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Austenite grain growth in a fine-grained 0.5% C hypoeutectoid steel (alumin...
Available to Purchase
in Problems Associated with Heat Treated Parts
> Analysis and Prevention of Component and Equipment Failures
Published: 30 August 2021
Fig. 9 Austenite grain growth in a fine-grained 0.5% C hypoeutectoid steel (aluminum deoxidized). 0.43C-0.23Si-0.75Mn (wt%). (a) Austenitized for 1 h at 850 °C, cooled at 300 °C/h. Austenite grain size: ASTM No. 7, 180 HV. Picral. 100x. (b) Austenitized for 1 h at 900°C, cooled at 300 °C/h
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Effect of peak temperature and precipitate (TiN) coarsening on austenite gr...
Available to PurchasePublished: 31 October 2011
Fig. 14 Effect of peak temperature and precipitate (TiN) coarsening on austenite grain growth in the heat-affected zone of a titanium-microalloyed steel. The points in the diagram are experimental data, whereas the curves are calculated. Source: Ref 4
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Series: ASM Handbook
Volume: 6A
Publisher: ASM International
Published: 31 October 2011
DOI: 10.31399/asm.hb.v06a.a0005613
EISBN: 978-1-62708-174-0
..., the longer the retention time above Ac 3 and thus the more severe the grain growth becomes. As the peak temperature decreases with distance from the fusion line, the austenite grain size decreases sharply. Regions of the HAZ further away from the fusion line become only partially austenitic during...
Abstract
Solid-state transformations occurring in a weld are highly nonequilibrium in nature and differ distinctly from those experienced during casting, thermomechanical processing, and heat treatment. This article provides a description of the special factors affecting transformation behavior in a weldment. It reviews the heat-affected and fusion zones of single-pass and multi-pass weldments. The article also includes a discussion on the welds in alloy systems, such as stainless steels and aluminum-base, nickel-base, and titanium-base alloys.
Series: ASM Handbook
Volume: 14A
Publisher: ASM International
Published: 01 January 2005
DOI: 10.31399/asm.hb.v14a.a0003995
EISBN: 978-1-62708-185-6
... alloy additions to retard grain growth at high temperature and/or alloying to allow special thermomechanical conditioning of the microstructure. For example, to retard the growth of austenite grains during hot working of steels, aluminum is added to allow precipitation of aluminum-nitrogen precipitates...
Abstract
Thermomechanical processing (TMP) refers to various metal forming processes that involve careful control of thermal and deformation conditions to achieve products with required shape specifications and good properties. This article describes TMP methods in producing hot-rolled steel and reviews how improvements in the strength and toughness depend on the synergistic effect of microalloy additions and on carefully controlled thermomechanical conditions. It discusses TMP variables and the general distinctions between conventional hot rolling and common types of controlled-rolling schedules. The article describes the metallurgical processes in grain refinement of austenite steel by hot working, such as recovery and recrystallization and strain-induced transformation. The grain refinement in high strength low alloy steel by alloy addition is also discussed. The article provides an outline on the key stages of deformation, and the required metallurgical information at each of these stages.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005786
EISBN: 978-1-62708-165-8
... binary phase diagram. It also describes the effects of austenite grain size, and provides useful information on controlling the austenite grain size using the thermomechanical process. austenite austenitizing grain growth steel Introduction Austenite is the intermediate starting...
Abstract
Austenitization refers to heating into the austenite phase field, during which the austenite structure is formed. This article highlights the purpose of austenitization, and reviews the mechanism and importance of thermodynamics and kinetics of austenite structure using an iron-carbon binary phase diagram. It also describes the effects of austenite grain size, and provides useful information on controlling the austenite grain size using the thermomechanical process.
Book Chapter
Simulation of Microstructural Evolution in Steels
Available to PurchaseSeries: ASM Handbook
Volume: 22A
Publisher: ASM International
Published: 01 December 2009
DOI: 10.31399/asm.hb.v22a.a0005414
EISBN: 978-1-62708-196-2
... modeling metal flow austenite grain growth recrystallization flow stress STEEL is certainly one of the most widely used materials. It has a broad range of uses, primarily as raw material in the manufacture of automobiles, machinery, appliances, and also in the construction of buildings, bridges...
Abstract
Computer simulation of microstructural evolution during hot rolling of steels is a major topic of research and development in academia and industry. This article describes the methodology and procedures commonly employed to develop microstructural evolution models to simulate microstructural evolution in steels. It presents an example of the integration of finite element modeling and microstructural evolution models for the simulation of metal flow and microstructural evolution in a hot rolling process.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006131
EISBN: 978-1-62708-175-7
...) was cold isostatically pressed from water-atomized vacuum annealed powder, sintered at 1220 °C (2230 °F) to closed porosity, and forged to full density. Decreasing the temperature from 1255 to 1220 °C (2290 to 2230 °F) left less opportunity for carbide coarsening and austenite grain growth, though...
Abstract
The microstructure in the longitudinal direction of conventional high-alloy tool steels (HATS) depends very much on the degree of hot working. Comparing different processes, the highest processing temperature proves to be decisive for coarseness of the microstructure. This article provides a discussion on the microstructure of conventional HATS and hot isostatically pressed high-speed steel. The effects of the processing in cold worked HATS are illustrated.
Series: ASM Handbook
Volume: 11A
Publisher: ASM International
Published: 30 August 2021
DOI: 10.31399/asm.hb.v11A.a0006816
EISBN: 978-1-62708-329-4
... to achieve temperature equalization in a heavy section, whereas small parts may come to even temperature in just minutes. For quenched and tempered steels, the austenitizing temperature is a compromise between achieving rapid solution and diffusion of carbon and minimizing grain growth. The optimal...
Abstract
This article introduces some of the general sources of heat treating problems with particular emphasis on problems caused by the actual heat treating process and the significant thermal and transformation stresses within a heat treated part. It addresses the design and material factors that cause a part to fail during heat treatment. The article discusses the problems associated with heating and furnaces, quenching media, quenching stresses, hardenability, tempering, carburizing, carbonitriding, and nitriding as well as potential stainless steel problems and problems associated with nonferrous heat treatments. The processes involved in cold working of certain ferrous and nonferrous alloys are also covered.
Series: ASM Handbook
Volume: 1
Publisher: ASM International
Published: 01 January 1990
DOI: 10.31399/asm.hb.v01.a0001022
EISBN: 978-1-62708-161-0
... Titanium can behave as both a grain refiner and a precipitate strengthener, depending on its content ( Ref 3 ). At compositions greater than 0.050%, titanium carbides begin to exert a strengthening effect. However, at this time, titanium is used commercially to retard austenite grain growth and thus...
Abstract
Two high-strength low-alloy (HSLA) families, acicular-ferrite steels and pearlite-reduced steels, contain microalloying additions of vanadium and niobium. Vanadium, niobium, and titanium combine preferentially with carbon and/or nitrogen to form a fine dispersion of precipitated particles in the steel matrix. This article summarizes the metallurgical effects of vanadium, niobium, molybdenum, and titanium. The metallurgical fundamentals were first applied to forgings in the early 1970s. The ultimate strength of first- and second-generation microalloy steels is adequate for many engineering applications, but these steels do not achieve the toughness of conventional quenched and tempered alloys under normal hot-forging conditions. Third-generation microalloy steels differ from their predecessors in that they are direct quenched from the forging temperature to produce microstructures of lath martensite with uniformly distributed temper carbides. Without subsequent heat treatment, these materials achieve properties, including toughness, similar to those of standard quenched and tempered steels.
Book Chapter
Microstructures and Characterization of Gray Irons
Available to PurchaseSeries: ASM Handbook
Volume: 1A
Publisher: ASM International
Published: 31 August 2017
DOI: 10.31399/asm.hb.v01a.a0006343
EISBN: 978-1-62708-179-5
... at the start of solidification. In the case of hypoeutectic composition, for example, nucleation of a solid phase begins with austenite formation, with some dissolved carbon in the austenite. Some graphite may form during solidification of a hypoeutectic cast iron, because the growth of austenite grains...
Abstract
This article discusses the characterization of gray iron structures, following the sequence of structure formation, as it applies to unalloyed or low-alloyed gray iron. Austenite grains are the basic crystallographic entities of the metallic matrix in gray cast iron precipitated from the liquid melt. The article describes the macrostructure and dendrite morphology of primary austenite. Eutectoid transformation in the solid state causes the transformation of austenite to pearlite and/or ferrite, producing the as-cast structure. The article discusses the observations of the graphite and ferritic/pearlitic structure in as-cast gray iron.
Book Chapter
Physical Metallurgy Concepts in Interpretation of Microstructures
Available to PurchaseSeries: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003723
EISBN: 978-1-62708-177-1
... are useful in determining the conditions for proper heat treatment (solid-state transformation) of metals and alloys. The influence of the mechanisms of phase nucleation and growth on the morphology, size, and distribution of grains and second phases is also described. bainite eutectic alloy system...
Abstract
This article introduces basic physical metallurgy concepts that may be useful for understanding and interpreting variations in metallographic features and how processing affects microstructure. It presents some basic concepts in structure-property relationships. The article describes the use of equilibrium binary phase diagrams as a tool in the interpretation of microstructures. It reviews an account of the two types of solid-state phase transformations: isothermal and athermal. The article discusses isothermal transformation and continuous cooling transformation diagrams which are useful in determining the conditions for proper heat treatment (solid-state transformation) of metals and alloys. The influence of the mechanisms of phase nucleation and growth on the morphology, size, and distribution of grains and second phases is also described.
Book Chapter
Modeling of Metallurgical Microstructure Evolution in Fusion Welding
Available to PurchaseSeries: ASM Handbook
Volume: 6A
Publisher: ASM International
Published: 31 October 2011
DOI: 10.31399/asm.hb.v06a.a0005599
EISBN: 978-1-62708-174-0
... to extensive austenite grain growth within the high-peak-temperature regions of the HAZ, with consequent formation of undesirable (low-toughness) microstructures such as upper bainite and Widmanstätten ferrite during the γ-to-α transformation. Fig. 3 Schematic diagrams showing some characteristic...
Abstract
This article focuses on the general internal state variable method, and its simplification, for single-parameter models, in which the microstructure evolution may be treated as an isokinetic reaction. It explains that isokinetic microstructure models are applied to diffusional transformations in fusion welding, covering particle dissolution, growth, and coarsening of precipitates in the heat-affected zone. The article discusses the versatility of the internal state variable approach in modeling of nonisothermal transformations for various materials and processes. It describes the process models applied to predict the microstructure evolution in Al-Mg-Si alloys during multistage thermal processing involving heat treatment and welding. The article also provides information on the microstructure models exploited in engineering design to optimize the load-bearing capacity of welded aluminum components.
Book Chapter
Computational Models for Prediction of Solidification Microstructure
Available to PurchaseSeries: ASM Handbook
Volume: 1A
Publisher: ASM International
Published: 31 August 2017
DOI: 10.31399/asm.hb.v01a.a0006314
EISBN: 978-1-62708-179-5
... of undercooling, and the location of the nucleated grains is chosen randomly. As soon as an austenite grain forms, it begins to grow as a sphere with the growth rate v γ , i = A ⋅ Δ T / r γ , i ( Ref 60 ), where A is a constant equal to 2.87 × 10 −13 [m 2 K −1 s −1 ], Δ T is the undercooling, r γ , i...
Abstract
The microstructure that develops during the solidification stage of cast iron largely influences the subsequent solid-state transformations and mechanical properties of the cast components. This article provides a brief introduction of methods that can be used for simulating the solidification microstructure of cast iron. Analytical as well as numerical models describing solidification phenomena at both macroscopic and microscopic scales are presented. The article introduces macroscopic transport equations and presents analytical microscopic models for solidification. These models include the dendrite growth models and the cooperative eutectic growth models. The article provides some solutions using numerical models to simulate the kinetics of microstructure formation in cast iron. It concludes with a discussion on cellular automaton (CA) technique that can handle complex topology changes and reproduce most of the solidification microstructure features observed experimentally.
Series: ASM Handbook
Volume: 1A
Publisher: ASM International
Published: 31 August 2017
DOI: 10.31399/asm.hb.v01a.a0006319
EISBN: 978-1-62708-179-5
... reviews several factors, such as presence of graphite and austenite grain size, which affect the transformation rate of austenite during austempering of free-graphite cast irons. austenite austenite grain size austenite-to-ausferrite transformation bainite cast iron graphite heat treatment...
Abstract
The transformation of austenite of cast irons represents a more complex and less studied subject. This article discusses the general features of the decomposition of austenite into bainite. It describes the heat treatment cycles of austempered cast iron microstructure. The article reviews several factors, such as presence of graphite and austenite grain size, which affect the transformation rate of austenite during austempering of free-graphite cast irons.
Book Chapter
Bulk Formability of Steels
Available to PurchaseSeries: ASM Handbook
Volume: 1
Publisher: ASM International
Published: 01 January 1990
DOI: 10.31399/asm.hb.v01.a0001032
EISBN: 978-1-62708-161-0
... with the addition of austenite grain-growth inhibitors such as titanium nitride to refine the starting austenitic grain size and to restrict grain growth after recrystallization. Such processing would obviate the need for low-temperature controlled rolling ( Ref 11 , 12 , 13 ). However, even with optimum...
Abstract
This article discusses the bulk formability or workability of steels. It describes their formability characteristics and presents procedures for various formability tests used for carbon and alloy steels. Tests for bulk formability can be divided into two main categories: primary tests and specialized tests. The article compares the processing of microalloyed plate and bar products. The article focuses on the use of torsion testing to evaluate the forgeability of carbon and alloy steels and presents information on measuring flow stress. The article discusses the metallurgy and thermomechanical processing of high-strength low-alloy (microalloyed) steels and the various parts of the rolling operation. The article summarizes some of the common tests for determining formability in open-die and closed-die forgings.
Book Chapter
Microstructure Evolution during the Liquid/Solid Transformation in Cast Iron
Available to PurchaseSeries: ASM Handbook
Volume: 1A
Publisher: ASM International
Published: 31 August 2017
DOI: 10.31399/asm.hb.v01a.a0006304
EISBN: 978-1-62708-179-5
... Abstract The solidification of hypoeutectic cast iron starts with the nucleation and growth of austenite dendrites, while that of hypereutectic iron starts with the crystallization of primary graphite in the stable system or cementite in the metastable system. This article begins...
Abstract
The solidification of hypoeutectic cast iron starts with the nucleation and growth of austenite dendrites, while that of hypereutectic iron starts with the crystallization of primary graphite in the stable system or cementite in the metastable system. This article begins with a discussion on the nucleation and growth of austenite dendrites. It describes the nucleation of lamellar graphite, spheroidal graphite, and austenite-iron carbide eutectic. The article reviews three main graphite morphologies crystallizing from the iron melts during solidification: lamellar (LG), compacted or vermicular (CG), and spheroidal. It discusses the metastable solidification of austenite-iron carbide eutectic and concludes with information on gray-to-white structural transition of cast iron.
Book Chapter
High-Strength Structural and High-Strength Low-Alloy Steels
Available to PurchaseSeries: ASM Handbook
Volume: 1
Publisher: ASM International
Published: 01 January 1990
DOI: 10.31399/asm.hb.v01.a0001025
EISBN: 978-1-62708-161-0
... cooling from austenitizing temperatures and produces essentially the same ferrite-pearlite microstructure as that of hot-rolled carbon steel, except that the heat treatment produces a finer grain size. This grain refinement makes the steel stronger, tougher, and more uniform throughout. Typical product...
Abstract
This article considers four types of high-strength structural steels: heat-treated low-alloy steels, as-rolled carbon-manganese steels, heat-treated (normalized or quenched and tempered) carbon steels, and as-rolled high-strength low-alloy (HSLA) steels (which are also known as microalloyed steels). The article places emphasis on HSLA steels, which are an attractive alternative in structural applications because of their competitive price per-yield strength ratios. HSLA steels are primarily hot-rolled into the usual wrought product forms and are furnished in the as-hot-rolled condition. In addition to hot-rolled products, HSLA steels are also furnished as cold-rolled sheet and forgings. This article describes the different categories of HSLA steels and provides a summary of characteristics and intended uses of HSLA steels described in the American Society for Testing and Materials (ASTM) specifications. The article also presents some applications of HSLA steels.
Book Chapter
Solid-State Transformations
Available to PurchaseBook: Alloy Phase Diagrams
Series: ASM Handbook
Volume: 3
Publisher: ASM International
Published: 27 April 2016
DOI: 10.31399/asm.hb.v03.a0006228
EISBN: 978-1-62708-163-4
.... As shown in Fig. 7 , either ferrite or cementite nuclei form at austenite grain boundaries and then grow as colonies into the austenite grains, with the layers oriented in essentially the same direction within the colony. The concurrent growth of several colonies leads to the formation of a larger nodule...
Abstract
Eutectoid and peritectoid transformations are classified as solid-state invariant transformations. This article focuses primarily on the structures from eutectoid transformations with emphasis on the classic iron-carbon system of steel. It reviews peritectoid phase equilibria that are very common in several binary systems. The addition of substitutional alloying elements causes the eutectoid composition and temperature to shift in the iron-carbon system. The article graphically illustrates the effect of various substitutional alloying elements on the eutectoid transformation temperature and effective carbon content. The partitioning effect of substitutional alloying elements, such as chromium, manganese, and silicon, in pearlitic steel is also illustrated.
Book Chapter
Microstructures and Properties of Carburized Steels
Available to PurchaseSeries: ASM Handbook
Volume: 4D
Publisher: ASM International
Published: 01 October 2014
DOI: 10.31399/asm.hb.v04d.a0005982
EISBN: 978-1-62708-168-9
... inhibit grain growth and maintain very fine austenitic grain sizes. Figure 6 shows a martensite-carbide microstructure formed by reheating and quenching a carburized 8620 steel. The small, white, spherical particles are carbides retained during austenitizing and quenching. The matrix structure etches...
Abstract
This article describes the microstructure, properties, and performance of carburized steels, and elucidates the microstructural gradients associated with carbon and hardness gradients. It provides information on case depth measurement, the factors affecting case depth, and the formation and causes of microcracks. The article discusses the effects of alloying elements on hardenability, the effects of excessive retained austenite and massive carbides on fatigue resistance, the effects of residual stresses and internal oxidation on fatigue performance of carburized steels. In addition, the causes of intergranular fracture at austenite grain boundaries and their prevention methods are explored. The article also describes the major mechanisms of bending fatigue crack initiation in carburized steels.
Book Chapter
Solidification Structures of Steels and Cast Irons
Available to PurchaseSeries: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003725
EISBN: 978-1-62708-177-1
... solidification experiments. The typical dendritic structure of steel revealed by such a technique is presented in Fig. 1 ( Ref 1 ). The as-cast grain structure of steel can often be observed using classic metallographic etching because ferrite forms at the austenite grain boundaries during solid-state...
Abstract
The ferrous metals are the most significant class of commercial alloys. This article describes the solidification structures of plain carbon steel, low-alloy steel, high-alloy steel, and cast iron, with illustrations. The formation of nonmetallic inclusions in the liquid before and during solidification is also discussed.
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