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Series: ASM Handbook
Volume: 24
Publisher: ASM International
Published: 15 June 2020
DOI: 10.31399/asm.hb.v24.a0006568
EISBN: 978-1-62708-290-7
Abstract
Powder-bed additive manufacturing (AM) processes are some of the most commonly used techniques, necessitating the accurate measurement of powder flowability properties. This article discusses some powder flow tests that occur in powder-bed AM machines. These include the Hall/Carney flow test, bulk/tap density, rheometer, and the revolving or rotating drum technique. The three categories of powder properties that are available from rheometer experiments are discussed: bulk, dynamic flow, and shear properties. The article also describes the basic principles and applications of micro-X-ray computed tomography in studying powder porosity characteristics nondestructively.
Book Chapter
Series: ASM Handbook
Volume: 2B
Publisher: ASM International
Published: 15 June 2019
DOI: 10.31399/asm.hb.v02b.a0006605
EISBN: 978-1-62708-210-5
Series: ASM Handbook
Volume: 17
Publisher: ASM International
Published: 01 August 2018
DOI: 10.31399/asm.hb.v17.a0006445
EISBN: 978-1-62708-190-0
Abstract
The potential for introducing defects during processing becomes greater as the relative density of pressed and sintered powder metallurgy (PM) parts increases and more multilevel parts with complex geometric shapes are produced. This article discusses the potential defects in pressed and sintered PM parts: density variations, compaction and ejection cracks, microlaminations, poor degree of sintering, and voids from prior lubricant agglomerates. It describes the various methods applicable to green compacts: direct-current resistivity testing, radiographic techniques, computed tomography, and gamma-ray density determination. The article also discusses the methods for automated nondestructive testing of pressed and sintered PM parts: acoustic methods-resonance testing, eddy current testing, magnetic bridge comparator testing, ultrasonic techniques, radiographic techniques, gamma-ray density determination, and visual inspection.
Series: ASM Handbook
Volume: 18
Publisher: ASM International
Published: 31 December 2017
DOI: 10.31399/asm.hb.v18.a0006383
EISBN: 978-1-62708-192-4
Abstract
This article focuses on different aspects of wear particle analysis. It discusses the different wear regimes in the wear rate versus time (bathtub) curve. The article explains the essence of condition monitoring and how to properly sample lubricants for condition monitoring. It also discusses in-service lubricant analysis for condition monitoring, focusing on the spectrometric oil analysis program. The article describes the characteristics of wear particles and analytical techniques for characterizing them. It also describes the characteristics of different types of wear particles and the mechanisms by which they are generated. The article concludes with a summary of the major applications of wear particle analysis.
Series: ASM Handbook
Volume: 18
Publisher: ASM International
Published: 31 December 2017
DOI: 10.31399/asm.hb.v18.a0006415
EISBN: 978-1-62708-192-4
Abstract
Tribocorrosion is the subject dealing with complex, synergistic effects of chemical and mechanical conditions that cause wear. This article begins with a discussion on oxidative wear and corrosive wear, as well as quantitative measurements of corrosion, mechanical wear, and wear-corrosion effects. It illustrates the mechanism of corrosive-abrasive wear and discusses the factors affecting two-body wear. These factors include particle shape, size, density, and hardness; slurry velocity; slurry particle angle of attack; solids concentration in the slurry; hydrodynamic factors; corrosion products and the mass transfer of oxygen. The article describes slurry particle impingement tests and grinding tribocorrosion tests, as well as the factors to be considered for mitigating corrosive wear, such as materials selection, surface treatments, and environment modifications.
Series: ASM Handbook
Volume: 1A
Publisher: ASM International
Published: 31 August 2017
DOI: 10.31399/asm.hb.v01a.a0006324
EISBN: 978-1-62708-179-5
Abstract
This article discusses the influence of microstructure and chemical composition on the physical properties of cast iron. The physical properties include density, thermal expansion, thermal conductivity, specific heat, electrical conductivity, magnetic properties, and acoustic properties. The article describes the properties of liquid iron in terms of surface energy, contact angles, and viscosity. The conductive properties such as thermal and electrical conductivity, of the main metallographic phases present in cast iron are presented in a table. The article discusses the magnetic properties of cast iron in terms of magnetic intensity, magnetic induction, magnetic permeability, remanent magnetism, coercive force, and hysteresis loss. It concludes with a discussion on the acoustic properties of cast iron.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006088
EISBN: 978-1-62708-175-7
Abstract
Blending of powders is defined as the thorough intermingling of powders of the same nominal composition. Premixing is the preparation of a uniform mixture of two or more components. This article provides information on the blending and premixing variables required to produce adequate results in the powder mixture. It describes the effects of metal powder characteristics on blending and mixing: particle size, shape, density, and surface features. The article also provides information on the equipment, tumble-type blenders, and low-shear agitated-type blenders used for blending and premixing solids.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006097
EISBN: 978-1-62708-175-7
Abstract
This article provides an overview of the compaction of metal powder in a rigid die and reviews the compaction characteristics of stainless steel powders, including green density, compressibility, green strength, apparent density, flow rate, and sintered density. It describes the influence of compaction characteristics of stainless steel powders in tool materials selection, lubrication, annealing, double pressing/double sintering, and warm compaction.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006107
EISBN: 978-1-62708-175-7
Abstract
This article focuses on the theory, advantages, and limitations of various methods used for the determination of surface area, density, and porosity of powder. These include gas adsorption, permeametry, pycnometry, and mercury porosimetry. Information on various equipment used in these processes are also provided.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006127
EISBN: 978-1-62708-175-7
Abstract
Powder metallurgy (PM) high-alloy tool steels (HATS) have unique properties that assist them in solving various problems related to machining of metal components. This article describes the cost-intensive PM processing routes of HATS, as well as their major properties, including elastic properties, density, mechanical properties, grindability, fatigue and wear resistance, and thermophysical properties.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006129
EISBN: 978-1-62708-175-7
Abstract
This article describes the effects of undissolved carbides formed by segregation of alloying elements on the hardness of the powder-metallurgical (PM) high-alloy tool steels (HATS). It explains the calculation of exact stoichiometric carbon content that depends on the required martensite hardness, amount of carbon forming alloying elements, types of undissolved carbides during austenitizing, and the densities of the carbides. Microhardness values for carbides in HATS are also listed.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006109
EISBN: 978-1-62708-175-7
Abstract
This article describes the methods for determining the flow rate of metal powders. It examines the factors affecting flow rate, apparent density, and angle of repose of metal powders. The article reviews the frictional properties, cohesive strength, frictional properties, tap density, and compressibility of metal powders. It explains the mechanisms of powder segregation. The article provides information on green strength and springback value of rectangular test bar. It concludes with a discussion on the chemical composition of metal powders.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006083
EISBN: 978-1-62708-175-7
Abstract
Warm compaction uses both powder heating and die heating to effect higher component densities, whereas warm die compaction uses only die heating to achieve higher density. This article explains the influences of green and sintered properties and pore-free density during compaction of materials. It provides information on the concept of pore-free density and process considerations: die heating and powder heating. The article concludes with a review of the tooling design for warm compaction.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006119
EISBN: 978-1-62708-175-7
Abstract
Powder metallurgy (PM) stainless steels, as with conventional PM steels, are often used in the as-sintered condition. In addition to cost considerations, minimization of postsinter handling and secondary operations is also preferred because it reduces the potential for contamination of the parts with particulates and residues, which can result in the appearance of surface rust. This article provides information on various secondary operations, including tumbling, re-pressing, resin impregnation, annealing or heat treating, brazing, machining, and welding. It describes those aspects relating to welding of PM stainless steels, specifically, the effects of density, residual porosity, and sintered chemistry on weldability. Further, the article investigates the influence the sintering atmosphere has on machinability, as well as differences created by the presence of residual porosity.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006032
EISBN: 978-1-62708-175-7
Abstract
This article describes several factors, which help in determining the compressibility of metal powders: particle shape, density, composition, hardness, particle size, lubrication, and compacting. It discusses the uses of annealing metal powders and describes compressibility testing of the powders. The article details green strength and its mechanism and the variables affecting the strength. It also discusses two test methods for determining the green strength: the Rattler test and the transverse bend test.
Book: Powder Metallurgy
Series: ASM Handbook
Volume: 7
Publisher: ASM International
Published: 30 September 2015
DOI: 10.31399/asm.hb.v07.a0006074
EISBN: 978-1-62708-175-7
Abstract
This article describes the unique aspects of cold isostatic pressing (CIP) in comparison with die compaction, for powder metallurgy parts. It details the components of CIP equipment, including pressure vessels, pressure generators, and tooling material. The article reviews the part shapes and their influence in determining tap density of the filled mold. It provides a discussion on process parameters, such as dwell time, depressurization rate, evaluation of green strength and density, and thermal processing, and illustrates a process flowchart for the production of CIP parts.
Series: ASM Handbook
Volume: 4C
Publisher: ASM International
Published: 09 June 2014
DOI: 10.31399/asm.hb.v04c.a0005896
EISBN: 978-1-62708-167-2
Abstract
In an induction heating system, thermal and electromagnetic properties of heated materials make the greatest impact on the heat transfer and performance of induction heating process. This article focuses on major thermal properties, namely, thermal conductivity, heat capacity, and specific heat. It describes the two important electromagnetic properties, electrical resistivity (electrical conductivity) and magnetic permeability, which posses the most pronounced effect on the performance of the induction heating system, its efficiency, and selection of main design parameters. The article also discusses the magnetic properties of diamagnetic, paramagnetic, ferromagnetic, ferrimagnetic, antiferromagnetic, and metamagnetic materials.
Series: ASM Handbook
Volume: 4A
Publisher: ASM International
Published: 01 August 2013
DOI: 10.31399/asm.hb.v04a.a0005789
EISBN: 978-1-62708-165-8
Abstract
This article provides a discussion on probes for laboratory tests and resultant curves of industrial quenching processes. It describes the scope of the tests, and the calculation of heat-transfer coefficient (HTC) based on the tests. The article highlights the differences between the laboratory tests and characterization of industrial quenching processes. It reviews the importance of initial heat-flux density and first critical heat-flux density. The theoretical principle behind and the purpose of the temperature gradient method are discussed. The article provides information on the design of the probe, heat-extraction dynamics, and influence of wetting kinematics. It also includes discussions on the simplified 1-D temperature-distribution model, calculation of the HTC, and the finite-volume method for the heat-conduction equation.
Book Chapter
Series: ASM Handbook
Volume: 22A
Publisher: ASM International
Published: 01 December 2009
DOI: 10.31399/asm.hb.v22a.a0005442
EISBN: 978-1-62708-196-2
Abstract
This article contains a table that lists the density of metals and alloys. It presents information on aluminum, copper, iron, lead, magnesium, nickel, tin, titanium, and zinc, an their respective alloys. Information on wrought alloys, permanent magnet materials, precious metals, and rare earth metals is also listed.
Book: Casting
Series: ASM Handbook
Volume: 15
Publisher: ASM International
Published: 01 December 2008
DOI: 10.31399/asm.hb.v15.a0005240
EISBN: 978-1-62708-187-0
Abstract
There are several main sources of thermophysical property data that provide the most authoritative and comprehensive compilations of critically and systematically evaluated data that are presently available. This article provides thermophysical property data to assist in the materials properties selection for the simulation of casting processes. The measurements of thermophysical property are difficult due to high temperatures and the reactivity of some alloys. The article discusses the strategies adopted to minimize the effects of high temperatures and reactivity of alloys. It presents the thermophysical properties of pure metals and some commercial alloys and tabulates the enthalpy of fusion and solidus and liquidus temperatures for various alloys of commercial interest. The article also lists the density, thermal conductivity, surface tension, and viscosity for some commercial alloys.
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