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Image
The DSC thermogram representing a molding resin pellet that had produced br...
Available to PurchasePublished: 01 January 2002
Fig. 20 The DSC thermogram representing a molding resin pellet that had produced brittle parts. The thermogram shows a major melting transition associated with nylon 6/12 and a weaker transition attributed to polypropylene.
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Image
The DSC thermogram representing a second molding resin pellet that had prod...
Available to PurchasePublished: 01 January 2002
Fig. 21 The DSC thermogram representing a second molding resin pellet that had produced brittle parts. The thermogram shows a major melting transition associated with nylon 6/12 and a weaker transition attributed to nylon 6/6.
More
Image
Differential scanning calorimetry thermogram representing a molding resin p...
Available to PurchasePublished: 15 December 2019
Fig. 8 Differential scanning calorimetry thermogram representing a molding resin pellet that had produced brittle parts. The thermogram shows a major melting transition associated with nylon 6/12 and a weaker transition attributed to polypropylene. Source: Ref 6
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Image
Differential scanning calorimetry thermogram representing a molding resin p...
Available to PurchasePublished: 15 December 2019
Fig. 9 Differential scanning calorimetry thermogram representing a molding resin pellet that had produced brittle parts. The thermogram shows a major melting transition associated with nylon 6/12 and a weaker transition attributed to polypropylene. Source: Ref 6
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Book Chapter
Resin Transfer Molding and Structural Reaction Injection Molding
Available to PurchaseSeries: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003020
EISBN: 978-1-62708-200-6
... Abstract Resin transfer molding (RTM) and structural reaction injection molding (SRIM) are two similar processes that are well suited to the manufacture of large, complex, and high-performance structures. This article discusses the similarities and differences of RTM and SRIM processes...
Abstract
Resin transfer molding (RTM) and structural reaction injection molding (SRIM) are two similar processes that are well suited to the manufacture of large, complex, and high-performance structures. This article discusses the similarities and differences of RTM and SRIM processes and the unique design considerations with respect to the physical properties, geometry, surface quality, process economics, equipment, and tooling of a component that should be considered in choosing RTM or SRIM over other competing processes for fabricating reinforced components.
Book Chapter
Resin Transfer Molding and Structural Reaction Injection Molding
Available to PurchaseBook: Composites
Series: ASM Handbook Archive
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003413
EISBN: 978-1-62708-195-5
... Abstract Resin transfer molding and structural reaction injection molding belong to a family, sometimes denoted as liquid composite molding. This article provides information on the characteristics and automotive and aerospace applications of liquid composite molding. It reviews techniques...
Abstract
Resin transfer molding and structural reaction injection molding belong to a family, sometimes denoted as liquid composite molding. This article provides information on the characteristics and automotive and aerospace applications of liquid composite molding. It reviews techniques that use hard tooling and positive (superatmospheric) pressures to produce structures. The techniques include vacuum-assisted resin injection, vacuum infusion, resin-film infusion, and injection-compression molding. The article provides an overview of the materials that are commonly used together with some of processing characteristics that are important to processing speed and part quality. It concludes with a discussion on design guidelines for the liquid composite molding.
Series: ASM Desk Editions
Publisher: ASM International
Published: 01 December 1998
DOI: 10.31399/asm.hb.mhde2.a0003172
EISBN: 978-1-62708-199-3
..., dry sand molds, resin-bonded sand molds, and sodium silicate bonded sand. The article describes the casting processes that use these molds, including the no-bake process, cold box process, hot box process, the CO2 process, lost foam casting process and vacuum molding process. The casting processes...
Abstract
This article discusses classification of foundry processes based on the molding medium, such as sand molds, ceramic molds, and metallic molds. Sand molds can be briefly classified into two types: bonded sand molds, and unbonded sand molds. Bonded sand molds include green sand molds, dry sand molds, resin-bonded sand molds, and sodium silicate bonded sand. The article describes the casting processes that use these molds, including the no-bake process, cold box process, hot box process, the CO2 process, lost foam casting process and vacuum molding process. The casting processes that use ceramic molds include investment casting, and plaster casting. Metallic molds are used in permanent mold casting, die casting, semisolid casting, and centrifugal casting.
Series: ASM Handbook
Volume: 20
Publisher: ASM International
Published: 01 January 1997
DOI: 10.31399/asm.hb.v20.a0002492
EISBN: 978-1-62708-194-8
... contact molding, compression-type molding, resin-injection molding, and pultrusion are described. The article also discusses the various factors to be considered in designing for composite manufacturing. ceramic matrix composites composite manufacture compression-type molding contact molding...
Abstract
The goal of design is to improve the overall performance of the metal or ceramic matrix rather than to create a material with different response than the base matrix. This article focuses on the design for manufacturing polymeric composites. Specially developed methods including contact molding, compression-type molding, resin-injection molding, and pultrusion are described. The article also discusses the various factors to be considered in designing for composite manufacturing.
Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006672
EISBN: 978-1-62708-213-6
... such as molecular weight, crystallinity, and orientation, and this has a significant impact on the properties of the molded article. Additionally, plastic resins usually contain additives, such as reinforcing fillers, plasticizers, colorants, antidegradants, and process aids. It is this combination of molecular...
Abstract
Differential scanning calorimetry (DSC) is the most common thermal technique for polymer characterization. This article provides a detailed account of the various factors and processes involved in DSC. The discussion covers the equipment used, specimen preparation process, calibration requirements, data analysis, and provides examples of the applications and interpretation of DSC.
Book Chapter
Characterization of Plastics in Failure Analysis
Available to PurchaseSeries: ASM Handbook
Volume: 11B
Publisher: ASM International
Published: 15 May 2022
DOI: 10.31399/asm.hb.v11B.a0006933
EISBN: 978-1-62708-395-9
... distribution, crystallinity, tacticity, molecular orientation, and fusion. These characteristics have a significant impact on the properties of the molded article. Additionally, plastic resins are formulated with additives such as reinforcing fillers, plasticizers, colorants, antidegradants, and process aids...
Abstract
This article reviews analytical techniques that are most often used in plastic component failure analysis. The description of the techniques is intended to familiarize the reader with the general principles and benefits of the methodologies, namely Fourier transform infrared spectroscopy, energy-dispersive x-ray spectroscopy, differential scanning calorimetry, thermogravimetric analysis, and dynamic mechanical analysis. The article describes the methods for molecular weight assessment and mechanical testing to evaluate plastics and polymers. The descriptions of the analytical techniques are supplemented by a series of case studies to illustrate the significance of each method. The case studies also include pertinent visual examination results and the corresponding images that aided in the characterization of the failures.
Book Chapter
Characterization of Plastics in Failure Analysis
Available to PurchaseSeries: ASM Handbook Archive
Volume: 11
Publisher: ASM International
Published: 01 January 2002
DOI: 10.31399/asm.hb.v11.a0003525
EISBN: 978-1-62708-180-1
... ways but is most often taken as the inflection point of the step transition. A composite thermogram showing the glass transitions of several common plastic materials is presented in Fig. 7 . The T g of an amorphous resin has an important impact on the mechanical properties of the molded article...
Abstract
This article reviews the analytical techniques most commonly used in plastic component failure analysis. These include the Fourier transform infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, thermomechanical analysis, and dynamic mechanical analysis. The descriptions of the analytical techniques are supplemented by a series of case studies that include pertinent visual examination results and the corresponding images that aid in the characterization of the failures. The article describes the methods used for determining the molecular weight of a plastic resin. It explains the use of mechanical testing in failure analysis and also describes the considerations in the selection and use of test methods.
Book Chapter
Mounting of Specimens
Available to PurchaseSeries: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0003786
EISBN: 978-1-62708-177-1
... on compression molded mounts, which are molded with thermoplastic and thermosetting resins. The article reviews several resins and their key factors, which help in the selection of the most appropriate mounting method and resin. It also discusses the characteristics of plastic mounting materials. The article...
Abstract
Mounting of the specimen is often desirable or necessary for handling and metallographic polishing after the specimen is cut into an appropriate size. This article illustrates the different mechanical clamps used in mounting small specimens. It provides useful information on compression molded mounts, which are molded with thermoplastic and thermosetting resins. The article reviews several resins and their key factors, which help in the selection of the most appropriate mounting method and resin. It also discusses the characteristics of plastic mounting materials. The article provides information on the molds and resins used for castable mounts, vacuum treatment of mounts, special mount arrangements, and mount marking and storage.
Image
Thermogravimetric analysis thermogram comparison showing a difference in th...
Available to Purchase
in Characterization of Plastics in Failure Analysis
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
Fig. 19 Thermogravimetric analysis thermogram comparison showing a difference in the weight-loss profiles of the molding resin and the failed housing material
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Image
Differential scanning calorimetry thermogram comparison of first heating re...
Available to Purchase
in Characterization of Plastics in Failure Analysis
> Characterization and Failure Analysis of Plastics
Published: 15 May 2022
Fig. 32 Differential scanning calorimetry thermogram comparison of first heating results for the (a) molding resin and (b) failed part. An endotherm is present in the results obtained on the failed window material. The endotherm is characteristic of the melting of crystalline structure within
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Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005252
EISBN: 978-1-62708-187-0
... for preparation of resin-sand mixture for shell molding, namely, mixing resin and sand according to conventional dry mixing techniques, and coating the sand with resin. Shaping of shell molds and cores from resin sand mixtures is accomplished in machines. The article discusses the major steps in producing a mold...
Abstract
Shell molding is used for making production quantities of castings that range in weight from a few ounces to approximately 180 kg (400 lb), in both ferrous and nonferrous metals. This article lists the limitations or disadvantages of shell mold casting. It describes the two methods for preparation of resin-sand mixture for shell molding, namely, mixing resin and sand according to conventional dry mixing techniques, and coating the sand with resin. Shaping of shell molds and cores from resin sand mixtures is accomplished in machines. The article discusses the major steps in producing a mold or core and describes the problems most frequently encountered in shell-mold casting. The problems include mold cracking, soft molds, low hot tensile strength of molds, peelback, and mold shift. The article concludes with information on examples that provide some relative cost comparisons between shell molding and green sand molding.
Book Chapter
Rotational Molding
Available to PurchaseSeries: ASM Desk Editions
Publisher: ASM International
Published: 01 November 1995
DOI: 10.31399/asm.hb.emde.a0003017
EISBN: 978-1-62708-200-6
... function and property requirements for resins and additives; size, shape, design, and cost of molded parts; equipment type and size; and the type of mold to be used. Commonly used molds include cast aluminum, fabricated sheet metal, nickel deposit, machined aluminum, silicone, fiberglass, and prototype...
Abstract
Rotational molding is a simple but unique process that has the capability of producing small to large hollow items with very uniform wall thicknesses. Providing an overview of the operating principles of rotational molding, this article discusses the key selection factors, including function and property requirements for resins and additives; size, shape, design, and cost of molded parts; equipment type and size; and the type of mold to be used. Commonly used molds include cast aluminum, fabricated sheet metal, nickel deposit, machined aluminum, silicone, fiberglass, and prototype molds.
Book: Composites
Series: ASM Handbook Archive
Volume: 21
Publisher: ASM International
Published: 01 January 2001
DOI: 10.31399/asm.hb.v21.a0003398
EISBN: 978-1-62708-195-5
... the resin selection in designing the composite for use in a particular application. The article illustrates the various methods that are used to process a composite component, namely, wet lay-up, autoclave, resin transfer molding, and vacuum-assisted resin transfer molding. It provides a discussion...
Abstract
This article presents the basic guidelines considered in designing a composite structure, and the basic definitions of terms that apply to composites. It describes the analysis of a composite laminate based on stress-strain relationships, stress-strain load relationships, general load displacement case, and general load case solution. Factors affecting the composite materials properties and allowables of fiber-reinforced polymers are reviewed. The article discusses the process considerations for mold design, such as master model, metal tooling, composite tooling, and tool care. It explains the resin selection in designing the composite for use in a particular application. The article illustrates the various methods that are used to process a composite component, namely, wet lay-up, autoclave, resin transfer molding, and vacuum-assisted resin transfer molding. It provides a discussion on electromagnetic interference shielding, electrostatic discharge protection, metal plating, fire resistance, and corrosion resistance on composite materials.
Book Chapter
Introduction—Composite Materials and Optical Microscopy
Available to PurchaseSeries: ASM Handbook
Volume: 9
Publisher: ASM International
Published: 01 December 2004
DOI: 10.31399/asm.hb.v09.a0009071
EISBN: 978-1-62708-177-1
... transfer molding, vacuum-assisted resin transfer molding, and resin film infusion. It explains the composite- and matrix-toughening methods for fiber-reinforced composites, such as dispersed-phase toughening and interlayer toughening. The article concludes with information on optical microscopy, which...
Abstract
This article illustrates the polymer matrices used for composite materials. It describes the use of prepeg materials in manufacturing high-performance composites. The article discusses the various infusion processes for the development of fiber-reinforced composites, namely, resin transfer molding, vacuum-assisted resin transfer molding, and resin film infusion. It explains the composite- and matrix-toughening methods for fiber-reinforced composites, such as dispersed-phase toughening and interlayer toughening. The article concludes with information on optical microscopy, which provides an insight into the micro- and macrostructure of fiber-reinforced composites.
Image
Published: 01 January 2001
Book Chapter
Thermogravimetric Analysis
Available to PurchaseSeries: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006673
EISBN: 978-1-62708-213-6
... in part supplier had taken place between the approval of the prototype parts and the receipt of the first lot of production parts. The mechanical hinges were specified to be injection molded from an impact-modified, 13% glass-fiber-reinforced nylon 6/6 resin. A resin substitution was suspected...
Abstract
Thermogravimetric analysis (TGA) is a thermal analysis technique that measures the amount and rate of change in the weight of a material as a function of temperature or time in a controlled atmosphere. This article provides a detailed account of the concepts of TGA, covering the various criteria to be considered for specimen preparation and calibration of TGAs. The use of thermogravimetric analysis data in the assessment of failure analysis of plastics and the combined usage of TGA with other techniques to understand the changes in the sample are also covered. The article provides examples of applications and provides information on the interpretation of TGA.
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