This article describes the general factors that can influence fracture appearances. The focus is on the general practical relationships of fracture appearances, with factors presented in some broad categories, including: material conditions (e.g., crystal structure and microstructure); loading conditions (stress state, strain rate, and fatigue); manufacturing conditions (casting, metal-working, machining, heat treatment, etc.); and service and environmental factors (hydrogen embrittlement, stress corrosion, temperature, and corrosion fatigue).

This article discusses the importance of the care and handling of fracture specimens and what to look for during the preliminary field or laboratory observation and collection, the preservation of specimens, and the cleaning and preparation of fracture specimens for additional analyses. The preservation of nonmetallic specimens, medical devices, oversized components, light alloys, nondestructively tested components, and materials that are part of legal proceedings is addressed.

This article focuses on the fractography features of the conventional powdered metal (PM) process for ferrous powders. It discusses porosity, which is one of the inherent features present in components produced by conventional press-and-sinter processes, and green cracks, which are the most common fracture issue in conventional PM processes. It explains the effect of post-sintering operations. The article also presents the common ferrous powder metallurgy materials.

This article describes some of the underlying factors of tool steel and bearing steel fractures and appearances. It also briefly introduces the general types of cold work and hot work tool steels and their typical performance requirements. This includes the importance of microstructural conditions achieved with powder metallurgy (PM) tool steels and the need for steel “cleanliness,” especially in preventing contact fatigue in bearings or bending fatigue in gears.

This article discusses an experimental setup and a measuring setup for capturing acoustic emission during quenching. It presents the procedure for sound-emission measurement and an analysis of the acoustic spectrum obtained during quenching.

This article explains cooling mechanisms involving saltwater solutions used as quenchants. The analyses of cooling power include studies of cooling curves, heat-transfer coefficients, and cooling rates. The influence of other bath parameters, such as temperature and agitation, is also discussed. The article discusses solute additions and several factors impacting quenching.

The role of a mixer/agitator in quenching applications is to control the mixing environment in order to meet the process criteria. This article provides the basic fundamentals of the sizing of agitators, tank geometry importance, and other considerations for the application of agitators in quench tanks. It also discusses the differing methods for the sizing and selection of agitators for quench tank applications.

Computational fluid dynamics (CFD) provides an efficient, alternate, virtual approach for simulating and analyzing quenching processes with an impact on component design, manufacturing process, and quality. This article provides domain insights for quenching researchers and CFD practitioners for the modeling of the industrial quenching process and for supporting the diverse multifunctional needs in an industry, ranging from primary metallurgical companies (steel, aluminum, and other alloys), original equipment manufacturers, engineering companies, captive and commercial heat treating facilities, quench system manufacturers, and quench fluid suppliers. It describes the governing differential equations for the fluid flow and heat-transfer phenomena during quenching. The article also discusses different modeling categories to determine a CFD methodology for quenching.

Martempering and austempering processes may eliminate the need for conventional oil quenching and tempering. This article presents the suitability of steels for martempering and austempering. It discusses the compositions of oils suitable for marquenching and modified marquenching and also presents safety precautions recommended for the use of martempering oils. Finally, the article explains the effect of agitation and water in a molten salt bath.

Steels are among the most versatile materials in modifying their microstructure and properties by heat treatment. This article outlines the basic concepts of physical metallurgy relating to the heat treatment of steel. It considers the phases and microstructures of steel together with the transformations observed and critical temperatures during heat treatment. Additionally, the different types of steels, heat treatments, and their purposes are also discussed.

Hardening and depth of hardening of steel is a critically important material and process design parameter. This article presents a selective overview of experimental and predictive procedures to determine steel hardenability. It also covers the breadth of steel hardenability, ranging from shallow, to very difficult to harden, to air-hardening steels.

This article presents the modes of heat transfer and the stages of cooling during quenching. It provides an overview on the wetting process and then focuses on the evaluation of heat transfer during quenching. It also presents the challenges of thermal process evaluation based on an inverse heat conduction analysis. The article contains a compilation of best practice examples on heat transfer evaluation, which are intended to represent the practical aspects and applicability of the methods aiming the prediction of heat-transfer coefficients.

In this article, a metallurgical overview of the hardening process is provided. This overview is followed by the methodology involved in obtaining cooling curves, the currently accepted standardized methods of testing, and the use of newer methods of cooling curve data interpretation that describe the quenching process.

Flow visualization is an important characterization process to not only understand uniformity of the interfacial cooling mechanisms, but also to characterize the overall impact of agitation on the uniformity of the overall cooling process. This article focuses on thermal flow simulation and visualization in the quenching process. The study presents the effect of bubbling, boiling, and breaking the steam film on the heat-transfer coefficient during the agitated quenching process.

In this article, an in-depth overview of petroleum quenching oils is provided, including oil composition, use, mechanism of the oil quenching processes, oil degradation, toxicology and safety, and quenching bath maintenance.

This article presents the fundamentals and nomenclature of polymer quenchants and provides a detailed discussion on the polymers used for quenching formulation. The article describes the effect of polymer structure on the quenching mechanism. It also presents the factors affecting polymer quenchant performance. The article details the use of polymer quenchants for intensive quenching and then focuses on the wire patenting processes and polymer quenchant analysis. The article presents the application of polymer quenchants for induction hardening. Finally, it provides details on cooling curve analysis of polymer quenchants.

This article focuses on the quenching properties of vegetable and animal oils, including toxicity and biodegradability of vegetable/animal oils. The article provides a detailed discussion on the oxidation of vegetable/animal oils. The addition of antioxidants to stabilize soybean and palm oils is discussed, and the article concludes that substantially better performance is required if vegetable oils are to be effective functional equivalents to petroleum oil formulations. This may be done by selecting different vegetable oil compositions with less unsaturation, by applying genetic modification of soybean seed oils, or by chemically modifying and stabilizing the vegetable oil structure.

This article details investigations on the characterization of various nanofluids as quenchants for industrial heat treatment. It provides a discussion on the preparation, stability, thermophysical properties, and wetting characteristics of nanofluids. The article explains the mechanism of heat transfer in nanofluids and discusses the effect of the deposition of nanoparticles on the probe surface. The article also presents the microstructure and mechanical properties of steel quenched in nanofluids.

Agitation is one of the most critical areas of quench system design. This article provides an overview of the impact of agitation on quench uniformity, followed by a general discussion of the selection and use of various types of agitators, including recirculation pumps, jet mixers, forced air (sparging), and impellers. A brief overview of heat-exchanger types and their selection criteria is also provided, along with simplified calculations for approximating heat-exchange requirements. The methods of selecting a quenchant are provided. Recommendations for system maintenance are also described. Much effort is placed on the proper design of the furnace for temperature and atmosphere uniformity, proper temperature control, and exact carbon potential. However, the design of the quench tank can have a drastic effect on the overall system performance, with proper design ensuring proper mechanical properties (hardness, strength, and fracture toughness) as well as distortion control.

Intensive quenching (IQ) is an alternative method of hardening steel parts. Two types of IQ methods are used in heat treating practice: IQ-2 and IQ-3. IQ-2 is implemented in IQ water tanks, which are usually used for batch quenching of steel parts. IQ-3 is conducted in single-part processing using high-velocity water flow IQ units. This article presents a detailed description of IQ technology, related equipment, and IQ applications. A review of intensive quench system design and processing is provided, including numerical design criteria, steel selection, quenchants, properties (especially optimal residual stress profiles). Several specific applications of intensive quenching are also provided.