...
Book Chapter

By Debbie Aliya
Series: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003529
EISBN: 978-1-62708-180-1
... specimens. Format of a Bulk Metal Composition Analysis Report The following table is an example of a suggested format of a bulk metal composition analysis report. Note that the chemist has flagged (with an asterisk) the element (in this case, Mn) that does not meet the given specification...