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Series: ASM Handbook
Volume: 5B
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v05b.a0006005
EISBN: 978-1-62708-172-6
.... atomic number chemical bonding organic compounds polymers protective coatings BY VIRTUE OF ALL OF THE MANY TYPES of resins, pigments, solvents, and other constituents comprising a formulated coating, chemistry is an important consideration in this Volume. All of the articles in the Coating...
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003083
EISBN: 978-1-62708-199-3
... includes a series of tables: the first gives the names and symbols of the elements in alphabetical order and the second lists the elements in order by atomic number and give the atomic weight for each. The periodic table of the elements also is included in the article. actinides alkali metals...
Abstract
Chemical elements are the basic chemical substances; that is, they cannot be decomposed by chemical change or made by chemical union. These elements follow a periodic pattern related to the atomic mass of each that allows them to be arranged into a convenient table. This article includes a series of tables: the first gives the names and symbols of the elements in alphabetical order and the second lists the elements in order by atomic number and give the atomic weight for each. The periodic table of the elements also is included in the article.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006638
EISBN: 978-1-62708-213-6
... significance of the raw analytical total. Sections on accuracy of the standards-based k-ratio/matrix corrections protocol with EDS and processes of analysis when severe peak overlap occurs are also included. The article provides information on low-atomic-number elements, iterative qualitative-quantitative...
Abstract
This article is a detailed account of the principles of electron-excited X-ray microanalysis. It begins by discussing the physical basis of electron-excited X-ray microanalysis and the advantages and limitations of energy dispersive spectrometry (EDS) and wavelength dispersive spectrometry for electron probe microanalysis. Key concepts for performing qualitative analysis and quantitative analysis by electron-excited X-ray spectrometry are then presented. Several sources that lead to measurement uncertainties in the k-ratio/matrix corrections protocol are provided, along with the significance of the raw analytical total. Sections on accuracy of the standards-based k-ratio/matrix corrections protocol with EDS and processes of analysis when severe peak overlap occurs are also included. The article provides information on low-atomic-number elements, iterative qualitative-quantitative analysis for complex compositions, and significance of standardless analysis in the EDS software. It ends with a section on the processes involved in elemental mapping for major and minor constituents.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006653
EISBN: 978-1-62708-213-6
... lengths for absorption measurements to only a few millimeters. The measured absorbance is proportional to the number of absorbing species (i.e., gaseous atoms) within the optical viewing volume ( Ref 1 , 6 ). Therefore, the absorbance is related to both the path length of the incident light within...
Abstract
This article focuses on some of the factors pertinent to atomic absorption spectroscopy (AAS). It begins by describing the working principle, critical components, and construction of flame atomic absorption instrumentation. This is followed by sections discussing various types of interferences in AAS, namely vaporization, ionization, matrix interferences, and background correction. Some of the methods for the analysis of microliter-sized samples and methods of standard additions to the sample solution for generating calibration standards are then reviewed. The article concludes with a section on processes involved in matrix matching.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006658
EISBN: 978-1-62708-213-6
.... Fig. 20 A 2 × 2 μm atomic force microscopy image of an indium/tin oxide thin film deposited on a glass substrate. Nanometer-sized features are directly observed in this image. It should be noted that this material in optically transparent. With the advent of nanotechnology, a number of...
Abstract
This article focuses on laboratory atomic force microscopes (AFMs) used in ambient air and liquid environments. It begins with a discussion on the origin of AFM and development trends occurring in AFM. This is followed by a section on the general principles of AFM and a comprehensive list of AFM scanning modes. There is a brief description of how each mode works and what types of applications can be made with each mode. Some of the processes involved in preparation of samples (bulk materials and those placed on a substrate) scanned in an AFM are then presented. The article provides information on the factors applicable to the accuracy and precision of AFM measurements. It ends by discussing the applications for AFMs in the fields of science, technology, and engineering.
Book Chapter
Book: Alloy Phase Diagrams
Series: ASM Handbook
Volume: 3
Publisher: ASM International
Published: 27 April 2016
DOI: 10.31399/asm.hb.v03.a0006292
EISBN: 978-1-62708-163-4
... parameters for some of the simple metallic crystals. A table that lists the crystal structures of various metal elements is presented. The crystal structures are described by the Pearson symbols for crystal system, space lattice, total number of atoms per unit cell, and prototype structure. The article...
Abstract
This article defines crystallographic terms and concepts, including crystal structure, unit cell, structure symbols, lattice, space-group notation, and atom position. It schematically illustrates the atom positions, prototypes, structure symbols, space-group notations, and lattice parameters for some of the simple metallic crystals. A table that lists the crystal structures of various metal elements is presented. The crystal structures are described by the Pearson symbols for crystal system, space lattice, total number of atoms per unit cell, and prototype structure. The article tabulates the assorted structure types of metallurgical interest arranged according to Pearson symbol. It also provides information on crystal defects in all real crystals, explaining some significant ones, such as point defects, line defects, stacking faults, and twins.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006277
EISBN: 978-1-62708-169-6
... number of Burgers correspondence variants and orientation variants. The article also includes calculation of the transformation strain with contributions from defect structures developed at alpha/beta interfaces as a precipitates grow in size. In the CALculation of PHAse Diagram (CALPHAD) framework, the...
Abstract
This article describes the integration of thermodynamic modeling, mobility database, and phase-transformation crystallography into phase-field modeling and its combination with transformation texture modeling to predict phase equilibrium, phase transformation, microstructure evolution, and transformation texture development during heat treatment of multicomponent alpha/beta and beta titanium alloys. It includes quantitative description of Burgers orientation relationship and path, discussion of lattice correspondence between the alpha and beta phases, and determination of the total number of Burgers correspondence variants and orientation variants. The article also includes calculation of the transformation strain with contributions from defect structures developed at alpha/beta interfaces as a precipitates grow in size. In the CALculation of PHAse Diagram (CALPHAD) framework, the Gibbs free energies and atomic mobilities are established as functions of temperature, pressure, and composition and serve directly as key inputs of any microstructure modeling. The article presents examples of the integrated computation tool set in simulating microstructural evolution.
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005225
EISBN: 978-1-62708-187-0
... processes are the enormous amounts of solid remelting, compositional mixing, and equilibration that occur at and close to the preform top surface. Spray casting is an intrinsic or self-grain-refining casting process in which the purpose of the distinctive atomization step is to generate a large number...
Abstract
Spray casting, also known as spray forming, is a niche casting process for the manufacture of preforms. This article lists commercial examples of alloys manufactured by spray casting and provides sequential steps of the spray casting process. Gas atomization is a chaotic, stochastic process that always produces a wide range of droplet diameters. The article schematically illustrates typical log-normal droplet diameter probability density distribution on a mass or volume basis obtained by gas atomization. It also illustrates the changes in solid fraction during the spray casting process as a function of axial distance from the point of droplet atomization. The article concludes with a section on occurrence of macrosegregation and coarsening in spray cast preforms.
Book Chapter
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005819
EISBN: 978-1-62708-165-8
... structure is referred to as an allotropy (existing in another form). For example, both iron and carbon have a number of allotropic forms. Carbon can exist as diamond, soot, graphite, and the more recently discovered form of fullerenes. However, the allotropy of carbon is not a significant variable as an...
Abstract
The heat treatment of steel is based on the physical metallurgical principles that relate to its processing, properties, and structure. The microstructures that result from the heat treatment of steel are composed of one or more phases in which the atoms of iron, carbon, and other elements in steel are associated. This article describes the phases of heat treated steel, and provides information on effect of temperature change and the size of carbon atoms relative to that of iron atoms during the heat treatment.
Series: ASM Handbook
Volume: 22A
Publisher: ASM International
Published: 01 December 2009
DOI: 10.31399/asm.hb.v22a.a0005441
EISBN: 978-1-62708-196-2
... (33) × 10 −34 J · s Pianck constant/2π h ( bar ) 1.054571628 (53) × 10 −34 J · s Avogadro constant (number) N A 6.02214179 (30) × 10 23 mol −1 Atomic mass unit amu or u 1.660538782 (83) × 10 −27 kg Electron rest mass m e 9.10938215 (45) × 10 −31 kg Proton...
Abstract
This article presents a comprehensive collection of tables that list fundamental physical constants, standard atomic weights, melting points, atomic size parameters, heats of transition, thermal properties, temperature-dependent allotropic structures, pressure-dependent allotropic structures, and magnetic phase transition temperatures of the elements.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006628
EISBN: 978-1-62708-213-6
... Z 1 is the atomic number of the projectile, Z 2 is the atomic number of the target atom, e is the unit electrical charge, a is the ZBL screening length, and a 0 is the first Bohr radius. The TFM potential is expressed as ( Ref 11 ): (Eq 5) V r = Z 1 Z 2 r e...
Abstract
This article is a brief account of low-energy ion-scattering spectroscopy (LEIS) for determining the atomic structure of solid surfaces. It begins with a description of the general principles of LEIS. This is followed by a section providing information on the equipment used for LEIS. Various steps involved in the sample preparation, calibration, and data analysis are then discussed. The article concludes with a section on the applications and interpretation of LEIS in material analysis, including discussion on surface structural analysis, layer-by-layer (Frank-van der Merwe) growth, and low-energy atom-scattering spectroscopy.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003084
EISBN: 978-1-62708-199-3
... letter to identify the crystal system and a capital letter to identify the space lattice. To these is added a number equal to the number of atoms in the unit cell conventionally selected for the particular crystal type. When determining the number of atoms in the unit cell, it should be remembered that...
Abstract
Crystal structure is the arrangement of atoms or molecules in the solid state that involves consideration of defects, or abnormalities, in idealized atomic/molecular arrangements. The three-dimensional aggregation of unit cells in the crystal forms a space lattice or Bravais lattice. This article provides a brief review of the terms and basic concepts associated with crystal structures. It also discusses some of the significant defects obstructing plastic flow in real crystals, namely point defects, line defects, stacking faults, twins, and cold work. Several tables in the article provide information on the crystal structures and lattice parameters of allotropes of metallic elements.
Book: Surface Engineering
Series: ASM Handbook
Volume: 5
Publisher: ASM International
Published: 01 January 1994
DOI: 10.31399/asm.hb.v05.a0001288
EISBN: 978-1-62708-170-2
... defined as the number of atoms ejected from the target surface per incident ion. The sputtering yield is dependent on the characteristics of the target material, incident ion energy, ion mass, and angle of incidence, as shown in Table 1 . Detailed studies of sputtering yields for a large variety of...
Abstract
Sputtering is a nonthermal vaporization process in which the surface atoms are physically ejected from a surface by momentum transfer from an energetic bombarding species of atomic/molecular size. It uses a glow discharge or an ion beam to generate a flux of ions incident on the target surface. This article provides an overview of the advantages and limitations of sputter deposition. It focuses on the most common sputtering techniques, namely, diode sputtering, radio-frequency sputtering, triode sputtering, magnetron sputtering, and unbalanced magnetron sputtering. The article discusses the fundamentals of plasma formation and the interactions on the target surface. A comparison of reactive and nonreactive sputtering is also provided. The article concludes with a discussion on the several methods of process control and the applications of sputtered films.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006647
EISBN: 978-1-62708-213-6
..., with an energy corresponding to the difference between the two energy levels. According to the laws of quantum mechanics, the electrons surrounding an atom can only attain a limited number of discrete energy levels. Therefore, each element is associated with a characteristic emission spectrum. This...
Abstract
This article provides a clear but nonexhaustive description of the general principle of atomic emission, with a particular focus on instrumentation, and summarizes the main characteristics of the inductively coupled plasma optical emission spectrometer technique. Basic atomic theory as well as the instrument characteristics and their influence on the instrument performances are presented. The advantages, drawbacks, and developments of this technique are discussed, and, finally, alternative techniques and examples of applications are provided.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003251
EISBN: 978-1-62708-199-3
...) Random solid solution: All planes have equal numbers of A and B atoms, hence equal average scattering power, scattered beams from planes I and II are 180° out of phase and equal in amplitude, so net diffracted intensity is zero. (b) Ordered compound: Adjacent planes are made up entirely of A and B atoms...
Abstract
X-ray diffraction (XRD) is the most extensively used method for identifying and characterizing various aspects of metals related to the arrangements and spacings of their atoms for bulk structural analysis. XRD techniques are also applicable to ceramics, geologic materials, and most inorganic chemical compounds. This article describes the operating principles and types of XRD analyses, along with information about the threshold sensitivity and precision, limitations, sample requirements, and capabilities of related techniques. The necessary instrumentation for XRD analyses include the Debye-Scherrer camera and the X-ray diffractometer. The article also describes the uses of XRD analyses, such as the identification of phases or compounds in metals and ceramics; detection of order and disorder transformation; determination of lattice parameters and changes in lattice parameters due to alloying and temperature effects; measurement of residual stresses; characterization of crystallite size and perfection; characterization of preferred orientations; and determination of single crystal orientations.
Book Chapter
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006678
EISBN: 978-1-62708-213-6
... structure and composition of materials is due to the differential absorption of x-rays by materials of different density, composition, and homogeneity. The higher the atomic number of a material, the more x-rays are absorbed. Microstructural analysis is the combined characterization of the...
Abstract
This article briefly discusses popular techniques for metals characterization. It begins with a description of the most common techniques for determining chemical composition of metals, namely X-ray fluorescence, optical emission spectroscopy, inductively coupled plasma optical emission spectroscopy, high-temperature combustion, and inert gas fusion. This is followed by a section on techniques for determining the atomic structure of crystals, namely X-ray diffraction, neutron diffraction, and electron diffraction. Types of electron microscopies most commonly used for microstructural analysis of metals, such as scanning electron microscopy, electron probe microanalysis, and transmission electron microscopy, are then reviewed. The article contains tables listing analytical methods used for characterization of metals and alloys and surface analysis techniques. It ends by discussing the objective of metallography.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006675
EISBN: 978-1-62708-213-6
... an atomic number of lithium and higher, chemical state identification of surface elements, composition and chemical state depth profiles with ion gun sputtering, determination of oxidation states of metal atoms in metal compounds, identification of surface contaminations, measurement of surface film...
Abstract
This article is an overview of the division Surface Analysis of this volume. The division covers various developed surface-analysis techniques, such as scanning probe and atomic force microscopy. The division focuses on the analysis of surface layers that are less than 100 nm. A quick reference summary of surface-analysis methods is presented in this article.
Book Chapter
Book: Alloy Phase Diagrams
Series: ASM Handbook
Volume: 3
Publisher: ASM International
Published: 27 April 2016
DOI: 10.31399/asm.hb.v03.a0006223
EISBN: 978-1-62708-163-4
... randomly arranged and the entropy of mixing is given by Eq 28 . In such a solution it can also be shown that: (Eq 38) P A B = N a z X A A X B B where N a is Avogadro's number, and z is the number of bonds per atom. If ε < 0, the atoms in the solution will...
Abstract
Thermodynamic descriptions have become available for a large number of alloy systems and allow the calculation of the phase diagrams of multicomponent alloys. This article begins with a discussion on three laws of thermodynamics: the Law of Conservation of Energy, the Second Law of Thermodynamics, and the Third Law of Thermodynamics. It informs that for transformations that occur at a constant temperature and pressure, the relative stability of the system is determined by its Gibbs free energy. The article describes the Gibbs free energy of a single-component unary system and the Gibbs free energy of a binary solution. It schematically illustrates the structure of a binary solid solution with interatomic bonds and shows how the equilibrium state of an alloy can be obtained from the free-energy curves at a given temperature. The article concludes with information on the construction of eutectic and binary phase diagrams from Gibbs free-energy curves.
Series: ASM Handbook
Volume: 5B
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v05b.a0006025
EISBN: 978-1-62708-172-6
... Abstract The process of transferring coating materials from the container to the surface to be coated can be accomplished in a number of ways. This article describes seven methods of coating application: brushes, rollers, and daubers; conventional air spray; high-volume low-pressure spray...
Abstract
The process of transferring coating materials from the container to the surface to be coated can be accomplished in a number of ways. This article describes seven methods of coating application: brushes, rollers, and daubers; conventional air spray; high-volume low-pressure spray; airless spray; air-assisted airless spray; plural-component spray; and electrostatic spray. Factors to be considered when deciding on an application method include the size and configuration of the surfaces to be coated, the type of coating being applied, environmental regulations/restrictions, the proximity to other operations or personnel, and the recommendations of the coating manufacturer.
Series: ASM Handbook
Volume: 23
Publisher: ASM International
Published: 01 June 2012
DOI: 10.31399/asm.hb.v23.a0005685
EISBN: 978-1-62708-198-6
... energy of the emitted Auger electron is characteristic of the element from which it was emitted. Because the Auger process is a three-electron process, only elements with an atomic number equal to or greater than three (lithium) can be analyzed using this technique. Detection and energy analysis of the...
Abstract
This article focuses on the modes of operation, physical basis, sample requirements, properties characterized, advantages, and limitations of common characterization methods that are used to evaluate the physical morphology and chemical properties of component surfaces for medical devices. The methods include light microscopy, scanning electron microscopy, atomic force microscopy, energy-dispersive x-ray spectroscopy, Auger electron spectroscopy, secondary ion mass spectrometry, x-ray photoelectron spectroscopy, Fourier transform infrared spectroscopy, and Raman spectroscopy.