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Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006262
EISBN: 978-1-62708-169-6
... reaging tment with each step conducted immediately after one another Fig. 3 Temperature-time profile of production retrogression and reaging treatment with each step conducted separately Abstract Retrogression and reaging (RRA) is an established form of postquench aging heat treatment...
Abstract
Retrogression and reaging (RRA) is an established form of postquench aging heat treatment. RRA treatments can be applied to precipitation-hardened aluminum alloys that are used in aerospace applications. This article provides information on the development background of RRA and the steps involved in the RRA treatments. It discusses the process descriptions, applications, microstructural consequences, and limitations of RRA. In addition, the article describes the influence of RRA on mechanical properties.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003204
EISBN: 978-1-62708-199-3
...) Artificially aged in laboratory from T4 to T6 Table 1(c) Typical solution and precipitation heat treatments for heat-treatable Zn-Mg aluminum alloys from the 7 xxx series Alloy Product form Solution heat treatment (a) Precipitation heat treatment Metal temperature (b) Temper...
Abstract
This article discusses different heat treating techniques, including quenching, homogenizing, annealing, stress relieving, stress equalizing, quench hardening, strain hardening, tempering, solution heat treating, and precipitation heat treating (age hardening) for different grades of aluminum alloys, copper alloys, magnesium alloys, nickel and nickel alloys, and titanium and titanium alloys and its product forms.
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005230
EISBN: 978-1-62708-187-0
... center of a specimen are shown in Fig. 1 , respectively. Aging refers to the controlled breakdown of supersaturated solid solution at room temperature (natural aging) or at elevated temperature (artificial aging) to form nanosized precipitates in the matrix. These precipitates strengthen materials by...
Abstract
This article provides an overview of heat treatment processes, namely, solution heat treatment, quenching, and natural and artificial aging. It contains a table that lists various heat treatment tempers commonly practiced for nonferrous castings. The article describes microstructural changes that occur due to the heat treatment of cast alloys.
Series: ASM Handbook
Volume: 14A
Publisher: ASM International
Published: 01 January 2005
DOI: 10.31399/asm.hb.v14a.a0004014
EISBN: 978-1-62708-185-6
... be stress relieved, annealed, and/or aged differently after flow forming to alter the mechanical properties. Table 3 lists resulting mechanical properties of various materials in different conditions after cold flow forming. Table 2 Alloys flow formed at ambient and elevated temperatures...
Abstract
A wide range of flow-formed open- and close-ended shapes are currently available in a variety of difficult-to-form materials, including titanium alloys and nickel-base super alloys. This article describes the two basic methods of flow forming that are characterized by the position of the rolls during the forming process. The flow forming methods include staggered-roll flow forming process and in-line flow-forming process. Typical mechanical properties of flow-formed materials in various conditions are summarized in a table. Proper process controls and subsequent product qualification tests are critical to assure optimal performance of the flow-formed tubular component. The article discusses the most commonly required process control parameters and the effects of forming speed and temperature in the flow forming process.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006268
EISBN: 978-1-62708-169-6
... on the application envisaged. In the course of aging, the solid solution decomposes into various phases as the atoms dissolved in the aluminum matrix start diffusing, mediated by excess or equilibrium vacancies. In a first stage, small clusters of solute atoms are formed—most likely by homogeneous...
Abstract
This article describes the effects of alloying and heat treatment on the metastable transition precipitates that occur in age hardenable aluminum alloys. Early precipitation stages are less well understood than later ones. This article details the aging sequence and characteristics of precipitates that occur in the natural aging and artificial aging of Al-Mg-Si-(Cu) alloys, Al-Mg-Cu alloys, microalloyed Al-Mg-Cu-(Ag, Si) alloys, aluminum-lithium-base alloys, and Al-Zn-Mg-(Cu) alloys. Crystal structure, composition, dimensions, and aging conditions of precipitates are detailed. Effects of reversion, duplex annealing, and retrogression and re-aging are included.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006288
EISBN: 978-1-62708-169-6
... Aluminum-lithium alloys with age hardening from the continuous precipitation of δ′ (Al 3 Li) Table 1 Typical solution and precipitation heat treatments for commercial heat treatable aluminum alloy mill products with copper alloying Alloy Product form Solution heat treatment Precipitation...
Abstract
This article focuses on the aging characteristics of solution and precipitation heat treated aluminum alloy systems and their corresponding types. It includes information on aluminum-copper systems, aluminum-copper-magnesium systems, aluminum-magnesium-silicon systems, aluminum-zinc-magnesium systems, aluminum-zinc-magnesium-copper systems, and aluminum-lithium alloys.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006259
EISBN: 978-1-62708-169-6
... typical properties and compositions of silver-copper alloys and gold jewelry alloys such as colored gold alloys and white gold alloys. annealing gold alloys precious metals silver-copper alloys PRECIOUS METALS comprise gold (Au), silver (Ag), platinum (Pt), palladium (Pd), iridium (Ir...
Abstract
This article describes the annealing behavior of precious metals, namely, gold, silver, platinum, palladium, iridium, rhodium, ruthenium, and osmium. It discusses the annealing practices and their effect on the basic properties of common precious metal alloys. The article presents the typical properties and compositions of silver-copper alloys and gold jewelry alloys such as colored gold alloys and white gold alloys.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006287
EISBN: 978-1-62708-169-6
... treatment, so that the particles act as heterogeneous nucleation sites for the η phase. Precipitates are fine phases or clusters that form during aging of a supersaturated solid solution (see also the article “Age Hardening of Aluminum Alloys” in this Volume). In many (but not all) metals, alloying...
Abstract
This article describes the general categories and metallurgy of heat treatable aluminum alloys. It briefly reviews the key impurities and each of the principal alloying elements in aluminum alloys, namely, copper, magnesium, manganese, silicon, zinc, iron, lithium, titanium, boron, zirconium, chromium, vanadium, scandium, nickel, tin, and bismuth. The article discusses the secondary phases in aluminum alloys, namely, nonmetallic inclusions, porosity, primary particles, constituent particles, dispersoids, precipitates, grain and dislocation structure, and crystallographic texture. It also discusses the mechanisms used for strengthening aluminum alloys, including solid-solution hardening, grain-size strengthening, work or strain hardening, and precipitation hardening. The process of precipitation hardening involves solution heat treatment, quenching, and subsequent aging of the as-quenched supersaturated solid solution. The article briefly discusses these processes of precipitation hardening. It also reviews precipitation in various alloy systems, including 2xxx, 6xxx, 7xxx, aluminum-lithium, and Al-Mg-Li systems.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006274
EISBN: 978-1-62708-169-6
... following variables must be closely controlled: Solution temperature Time at temperature Time lapse between furnace and quenching medium Cooling rate The third step involves aging, where the supersaturated solid solution forms new precipitates or dispersions of fine particles. If this...
Abstract
This article describes the different types of precipitation and transformation processes and their effects that can occur during heat treatment of various nonferrous alloys. The nonferrous alloys are aluminum alloys, copper alloys, magnesium alloys, nickel alloys, titanium alloys, cobalt alloys, zinc alloys, and heat treatable silver alloys, gold alloys, lead alloys, and tin alloys. It also provides a detailed discussion on the effects due to precipitation and transformation processes in these non-ferrous alloys.
Book Chapter
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006275
EISBN: 978-1-62708-169-6
... quickly followed by softening as the coarse structure is formed. At suitable solute concentrations in lead-antimony alloys, the structure may remain single phase with hardening by Guinier-Preston (GP) zones formed during aging. At higher concentrations, and in certain other systems, aging may produce...
Abstract
This article discusses the various heat treating processes, namely, solid-solution hardening, solution treating, solution aging and dispersion hardening, for low-melting-point alloys such as lead alloys, tin-rich alloys, and zinc alloys. Heat treating of tin-rich alloys has been practiced for bearing alloys, pewterware, and organ pipe alloys. The article reviews the principles underlying these applications.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006264
EISBN: 978-1-62708-169-6
... found immediately after casting. In other words, the treatment was used to dissolve the GP zones and other precipitates that had formed by natural aging since the alloy was cast. However, this short solution treatment was not sufficient to completely homogenize the structure. Immediately following the...
Abstract
This article presents a detailed discussion on typical thermal treatment practices for hardening of various aluminum casting alloys. These practices are solution treatment, quenching or cooling, preaging, and artificial aging at an elevated temperature. The aluminum casting alloys considered here are: Al-Cu and Al-Cu-Mg (2xx) alloys, Al-Zn-Mg (7xx) alloys, Al-Si-Mg alloys, Al-Si-Cu, and Al-Si-Cu-Mg alloys.
Book Chapter
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003180
EISBN: 978-1-62708-199-3
...-formed parts should be fully annealed after final forming. If annealing causes distortion, the work can be formed within 10% of the intended shape, annealed, pickled, and then given the final forming. Depending on the size, amount, and dispersion of secondary phases, the age-hardenable alloys show...
Abstract
Characteristics of stainless steel that affect its formability include yield strength, tensile strength, and ductility, in addition to the effect of work hardening on these properties. This article discusses the forming process of stainless steel, heat-resistant alloys and refractory metals, detailing the major aspects of forming, including formability, lubrication, and forming methods and tools. The effect of factors such as alloy condition, cold reduction, forming direction (in the case of heat-resistant alloys) and temperature (in the case of refractory metals) on formability is also discussed.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003203
EISBN: 978-1-62708-199-3
... increase ductility to facilitate forming or machining, prepare for welding, relieve stresses after welding, produce specific microstructures, or soften age-hardened structures by resolution of second phases. Solution treating is intended to dissolve second phases to produce maximum corrosion resistance or...
Abstract
Heat treating of stainless steel produces changes in physical condition, mechanical properties, and residual stress level and restores maximum corrosion resistance when that property has been adversely affected by previous fabrication or heating. This article focuses on annealing of different types of stainless steels such as austenitic, ferritic, duplex, martensitic, and precipitation-hardening, and on the heat treatment of superalloys and refractory metals. It discusses the recommended procedures for solution annealing, austenite conditioning, transformation cooling, and age tempering of precipitation-hardening stainless steels. The article also lists general recommendations for the annealing temperatures of tantalum, niobium, molybdenum, tungsten, and their alloys.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006265
EISBN: 978-1-62708-169-6
...), Inconel (Ni-Cr-Mo), Hastelloy (Ni-Mo-Cr), and Incoloy (Ni-Fe-Cr) families of alloys. The heat treatment processes for gamma prime nickel alloys, gamma prime nickel-iron superalloys, and gamma double-prime nickel-iron superalloys are also included. The article also provides information on age-hardenable...
Abstract
This article describes the heat treatment of wrought solid-solution and precipitation-hardening alloys with a focus on the major families of wrought nickel alloys. It also provides information on the heat treatment of some representative solid-solution alloys in the Monel (Ni-Cu), Inconel (Ni-Cr-Mo), Hastelloy (Ni-Mo-Cr), and Incoloy (Ni-Fe-Cr) families of alloys. The heat treatment processes for gamma prime nickel alloys, gamma prime nickel-iron superalloys, and gamma double-prime nickel-iron superalloys are also included. The article also provides information on age-hardenable alloys, and the effects of cold work on aging response and grain growth with examples.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006263
EISBN: 978-1-62708-169-6
... because of the finer microstructural scale. Quenching from lower temperatures may create a volume fraction of metastable β, with the maximum volume depending on the alloy composition. Aging this metastable β will form a fine dispersion of α within the β phase. Therefore, the more martensite (and/or...
Abstract
This article provides a detailed discussion on the heat treatment processes for titanium and titanium alloys. These processes are age hardening, solution treatment, aging, and annealing. The article illustrates the characteristics of equilibrium phase diagrams that are important for understanding the heat treatment of titanium alloys. It explains the types of metastable phases encountered in titanium alloys. The article also provides information on the equilibrium phase relationships and properties of titanium alloys.
Series: ASM Handbook
Volume: 14A
Publisher: ASM International
Published: 01 January 2005
DOI: 10.31399/asm.hb.v14a.a0004010
EISBN: 978-1-62708-185-6
...-alpha titanium alloys. A longitudinal section of the macrostructure of a typical roll formed VT25 disk after heat treatment (solution at 950 °C, or 1740 °F, for 1 h followed by aging at 530 °C, or 990 °F, for 6 h) is shown in Fig. 11(a) . The microstructure at various positions in the disk is shown in...
Abstract
This article describes the roll forming of components of nickel, titanium, and aluminum alloys. The metallurgical characteristics of the roll formed components, such as macrostructures, microstructures, tensile strength, and stress rupture performance, are discussed. The article compares the resulting properties of roll formed and conventionally forged components.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006258
EISBN: 978-1-62708-169-6
... hydrogen atmosphere is employed to remove some of the brittle Mg-Zn-RE grain-boundary phases. The addition of silver and neodymium-rich mischmetal promotes age hardening when the alloy is given a full T6 treatment. The precipitates formed are relatively stable, and the alloy shows high mechanical strength...
Abstract
Magnesium-matrix composites (MgMCs) are very promising as structural materials because of their low density, high specific strength, and excellent castability. This article provides information on the characteristics, mechanical properties, and applications of magnesium alloys and composites. It discusses the microstructures used for the most common magnesium alloys used in metal-matrix composites, namely, magnesium-aluminum, magnesium-rare earth and magnesium-lithium alloys. The article focuses on the most common methods of heat treatment, including solution heat treatment, precipitation strengthening or aging, and annealing, applied to these alloys. Finally, it describes the microstructural aspects and precipitate-matrix relationships of MgMCs as well as the heat treatment methods for MgMCs.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006285
EISBN: 978-1-62708-169-6
... enhance formability, such as required for superplastic forming O3 Homogenized H Strain hardened (i.e., for non-age-hardening alloys, wrought products only); this temper applies to products that have their strength increased by strain hardening, with or without supplementary thermal treatment to...
Abstract
Annealing is an essential treatment in the fabrication of metal parts and semiproducts. This article discusses the processes involved in annealing, namely, recovery, recrystallization, and grain coarsening. It lists the heat treatment conditions of processed aluminum alloys. It provides information on the types of heat treatment, which include preheating, full anneal, stabilization, and stoving. The article describes the steps involved for achieving the age-hardening effect and the strongest hardening effect in aluminum. The steps to increase the strength of aluminum alloys by extremely fine, dispersed second-phase particles are: solution heat treatment, quenching, and age hardening. Finally, the article also discusses the process parameters of annealing, including the effect of strain, effect of temperature, effect of heating rate, and the effect of alloy elements, and the effect of annealing on anisotropy.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006281
EISBN: 978-1-62708-169-6
.... Bronzes originally (from the time of the Bronze Age) referred to alloys in which tin was the major alloying element. Today (2016), however, the term bronze is commonly used for a number of alloys that contain other elements with little, if any, tin. Bronzes can refer to copper alloys with various...
Abstract
Bronzes generally are used to describe many different copper-base alloys in which the major alloying addition is neither zinc nor nickel. They are generally classified by their major alloying elements, for example, tin bronzes with phosphorus used as a deoxidizer, aluminum bronzes, nickel-aluminum bronzes, silicon bronzes, and beryllium bronzes. This article briefly discusses the types, hardening mechanisms, heat treatment processes, applications, and mechanical properties of these bronzes and high-copper alloys.
Series: ASM Handbook
Volume: 4E
Publisher: ASM International
Published: 01 June 2016
DOI: 10.31399/asm.hb.v04e.a0006289
EISBN: 978-1-62708-169-6
... basis, even when magnesium and zinc are present in the ratio to form MgZn 2 . Table 4 shows typical values of electrical conductivity for some common aluminum alloys and tempers. Note the relatively strong effect of artificial aging on the conductivity values for the 2 xxx and 7 xxx alloys, which...
Abstract
Heat treatment of aluminum alloys is assessed by various quality-assurance methods that include metallographic examination, hardness measurements, mechanical property tests, corrosion-resistance tests, and electrical conductivity testing. The use of hardness measurements in the quality assurance of heat treated aluminum products is effectively used in conjunction with the measurement of surface electrical conductivity. This article provides a detailed discussion of the error sources in eddy-current conductivity measurements. It also presents useful information on the variation of electrical conductivity of alloy 2024 samples as a function of aging time at different isothermal holding temperatures.