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Differential scanning calorimetry

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Series: ASM Handbook
Volume: 10
Publisher: ASM International
Published: 15 December 2019
DOI: 10.31399/asm.hb.v10.a0006672
EISBN: 978-1-62708-213-6
... Abstract Differential scanning calorimetry (DSC) is the most common thermal technique for polymer characterization. This article provides a detailed account of the various factors and processes involved in DSC. The discussion covers the equipment used, specimen preparation process, calibration...
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Published: 01 June 2016
Fig. 27 Diagram of differential thermal analysis/differential scanning calorimetry chamber More
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Published: 30 September 2015
Fig. 21 Differential scanning calorimetry plot with an exothermic crystallization event and an endothermic melting event. Courtesy of KTA-Tator, Inc. More
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Published: 30 September 2015
Fig. 22 Differential scanning calorimetry spectrum of metallic zinc control revealing peak area of metallic zinc of 108 J/g. Courtesy of KTA-Tator, Inc. More
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Published: 30 September 2015
Fig. 23 Differential scanning calorimetry spectrum revealing sample peak area of metallic zinc of 98.0 J/g. Courtesy of KTA-Tator, Inc. More
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Published: 30 September 2015
Fig. 24 Differential scanning calorimetry spectrum revealing partially cured coating. Courtesy of KTA-Tator, Inc. More
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Published: 30 September 2015
Fig. 25 Differential scanning calorimetry spectrum revealing the original sample reheated under the same conditions. Courtesy of KTA-Tator, Inc. More
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Published: 15 May 2022
Fig. 25 Differential scanning calorimetry thermogram More
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Published: 15 May 2022
Fig. 27 Differential scanning calorimetry of polyethylene/polypropylene blend 10 mcal/s range; 20 °C/min (36 °F/min). PE, polyethylene; PP, polypropylene. Source: Ref 38 More
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Published: 01 June 2016
Fig. 45 Differential scanning calorimetry examination of quench-rate effects in 7075 at different distances (mm) from the quenched end of a Jominy end quench specimen. Source: Ref 57 More
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Published: 01 June 2016
Fig. 21 Differential scanning calorimetry examination of quench-rate effects in 7075 at different distances (mm) from the quenched end of a Jominy end-quench specimen. GP, Guinier-Preston. Source: Ref 32 More
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Published: 01 June 2016
Fig. 3 Differential scanning calorimetry trace of alloy Al-0.6Mg-0.8Si started directly after quenching. The heating rate is 10 K/s. GP, Guinier-Preston. Adapted from Ref 7 More
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Published: 01 January 2005
Fig. 15 Differential scanning calorimetry cell More
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Published: 01 January 2005
Fig. 5 Differential scanning calorimetry cell. 5, specimen; R, reference More
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Published: 01 November 1995
Fig. 5 Schematic differential scanning calorimetry thermogram More
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Published: 01 November 1995
Fig. 6 Differential scanning calorimetry thermogram of polyethylene/polypropylene blend, 10 mcal/s range, 20 °C (36 °F)/min heating rate. PE, polyethylene; PP, polypropylene. Source: Ref 56 More
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Published: 01 November 1995
Fig. 7 Differential scanning calorimetry determination of the effect of a plasticizer on T m of nylon 11. Range, 0.0024 W (10 mcal/s); heating rate, 20 °C/min (36 °F/min); weight, 6.8 mg (0.105 gr), both samples. Source: Ref 51 More
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Published: 01 November 1995
Fig. 8 Differential scanning calorimetry determination of polyethylene in impact polycarbonate. Range, 0.00048 W (2 mcal/s; heating rate, 20 °C/min (36 °F/min); weight, 23 mg (0.355 gr). Source: Ref 51 More
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Published: 01 November 1995
Fig. 10 Differential scanning calorimetry thermogram of Fiberite 934 epoxy, 4.89 mg (0.075 gr), 10 °C/min (18 °F/min) heating rate More
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Published: 01 January 2002
Fig. 5 Differential scanning calorimetry thermogram showing various transitions associated with polymeric materials. The (I) indicates that the numerical temperature was determined as the inflection point on the curve. More