Powder metallurgy (PM) high-alloy tool steels (HATS) have unique properties that assist them in solving various problems related to machining of metal components. This article describes the cost-intensive PM processing routes of HATS, as well as their major properties, including elastic properties, density, mechanical properties, grindability, fatigue and wear resistance, and thermophysical properties.

High-potential high-alloy tool steels (HATS) containing martensitic microstructure with undissolved hard phases are achieved by a number of complex heat treating cycles, predominantly tempering. This article focuses on three tempering treatments, namely, salt bath heat treatment, austenitizing, and vacuum heat treatment. It explains the result of these tempering processes with HSS M2 grade of HATS.

This article describes the effects of undissolved carbides formed by segregation of alloying elements on the hardness of the powder-metallurgical (PM) high-alloy tool steels (HATS). It explains the calculation of exact stoichiometric carbon content that depends on the required martensite hardness, amount of carbon forming alloying elements, types of undissolved carbides during austenitizing, and the densities of the carbides. Microhardness values for carbides in HATS are also listed.

This article is a comprehensive collection of tables that list the nominal chemical composition of common powder metallurgy (PM) high-alloy tool steels, namely, PM high-speed, cold working, and corrosion-resistant tool steels.

The microstructure in the longitudinal direction of conventional high-alloy tool steels (HATS) depends very much on the degree of hot working. Comparing different processes, the highest processing temperature proves to be decisive for coarseness of the microstructure. This article provides a discussion on the microstructure of conventional HATS and hot isostatically pressed high-speed steel. The effects of the processing in cold worked HATS are illustrated.

Safety is an important consideration in all welding, cutting, and related work. This article discusses the basic elements of safety general to all welding, cutting, and related processes. It includes safety procedures common to a variety of applications. The most important component of an effective safety and health program is management support and direction. The article reviews the role of management, training, housekeeping, and public demonstrations in welding safety to minimize personal injury and property damage. It provides information on the safety measures for eye and face protection in various welding and cutting operations. Injuries and fatalities from electric shock in welding and cutting operations can occur if proper precautionary measures are not followed. The article discusses the electrical safety aspects to be considered for various welding and cutting operations.

Low-pressure carburizing (LPC) is one of the most popular case-hardening processes and is applied to increase the fatigue limit of dynamically loaded components. It takes place in a pressure range between 5 and 15 mbar (4 and 11 torr) and at temperature range between 870 and 1050 deg C. The LPC process runs in two different types of equipment: single-chamber furnaces and treatment chambers. This article reviews the use of simulation software for prediction of carbon profiles and typical quality control procedures. It describes the physical principles and typical applications of LPC.

This article describes the analytical methods for analyzing surfaces for corrosion and corrosion inhibition processes as well as failure analysis based on surface structure and chemical identity and composition. The principles and applications of the surface-structure analysis techniques, namely, optical microscopy, scanning electron microscopy, scanning tunneling microscopy, and atomic force microscopy, are reviewed. The article discusses the principles and applications of chemical identity and composition analysis techniques. These techniques include the energy dispersive X-ray spectroscopy, Auger electron spectroscopy, X-ray photoelectron spectroscopy, ion scattering spectroscopy, reflectance Fourier transform infrared absorption spectroscopy, Raman and surface enhanced Raman spectroscopy, and extended X-ray absorption fine structure analysis.

The purpose of fractography is to analyze fracture features and attempt to relate the topography of the fracture surface to the causes and/or basic mechanisms of fracture. This article reviews the historical development of fractography, from the early studies of fracture appearance dating back to the sixteenth century to the state-of-the-art work in electron fractography and quantitative fractography. It also describes the applications and limitations of scanning electron microscope and transmission electron microscope.

Bending fatigue of carburized steel components is a result of cyclic mechanical loading. This article reviews the alloying and processing factors that influence the microstructures and bending fatigue performance of carburized steels. These include austenitic grain size, surface oxidation, retained austenite, subzero cooling, residual stresses, and shot peening. The article describes the analysis of bending fatigue behavior of the steels based on S-N curves that represents a stress-based approach to fatigue. It discusses the types of specimen used to evaluate bending fatigue in carburized steels. The stages of fatigue and fracture of the steels, namely crack initiation, stable crack propagation, and unstable crack propagation, are reviewed. The article analyzes the intergranular fracture at the prior-austenite grain boundaries of high-carbon case microstructures that dominates bending fatigue crack initiation and unstable crack propagation of direct-quenched carburized steels.

X-ray spectroscopy is generally accepted as the most useful ancillary technique that can be added to any scanning electron microscope (SEM), even to the point of being considered a necessity by most operators. While “stand-alone” x-ray detection systems are used less frequently in failure analysis than the more exact instrumentation employed in SEMs, the technology is advancing and is worthy of note due to its capability for nondestructive analysis and application in the field. This article begins with information on the basis of the x-ray signal. This is followed by information on the operating principles and applications of detectors for x-ray spectroscopy, namely energy-dispersive spectrometers, wavelength-dispersive spectrometers, and handheld x-ray fluorescence systems. The processes involved in x-ray analysis in the SEM and handheld x-ray fluorescence analysis are then covered. The article ends with a discussion on the applications of x-ray spectroscopy in failure analysis.

Crucible furnaces, as compared to electric arc furnaces, are increasingly deployed in various melting practices due to their environmental and workplace friendliness and their process benefits. This article focuses on the application of induction crucible furnaces for melting and pouring operations in small-and medium-sized steel foundries, including aluminum, copper, and zinc industries. It also provides information on the process engineering benefits of melting and pouring operations.

Nitriding is a general term for all processes based on the addition of nitrogen to the surface of steel. When carbon is added along with the nitrogen, the process is called nitrocarburizing. This article provides a detailed discussion on the functional and structural properties of nitrided layers. It describes the structural changes on the surface of carbon steels, alloy steels, and austenitic stainless steels. The article explains the effects of the various nitriding processes, namely, gaseous nitriding, plasma nitriding, gaseous nitrocarburizing, and salt bath nitrocarburizing, on the structure and properties of nitrided layers.

Dimensional and shape changes caused by heat treatment have been the subject of scientific and industrial research for a very long time. This article provides an overview of the complexity of distortion and stress generation during heat treatment of steels. It discusses the measurement and evaluation of dimensional and shape changes with examples. The article describes the mechanisms at work during the generation of stresses and distortion during heat treatment. A hypothetical experiment with increasing application to real life is used to develop a systematization of unavoidable size and shape changes. The article also provides information on the carriers of distortion potential that cause measureable size and shape changes.

This article describes a scientific approach to the planning and evaluation of fatigue tests based on the determination of probabilities for detected fracture positions within the observed range of fatigue scatter. It schematically illustrates a constant-amplitude stress cycling about a possible mean load that leads to the fracture of a single part or specimen. The article discusses the evaluation of the range of transition and of the finite-endurance range for fatigue curves. It concludes with a discussion on extrapolation from the range of finite endurance into the range of transition.

This article provides an overview of the incremental sheet forming (ISF) process and discusses the process variations of ISF. These variations include single-point incremental forming, two-point incremental forming, and kinematic incremental sheet forming. The article discusses the machines and equipment used in the process and describes the process parameters, process mechanics, and process limits. It illustrates multistage forming strategies and summarizes difficulties that exist with regard to the finite-element process simulation of ISF process. The article also describes hybrid process variations, such as stretch forming and laser-assisted ISF.