This article focuses on the theory, advantages, and limitations of various methods used for the determination of surface area, density, and porosity of powder. These include gas adsorption, permeametry, pycnometry, and mercury porosimetry. Information on various equipment used in these processes are also provided.

This article describes testing and characterization methods of ceramics for chemical analysis, phase analysis, microstructural analysis, macroscopic property characterization, strength and proof testing, thermophysical property testing, and nondestructive evaluation techniques. Chemical analysis is carried out by X-ray fluorescence spectrometry, atomic absorption spectrophotometry, and plasma-emission spectrophotometry. Phase analysis is done by X-ray diffraction, spectroscopic methods, thermal analysis, and quantitative analysis. Techniques used for microstructural analysis include reflected light microscopy using polarized light, scanning electron microscopy, transmission electron microscopy, energy dispersive analysis of X-rays, and wavelength dispersive analysis of X-rays. Macroscopic property characterization involves measurement of porosity, density, and surface area. The article describes testing methods such as room and high-temperature strength test methods, proof testing, fracture toughness measurement, and hardness and wear testing. It also explains methods for determining thermal expansion, thermal conductivity, heat capacity, and emissivity of ceramics and glass and measurement of these properties as a function of temperature.

Most surfaces have regular and irregular spacings that tend to form a pattern or texture on the surface. This article provides information on the general background of surface topography and discusses the different methods for measuring surface topography, namely, contact and noncontact techniques, and the focus-follow method. Examples of different types of parameters obtained and how they are applied can best be described by discussing the various types of surfaces generated by finishing methods. The surfaces include ground, turned, and milled machined surfaces; surfaces subjected to stress; bearing surfaces; plateau honed and tapped surfaces; and reflective, painted, elastic, and wear-resistant surfaces.